RU2015105523A - Раствор, улучшающий прозрачность диоксидциркониевой керамики - Google Patents
Раствор, улучшающий прозрачность диоксидциркониевой керамики Download PDFInfo
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- RU2015105523A RU2015105523A RU2015105523A RU2015105523A RU2015105523A RU 2015105523 A RU2015105523 A RU 2015105523A RU 2015105523 A RU2015105523 A RU 2015105523A RU 2015105523 A RU2015105523 A RU 2015105523A RU 2015105523 A RU2015105523 A RU 2015105523A
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- zirconia
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- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 title claims abstract 45
- 239000000919 ceramic Substances 0.000 title claims 7
- 238000001179 sorption measurement Methods 0.000 claims abstract 10
- 238000003795 desorption Methods 0.000 claims abstract 9
- 239000000203 mixture Substances 0.000 claims abstract 9
- 239000002904 solvent Substances 0.000 claims abstract 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract 4
- 239000000654 additive Substances 0.000 claims abstract 4
- 230000000996 additive effect Effects 0.000 claims abstract 4
- 239000008139 complexing agent Substances 0.000 claims abstract 4
- 239000003550 marker Substances 0.000 claims abstract 4
- 239000000126 substance Substances 0.000 claims abstract 4
- 239000002562 thickening agent Substances 0.000 claims abstract 4
- 238000005452 bending Methods 0.000 claims abstract 3
- 150000001768 cations Chemical group 0.000 claims abstract 3
- 150000002500 ions Chemical class 0.000 claims abstract 3
- 239000011148 porous material Substances 0.000 claims abstract 3
- 229910052688 Gadolinium Inorganic materials 0.000 claims abstract 2
- 229910052775 Thulium Inorganic materials 0.000 claims abstract 2
- 229910052769 Ytterbium Inorganic materials 0.000 claims abstract 2
- 239000003086 colorant Substances 0.000 claims abstract 2
- 229910052746 lanthanum Inorganic materials 0.000 claims abstract 2
- 229910052749 magnesium Inorganic materials 0.000 claims abstract 2
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract 2
- 229910052727 yttrium Inorganic materials 0.000 claims abstract 2
- 239000000243 solution Substances 0.000 claims 13
- 150000003839 salts Chemical class 0.000 claims 5
- 239000011351 dental ceramic Substances 0.000 claims 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims 2
- 238000004438 BET method Methods 0.000 claims 2
- 238000000034 method Methods 0.000 claims 2
- 229920000058 polyacrylate Polymers 0.000 claims 2
- POILWHVDKZOXJZ-ARJAWSKDSA-M (z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 claims 1
- VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical compound NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 claims 1
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims 1
- DHMQDGOQFOQNFH-UHFFFAOYSA-M Aminoacetate Chemical compound NCC([O-])=O DHMQDGOQFOQNFH-UHFFFAOYSA-M 0.000 claims 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims 1
- JVTAAEKCZFNVCJ-UHFFFAOYSA-M Lactate Chemical compound CC(O)C([O-])=O JVTAAEKCZFNVCJ-UHFFFAOYSA-M 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000001298 alcohols Chemical class 0.000 claims 1
- 238000004458 analytical method Methods 0.000 claims 1
- 229940072107 ascorbate Drugs 0.000 claims 1
- 235000010323 ascorbic acid Nutrition 0.000 claims 1
- 239000011668 ascorbic acid Substances 0.000 claims 1
- 230000005540 biological transmission Effects 0.000 claims 1
- 239000007853 buffer solution Substances 0.000 claims 1
- 229910001424 calcium ion Inorganic materials 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 claims 1
- 238000004040 coloring Methods 0.000 claims 1
- 150000003983 crown ethers Chemical class 0.000 claims 1
- 239000002739 cryptand Substances 0.000 claims 1
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- 229940071106 ethylenediaminetetraacetate Drugs 0.000 claims 1
- OUDSFQBUEBFSPS-UHFFFAOYSA-N ethylenediaminetriacetic acid Chemical compound OC(=O)CNCCN(CC(O)=O)CC(O)=O OUDSFQBUEBFSPS-UHFFFAOYSA-N 0.000 claims 1
