RU2008115525A - Способ получения полиизоцианатов - Google Patents
Способ получения полиизоцианатов Download PDFInfo
- Publication number
- RU2008115525A RU2008115525A RU2008115525/04A RU2008115525A RU2008115525A RU 2008115525 A RU2008115525 A RU 2008115525A RU 2008115525/04 A RU2008115525/04 A RU 2008115525/04A RU 2008115525 A RU2008115525 A RU 2008115525A RU 2008115525 A RU2008115525 A RU 2008115525A
- Authority
- RU
- Russia
- Prior art keywords
- isomers
- polyisocyanate
- polyisocyanates
- impurities
- solvent
- Prior art date
Links
- 229920001228 polyisocyanate Polymers 0.000 title claims abstract 26
- 239000005056 polyisocyanate Substances 0.000 title claims abstract 26
- 238000004519 manufacturing process Methods 0.000 title claims 4
- 239000012535 impurity Substances 0.000 claims abstract 11
- 239000002904 solvent Substances 0.000 claims abstract 7
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 claims abstract 6
- 238000000034 method Methods 0.000 claims abstract 6
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 claims abstract 5
- 125000003118 aryl group Chemical group 0.000 claims abstract 5
- QARVLSVVCXYDNA-UHFFFAOYSA-N bromobenzene Chemical compound BrC1=CC=CC=C1 QARVLSVVCXYDNA-UHFFFAOYSA-N 0.000 claims abstract 4
- 150000001875 compounds Chemical class 0.000 claims abstract 4
- 239000012442 inert solvent Substances 0.000 claims abstract 4
- LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 claims abstract 4
- OCJBOOLMMGQPQU-UHFFFAOYSA-N 1,4-dichlorobenzene Chemical compound ClC1=CC=C(Cl)C=C1 OCJBOOLMMGQPQU-UHFFFAOYSA-N 0.000 claims abstract 3
- XEMRAKSQROQPBR-UHFFFAOYSA-N (trichloromethyl)benzene Chemical class ClC(Cl)(Cl)C1=CC=CC=C1 XEMRAKSQROQPBR-UHFFFAOYSA-N 0.000 claims abstract 2
- RELMFMZEBKVZJC-UHFFFAOYSA-N 1,2,3-trichlorobenzene Chemical class ClC1=CC=CC(Cl)=C1Cl RELMFMZEBKVZJC-UHFFFAOYSA-N 0.000 claims abstract 2
- WDCYWAQPCXBPJA-UHFFFAOYSA-N 1,3-dinitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC([N+]([O-])=O)=C1 WDCYWAQPCXBPJA-UHFFFAOYSA-N 0.000 claims abstract 2
- BFCFYVKQTRLZHA-UHFFFAOYSA-N 1-chloro-2-nitrobenzene Chemical class [O-][N+](=O)C1=CC=CC=C1Cl BFCFYVKQTRLZHA-UHFFFAOYSA-N 0.000 claims abstract 2
- RNEMUWDQJSRDMQ-UHFFFAOYSA-N 1-chloro-2-propan-2-ylbenzene Chemical compound CC(C)C1=CC=CC=C1Cl RNEMUWDQJSRDMQ-UHFFFAOYSA-N 0.000 claims abstract 2
- CAHQGWAXKLQREW-UHFFFAOYSA-N Benzal chloride Chemical class ClC(Cl)C1=CC=CC=C1 CAHQGWAXKLQREW-UHFFFAOYSA-N 0.000 claims abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract 2
- BVJSGOYEEDZAGW-UHFFFAOYSA-N [chloro(nitro)methyl]benzene Chemical class [O-][N+](=O)C(Cl)C1=CC=CC=C1 BVJSGOYEEDZAGW-UHFFFAOYSA-N 0.000 claims abstract 2
- KCXMKQUNVWSEMD-UHFFFAOYSA-N benzyl chloride Chemical class ClCC1=CC=CC=C1 KCXMKQUNVWSEMD-UHFFFAOYSA-N 0.000 claims abstract 2
- 238000006243 chemical reaction Methods 0.000 claims abstract 2
- CZZYITDELCSZES-UHFFFAOYSA-N diphenylmethane Chemical class C=1C=CC=CC=1CC1=CC=CC=C1 CZZYITDELCSZES-UHFFFAOYSA-N 0.000 claims abstract 2
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims abstract 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims abstract 2
- 239000007788 liquid Substances 0.000 claims abstract 2
- 239000000203 mixture Substances 0.000 claims abstract 2
- VLZLOWPYUQHHCG-UHFFFAOYSA-N nitromethylbenzene Chemical compound [O-][N+](=O)CC1=CC=CC=C1 VLZLOWPYUQHHCG-UHFFFAOYSA-N 0.000 claims abstract 2
- 229920000768 polyamine Polymers 0.000 claims abstract 2
- 150000001491 aromatic compounds Chemical class 0.000 claims 2
