RU2017122209A - Источник для нанесения покрытия - Google Patents

Источник для нанесения покрытия Download PDF

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RU2017122209A
RU2017122209A RU2017122209A RU2017122209A RU2017122209A RU 2017122209 A RU2017122209 A RU 2017122209A RU 2017122209 A RU2017122209 A RU 2017122209A RU 2017122209 A RU2017122209 A RU 2017122209A RU 2017122209 A RU2017122209 A RU 2017122209A
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phase
layer
source
composite
metal
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RU2017122209A
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RU2707375C2 (ru
RU2017122209A3 (ru
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Петер ПОЛЬЦИК
Забине ВЁРЛЕ
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Планзее Композит Материалс Гмбх
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/24Vacuum evaporation
    • C23C14/32Vacuum evaporation by explosion; by evaporation and subsequent ionisation of the vapours, e.g. ion-plating
    • C23C14/325Electric arc evaporation
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/34Sputtering
    • C23C14/3407Cathode assembly for sputtering apparatus, e.g. Target
    • C23C14/3414Metallurgical or chemical aspects of target preparation, e.g. casting, powder metallurgy
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    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/02Compacting only
    • BPERFORMING OPERATIONS; TRANSPORTING
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    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • BPERFORMING OPERATIONS; TRANSPORTING
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    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/14Both compacting and sintering simultaneously
    • BPERFORMING OPERATIONS; TRANSPORTING
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    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/14Both compacting and sintering simultaneously
    • B22F3/15Hot isostatic pressing
    • BPERFORMING OPERATIONS; TRANSPORTING
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    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/16Both compacting and sintering in successive or repeated steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
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    • B22F7/00Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression
    • B22F7/02Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression of composite layers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
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    • B22F7/00Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression
    • B22F7/06Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression of composite workpieces or articles from parts, e.g. to form tipped tools
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B15/00Layered products comprising a layer of metal
    • B32B15/01Layered products comprising a layer of metal all layers being exclusively metallic
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B15/00Layered products comprising a layer of metal
    • B32B15/02Layer formed of wires, e.g. mesh
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/04Making non-ferrous alloys by powder metallurgy
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    • C22C1/04Making non-ferrous alloys by powder metallurgy
    • C22C1/05Mixtures of metal powder with non-metallic powder
    • C22C1/059Making alloys comprising less than 5% by weight of dispersed reinforcing phases
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    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C32/00Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ
    • C22C32/0047Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with carbides, nitrides, borides or silicides as the main non-metallic constituents
    • C22C32/0078Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with carbides, nitrides, borides or silicides as the main non-metallic constituents only silicides
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    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/06Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
    • C23C14/14Metallic material, boron or silicon
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    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/34Sputtering
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32431Constructional details of the reactor
    • H01J37/32532Electrodes
    • H01J37/32614Consumable cathodes for arc discharge
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/34Gas-filled discharge tubes operating with cathodic sputtering
    • H01J37/3411Constructional aspects of the reactor
    • H01J37/3414Targets
    • H01J37/3426Material
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/34Gas-filled discharge tubes operating with cathodic sputtering
    • H01J37/3411Constructional aspects of the reactor
    • H01J37/3414Targets
    • H01J37/3426Material
    • H01J37/3429Plural materials
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/34Gas-filled discharge tubes operating with cathodic sputtering
    • H01J37/3488Constructional details of particle beam apparatus not otherwise provided for, e.g. arrangement, mounting, housing, environment; special provisions for cleaning or maintenance of the apparatus
    • H01J37/3491Manufacturing of targets
    • BPERFORMING OPERATIONS; TRANSPORTING
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    • B22F2202/00Treatment under specific physical conditions
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    • B22F2202/00Treatment under specific physical conditions
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    • B22F2301/00Metallic composition of the powder or its coating
    • B22F2301/20Refractory metals
    • B22F2301/205Titanium, zirconium or hafnium
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Claims (22)