- 235000002864 food coloring agent Nutrition 0.000 claims 1
- 150000004676 glycans Chemical class 0.000 claims 1
- RBNPOMFGQQGHHO-UHFFFAOYSA-N glyceric acid Chemical compound OCC(O)C(O)=O RBNPOMFGQQGHHO-UHFFFAOYSA-N 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 239000007943 implant Substances 0.000 claims 1
- 229910052742 iron Inorganic materials 0.000 claims 1
- 150000002576 ketones Chemical class 0.000 claims 1
- 229910052748 manganese Inorganic materials 0.000 claims 1
- 229920000609 methyl cellulose Polymers 0.000 claims 1
- 239000001923 methylcellulose Substances 0.000 claims 1
- 235000010981 methylcellulose Nutrition 0.000 claims 1
- 229910052750 molybdenum Inorganic materials 0.000 claims 1
- MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical compound OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 claims 1
- 235000006408 oxalic acid Nutrition 0.000 claims 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical compound N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 claims 1
- 229920005862 polyol Polymers 0.000 claims 1
- 150000003077 polyols Chemical class 0.000 claims 1
- 229920001282 polysaccharide Polymers 0.000 claims 1
- 239000005017 polysaccharide Substances 0.000 claims 1
- RKCAIXNGYQCCAL-UHFFFAOYSA-N porphin Chemical compound N1C(C=C2N=C(C=C3NC(=C4)C=C3)C=C2)=CC=C1C=C1C=CC4=N1 RKCAIXNGYQCCAL-UHFFFAOYSA-N 0.000 claims 1
- 239000003755 preservative agent Substances 0.000 claims 1
- 230000002335 preservative effect Effects 0.000 claims 1
- 102000004196 processed proteins & peptides Human genes 0.000 claims 1
- 108090000765 processed proteins & peptides Proteins 0.000 claims 1
- AOHJOMMDDJHIJH-UHFFFAOYSA-N propylenediamine Chemical compound CC(N)CN AOHJOMMDDJHIJH-UHFFFAOYSA-N 0.000 claims 1
- YGSDEFSMJLZEOE-UHFFFAOYSA-M salicylate Chemical compound OC1=CC=CC=C1C([O-])=O YGSDEFSMJLZEOE-UHFFFAOYSA-M 0.000 claims 1
- 229960001860 salicylate Drugs 0.000 claims 1
- 238000005245 sintering Methods 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000003381 stabilizer Substances 0.000 claims 1
- 238000010186 staining Methods 0.000 claims 1
- 150000005846 sugar alcohols Polymers 0.000 claims 1
- 229910052720 vanadium Inorganic materials 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 239000000230 xanthan gum Substances 0.000 claims 1
- 229920001285 xanthan gum Polymers 0.000 claims 1
- 229940082509 xanthan gum Drugs 0.000 claims 1
- 235000010493 xanthan gum Nutrition 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
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| PCT/US2013/029743 WO2014021940A1 (en) | 2012-08-03 | 2013-03-08 | Translucency enhancing solution for zirconia ceramics |
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| WO2014021940A1 (en) | 2012-08-03 | 2014-02-06 | 3M Innovative Properties Company | Translucency enhancing solution for zirconia ceramics |
| US10292795B2 (en) | 2012-09-20 | 2019-05-21 | 3M Innovation Properties Company | Coloring solution for zirconia ceramics |
| EP2909029A1 (en) | 2012-10-17 | 2015-08-26 | 3M Innovative Properties Company | Multi sectional dental zirconia milling block, process of production and use thereof |
| WO2016114265A1 (ja) * | 2015-01-15 | 2016-07-21 | 東ソー株式会社 | 透光性ジルコニア焼結体及びその製造方法並びにその用途 |
| WO2016191162A1 (en) * | 2015-05-28 | 2016-12-01 | 3M Innovative Properties Company | Additive manufacturing process for producing ceramic articles using a sol containing nano-sized particles |
| CH711817A1 (de) * | 2015-11-27 | 2017-05-31 | Lakeview Innovation Ltd | Verfahren und Vorrichtung zur Herstellung von Keramikteilen. |
| JP6093900B1 (ja) * | 2016-07-29 | 2017-03-08 | 株式会社松風 | 内部を着色された歯科用仮焼成体 |
| CN117800719A (zh) * | 2017-02-21 | 2024-04-02 | 株式会社松风 | 氧化锆被切削体及其制造方法、透明性提高液及其使用方法 |
| US10667992B2 (en) | 2017-03-16 | 2020-06-02 | James R. Glidewell Dental Ceramics, Inc. | Methods for enhancing optical and strength properties in ceramic bodies having applications in dental restorations |
| WO2019083967A1 (en) | 2017-10-23 | 2019-05-02 | James R. Glidewell Dental Ceramics, Inc. | CERAMIC BODY WITH ANTIMICROBIAL PROPERTIES AND METHODS OF MAKING SAME |