- 238000001704 evaporation Methods 0.000 claims 2
- 230000008020 evaporation Effects 0.000 claims 2
- DYSXLQBUUOPLBB-UHFFFAOYSA-N 2,3-dinitrotoluene Chemical class CC1=CC=CC([N+]([O-])=O)=C1[N+]([O-])=O DYSXLQBUUOPLBB-UHFFFAOYSA-N 0.000 claims 1
- 229920005830 Polyurethane Foam Polymers 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- 229940117389 dichlorobenzene Drugs 0.000 claims 1
- 238000004821 distillation Methods 0.000 claims 1
- 239000011496 polyurethane foam Substances 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 238000005829 trimerization reaction Methods 0.000 claims 1
- 239000003039 volatile agent Substances 0.000 claims 1
- 150000004768 bromobenzenes Chemical class 0.000 abstract 1
- 150000004816 dichlorobenzenes Chemical class 0.000 abstract 1
- VMMLSJNPNVTYMN-UHFFFAOYSA-N dinitromethylbenzene Chemical class [O-][N+](=O)C([N+]([O-])=O)C1=CC=CC=C1 VMMLSJNPNVTYMN-UHFFFAOYSA-N 0.000 abstract 1
- YXFVVABEGXRONW-UHFFFAOYSA-N toluene Substances CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
- C08G18/7657—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings
- C08G18/7664—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings containing alkylene polyphenyl groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
- C07C263/20—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/02—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only
- C08G18/022—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only the polymeric products containing isocyanurate groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2110/00—Foam properties
- C08G2110/0008—Foam properties flexible
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyurethanes Or Polyureas (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP05108750 | 2005-09-22 | ||
| EP05108750.0 | 2005-09-22 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RU2008115525A true RU2008115525A (ru) | 2009-10-27 |
Family
ID=35707266
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2008115525/04A RU2008115525A (ru) | 2005-09-22 | 2006-08-29 | Способ получения полиизоцианатов |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US20080249202A1 (enExample) |
| EP (1) | EP1928928B1 (enExample) |
| JP (1) | JP2009508904A (enExample) |
| KR (1) | KR101290897B1 (enExample) |
| CN (1) | CN101268113B (enExample) |
| AU (1) | AU2006298927B2 (enExample) |
| BR (1) | BRPI0616145A2 (enExample) |
| CA (1) | CA2621331A1 (enExample) |
| ES (1) | ES2663870T3 (enExample) |
| HU (1) | HUE036153T2 (enExample) |
| PT (1) | PT1928928T (enExample) |
| RU (1) | RU2008115525A (enExample) |
| WO (1) | WO2007039362A1 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2014641A3 (en) * | 2007-06-06 | 2009-03-18 | Huntsman International Llc | Process for preparing mixtures of diphenylmethane diisocyanates and polyphenyl polymethylene polyisocyanates |
| JP6710159B2 (ja) * | 2014-04-11 | 2020-06-17 | コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ | 気相中においてキシリレンジイソシアネートを製造するための方法 |
| KR102187896B1 (ko) | 2019-01-24 | 2020-12-08 | 주식회사 코씨드바이오팜 | 식물추출물을 함유하는 세포보습, 세포간 보습, 피부 장벽보습에 효과적인 화장료 조성물 |
| KR102839458B1 (ko) * | 2020-12-30 | 2025-07-25 | 한화솔루션 주식회사 | 이소시아네이트 화합물의 제조 방법 |
| CN115490829B (zh) * | 2021-06-17 | 2025-04-01 | 万华化学集团股份有限公司 | 一种异氰酸酯组合物及其制备方法、一种光学材料 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3287387A (en) | 1963-07-29 | 1966-11-22 | Olin Mathieson | Process for the production of aromatic isocyanates |
| BE631132A (enExample) * | 1965-05-17 | |||