1. Способ получения источника (1) для нанесения покрытия посредством физического осаждения из паровой фазы, в котором источник (1) для нанесения покрытия включает, по меньшей мере,
слой (2) мишени, состоящий из по меньшей мере двухфазного композита, который содержит металлическую фазу (М) и по меньшей мере одну дополнительную фазу (Р),
стабилизирующий механические свойства слой (3), который соединяют со слоем (2) мишени с одной стороны слоя (2) мишени,
отличающийся тем, что первую порошковую смесь (6), которая соответствует в показателях ее состава по меньшей мере двухфазному композиту, и вторую порошковую смесь (7), которая соответствует в показателях ее состава стабилизирующему механические свойства слою (3), уплотняют в горячем состоянии в виде наложенных друг на друга слоев.
2. Способ по п. 1, в котором наложенные друг на друга слои подвергают горячему прессованию.
3. Способ по п. 1 или 2, в котором в процессе уплотнения к наложенным друг на друга слоям прикладывают электрический ток и/или подвергают их индукционному нагреву.
4. Способ по любому из предшествующих пунктов, в котором первую и/или вторую порошковую смесь (6, 7) используют в форме только промежуточной предварительно уплотненной прессованной заготовки, а окончательное уплотнение и соединение осуществляют посредством уплотнения в горячем состоянии.
5. Способ по любому из предшествующих пунктов, в котором в качестве металлической фазы (М) по меньшей мере двухфазного композита используют титан или титановый сплав.
6. Способ по любому из предшествующих пунктов, в котором материал для металлической фазы (М) по меньшей мере двухфазного композита и материал стабилизирующего механические свойства слоя состоят по меньшей мере на 80 ат. % из одинакового металла.
7. Способ по любому из предшествующих пунктов, в котором дополнительную фазу (Р) используют в количестве более 25 об. %, исходя из по меньшей мере двухфазного композита.
8. Способ по любому из предшествующих пунктов, в котором в качестве дополнительной фазы (Р) используют элемент, отличный от титана и/или соединения титана.
9. Способ по любому из предшествующих пунктов, в котором первую и вторую порошковые смеси (6, 7) располагают одну над другой так, что они прилегают друг другу по своей полной площади.
10. Источник (1) для нанесения покрытия посредством физического осаждения из паровой фазы, включающий
слой (2) мишени, состоящий по меньшей мере из двухфазного композита, который содержит металлическую фазу (М) и по меньшей мере дополнительную фазу (Р), где металлическая фаза (М) и все дополнительные присутствующие фазы имеют температуру плавления более 1000°С,
стабилизирующий механические свойства слой (3), который соединен со слоем (2) мишени с одной стороны слоя (2) мишени,
отличающийся тем, что слой (2) мишени и стабилизирующий механические свойства слой (3) соединены посредством соединительной зоны (4), которая имеет повышающуюся концентрацию частиц дополнительной фазы (Р) по меньшей мере двухфазного композита в направлении от стабилизирующего механические свойства слоя (3) к слою (2) мишени, без образования границы раздела.
11. Источник (1) для нанесения покрытия по п. 10, в котором металлическая фаза (М) по меньшей мере двухфазного композита включает титан или сплав титана.
12. Источник (1) для нанесения покрытия по п. 10 или п. 11, в котором материал металлической фазы (М) по меньшей мере двухфазного композита и материал стабилизирующего механические свойства слоя (3) состоят по меньшей мере на 80 ат. % из одинакового металла.
13. Источник (1) для нанесения покрытия по пп. 10-12, в котором дополнительная фаза (Р) присутствует в количестве более 25 об. %, исходя из по меньшей мере двухфазного композита.
14. Источник (1) для нанесения покрытия по пп. 10-13, в котором дополнительная фаза (Р) состоит из элемента, отличного от титана и/или соединения титана.
15. Источник (1) для нанесения покрытия по пп. 10-14, в котором стабилизирующий механические свойства слой (3) состоит из того же металлического материала, который образует металлическую фазу (М) слоя (2) мишени, и по меньшей мере по существу не содержит частиц дополнительной фазы (Р) по меньшей мере двухфазного композита.
16. Источник (1) для нанесения покрытия по пп. 10-14, в котором стабилизирующий механические свойства слой (3) сам по себе состоит по меньшей мере из двухфазного композита.
RU2017122209A 2015-01-26 2016-01-20 Источник для нанесения покрытия RU2707375C2 (ru)

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Application Number Priority Date Filing Date Title
ATGM17/2015U AT14497U1 (de) 2015-01-26 2015-01-26 Beschichtungsquelle
ATGM17/2015 2015-01-26
PCT/EP2016/000092 WO2016120002A1 (de) 2015-01-26 2016-01-20 Beschichtungsquelle

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TWI658885B (zh) 2019-05-11
JP2018505313A (ja) 2018-02-22
KR102526957B1 (ko) 2023-04-27
CN107208257A (zh) 2017-09-26
JP2021046610A (ja) 2021-03-25
JP7116131B2 (ja) 2022-08-09
US10787735B2 (en) 2020-09-29
AT14497U1 (de) 2015-12-15
RU2707375C2 (ru) 2019-11-26
KR20170107442A (ko) 2017-09-25
WO2016120002A1 (de) 2016-08-04
EP3251145A1 (de) 2017-12-06
RU2017122209A3 (ru) 2019-05-17
TW201637753A (zh) 2016-11-01

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