| US10974997B2 (en) | 2018-01-29 | 2021-04-13 | James R. Glidewell Dental Ceramics, Inc. | Polychromatic zirconia bodies and methods of making the same |
| EP4371548B1 (en) * | 2018-03-30 | 2025-11-05 | Shofu Inc. | Method for applying an opaque imparting liquid for zirconia |
| KR102798872B1 (ko) | 2018-12-26 | 2025-04-21 | 쿠라레 노리타케 덴탈 가부시키가이샤 | 지르코니아용 착색 용액 |
| EP3935027B1 (en) * | 2019-03-04 | 2025-09-10 | Solventum Intellectual Properties Company | Process for producing a colored dental zirconia article |
| CN110078502B (zh) * | 2019-05-17 | 2021-07-13 | 福州大学 | 一种提高8ysz硬度的方法 |
| WO2021105848A1 (en) * | 2019-11-26 | 2021-06-03 | 3M Innovative Properties Company | Process for treating a porous dental zirconia block with coloring solutions |
| WO2021115727A1 (en) * | 2019-12-13 | 2021-06-17 | Institut Straumann Ag | Functionalized ceramic article |
| US12005131B2 (en) * | 2020-02-03 | 2024-06-11 | James R. Glidewell Dental Ceramics, Inc. | Method of masking a dental support structure of a dental prosthesis made of highly translucent ceramic material |
| US11672632B2 (en) | 2020-10-05 | 2023-06-13 | Pritidenta Gmbh | Multi-layered zirconia dental blank with reverse layers, process for its preparation and uses thereof |
| US12194112B2 (en) * | 2020-10-16 | 2025-01-14 | Shofu Inc. | Indium-containing translucency improving liquid for dental zirconia calcined body |
| US20240199494A1 (en) * | 2021-04-16 | 2024-06-20 | Kuraray Noritake Dental lnc. | Zirconia molded body, zirconia pre-sintered body, and zirconia sintered body, and methods of production thereof |
| CN113321520B (zh) * | 2021-07-04 | 2022-05-27 | 湖南洛兰新材料有限公司 | 一种抗粘结耐高温承烧器及其制备方法 |
| US20230303459A1 (en) * | 2022-03-28 | 2023-09-28 | James R. Glidewell Dental Ceramics, Inc. | FABRICATION OF POLYCHROMATIC/POLYTRANSLUCENT ZIRCONIA BLOCK FROM PRE-SHADED ZrO2 BLOCK BY INFILTRATION |
| CN117088674B (zh) * | 2023-07-07 | 2025-07-29 | 中国美术学院 | 一种轻质3d打印隔热防滑陶瓷杯的制备方法 |
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| DE19904522C5 (de) | 1999-02-04 | 2013-11-14 | 3M Deutschland Gmbh | Einfärbung von keramischem Zahnersatz mittels ionischer oder komplexhaltiger Lösungen |
| DE60302225T2 (de) | 2003-06-13 | 2006-08-10 | 3M Espe Ag | Gleichmässig gefärbte Gerüstkeramik sowie Färbelösung |
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| EP1961719A1 (en) | 2007-02-08 | 2008-08-27 | 3M Innovative Properties Company | Colouring solution for dental ceramic framework and related methods |
| EP2025659A1 (en) * | 2007-07-23 | 2009-02-18 | 3M Innovative Properties Company | Colouring solution for dental ceramic articles and related methods |
| JP4321636B2 (ja) | 2007-07-27 | 2009-08-26 | セイコーエプソン株式会社 | 歯科用インプラントの製造方法 |
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| CN102344285B (zh) | 2011-07-04 | 2013-04-17 | 辽宁爱尔创生物材料有限公司 | 改变牙科氧化锆材料透光性的方法 |
| WO2013022612A1 (en) | 2011-08-11 | 2013-02-14 | 3M Innovative Properties Company | Colouring solution for selectively treating the surface of dental ceramic and related methods |
| WO2014021940A1 (en) | 2012-08-03 | 2014-02-06 | 3M Innovative Properties Company | Translucency enhancing solution for zirconia ceramics |
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- 2013-03-08 BR BR112015002468A patent/BR112015002468A2/pt not_active Application Discontinuation
- 2013-03-08 EP EP13711226.4A patent/EP2879614B1/en active Active
- 2013-03-08 JP JP2015525416A patent/JP6382812B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN104918577B (zh) | 2018-10-23 |
| WO2014021940A1 (en) | 2014-02-06 |
| CN104918577A (zh) | 2015-09-16 |
| BR112015002468A2 (pt) | 2017-07-04 |
| US9872746B2 (en) | 2018-01-23 |
| US20150157430A1 (en) | 2015-06-11 |
| JP6382812B2 (ja) | 2018-08-29 |
| EP2879614B1 (en) | 2017-12-06 |
| JP2015532629A (ja) | 2015-11-12 |
| EP2879614A1 (en) | 2015-06-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FA92 | Acknowledgement of application withdrawn (lack of supplementary materials submitted) |
Effective date: 20160907 |