| FR1469105A (fr) | 1965-12-27 | 1967-02-10 | Toulousaine De Prod Chim Toloc | Procédé de fabrication d'esters isocyaniques |
| US3622577A (en) * | 1968-11-08 | 1971-11-23 | Du Pont | Trimerization of organic isocyanates |
| DE3129270A1 (de) * | 1981-07-24 | 1983-02-10 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von polyisocyanaten |
| DE3413174A1 (de) * | 1984-04-07 | 1985-10-17 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von polyisocyanaten |
| BR9510351A (pt) * | 1994-11-17 | 1997-12-23 | Bayer Ag | Processo para a preparação de isocianatos |
| EP0816357B1 (en) * | 1996-06-27 | 2002-01-09 | Pfizer Inc. | Substituted indazole derivatives |
| US5770659A (en) * | 1997-11-10 | 1998-06-23 | Arco Chemical Technology, L.P. | Process for making storage-stable epoxy-capped polyetherester resins |
| US6306918B1 (en) * | 1999-03-09 | 2001-10-23 | Kao Corporation | Semi-rigid polyurethane foam |
| US6423758B2 (en) * | 1999-06-03 | 2002-07-23 | Gaska Tape, Inc. | Low volatility cellular foam |
| US6458860B1 (en) * | 2001-06-01 | 2002-10-01 | Huntsman Petrochemical Corporation | Advances in urethane foam catalysis |
| EP1371633A1 (en) * | 2002-06-14 | 2003-12-17 | Bayer Ag | Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column |
| DE10260092A1 (de) | 2002-12-19 | 2004-07-01 | Basf Ag | Verfahren zur Reinigung von Isocyanaten |
| DE10261187A1 (de) * | 2002-12-20 | 2004-07-08 | Basf Ag | Verfahren zur Herstellung von Isocyanaten |
| DE102004005319A1 (de) * | 2004-02-04 | 2005-08-25 | Bayer Materialscience Ag | Verfahren zur Herstellung von hochreinem 2,4'-Methylendiphenyldiisocyanat |
| BRPI0418975B1 (pt) | 2004-07-28 | 2015-07-28 | Huntsman Int Llc | Processo para a produção de um poliisocianato |
-
2006
- 2006-08-29 RU RU2008115525/04A patent/RU2008115525A/ru not_active Application Discontinuation
- 2006-08-29 US US12/067,197 patent/US20080249202A1/en not_active Abandoned
- 2006-08-29 JP JP2008531654A patent/JP2009508904A/ja active Pending
- 2006-08-29 BR BRPI0616145-6A patent/BRPI0616145A2/pt not_active IP Right Cessation
- 2006-08-29 ES ES06793066.9T patent/ES2663870T3/es active Active
- 2006-08-29 KR KR1020087006922A patent/KR101290897B1/ko not_active Expired - Fee Related
- 2006-08-29 HU HUE06793066A patent/HUE036153T2/hu unknown
- 2006-08-29 WO PCT/EP2006/065786 patent/WO2007039362A1/en not_active Ceased
- 2006-08-29 CN CN2006800343965A patent/CN101268113B/zh not_active Expired - Fee Related
- 2006-08-29 CA CA002621331A patent/CA2621331A1/en not_active Abandoned
- 2006-08-29 PT PT67930669T patent/PT1928928T/pt unknown
- 2006-08-29 AU AU2006298927A patent/AU2006298927B2/en not_active Ceased
- 2006-08-29 EP EP06793066.9A patent/EP1928928B1/en not_active Revoked
Also Published As
| Publication number | Publication date |
|---|---|
| HUE036153T2 (hu) | 2018-06-28 |
| WO2007039362A1 (en) | 2007-04-12 |
| KR20080057247A (ko) | 2008-06-24 |
| ES2663870T3 (es) | 2018-04-17 |
| CN101268113B (zh) | 2013-05-22 |
| US20080249202A1 (en) | 2008-10-09 |
| CN101268113A (zh) | 2008-09-17 |
| BRPI0616145A2 (pt) | 2011-06-07 |
| JP2009508904A (ja) | 2009-03-05 |
| EP1928928B1 (en) | 2018-02-21 |
| PT1928928T (pt) | 2018-03-26 |
| AU2006298927A1 (en) | 2007-04-12 |
| EP1928928A1 (en) | 2008-06-11 |
| KR101290897B1 (ko) | 2013-07-29 |
| AU2006298927B2 (en) | 2011-07-07 |
| CA2621331A1 (en) | 2007-04-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FA92 | Acknowledgement of application withdrawn (lack of supplementary materials submitted) |
Effective date: 20110914 |