PL93670B1 - - Google Patents

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Publication number
PL93670B1
PL93670B1 PL1974175326A PL17532674A PL93670B1 PL 93670 B1 PL93670 B1 PL 93670B1 PL 1974175326 A PL1974175326 A PL 1974175326A PL 17532674 A PL17532674 A PL 17532674A PL 93670 B1 PL93670 B1 PL 93670B1
Authority
PL
Poland
Prior art keywords
formula
bromo
mole
ethyl
c3h7s
Prior art date
Application number
PL1974175326A
Other languages
English (en)
Chinese (zh)
Original Assignee
Bayer Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Ag filed Critical Bayer Ag
Publication of PL93670B1 publication Critical patent/PL93670B1/zh

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Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/14Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing aromatic radicals
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/06Phosphorus compounds without P—C bonds
    • C07F9/16Esters of thiophosphoric acids or thiophosphorous acids
    • C07F9/165Esters of thiophosphoric acids
    • C07F9/18Esters of thiophosphoric acids with hydroxyaryl compounds

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Molecular Biology (AREA)
  • Agronomy & Crop Science (AREA)
  • Biochemistry (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Claims (1)

1. Zastrzezenie patentowe Srodek owadobójczy i roztoczobójczy, znamienny tym, ze zawiera jako substancje czynna ester O- etylo-S-n-prop'ylo-0-(2-bromo-4-cyjanofenylowy) kwasu tionotiolofosforowego o wzorze 1, oraz zna¬ ne nosniki i/lub substancje powierzchniowo czyn¬ ne. 15 Wyzej podany test toksycznosci wskazuje na niespodziewanie mala toksycznosc zwiazku o wzo¬ rze 1 w porównaniu ze zwiazkami analogicznymi o podobnym kierunku dzialania. Przyklad wytwarzania. Przyklad II. Do mieszaniny 19,8 g (0,1 mola) -2-bromo-4-cyjanofenolu i 14,5 g (0,105 mola) we¬ glanu potasu w 200 ml acetonitrylu wkrapla sie 21,8 g (0,1 mola) chlorku kwasu O-etylo-S-n-pro- pylotionotiolofosforowego. Reakcje prowadzi sie jeszcze przez 3 godziny w temperaturze 50°C, od¬ sacza wytracony chlorek potasu i przesacz wy¬ lewa do 500 ml toluenu. Przemywa sie nasyconym roztworem dwuweglanu sodu i woda, po czym osusza" siarczanem sodu. Rozpuszczalnik oddesty- lowuje sie i pozostalosc oczyszcza przez „poddesty- lowanie". -¦ T '. Otrzymuje sie 19 g (50% wydajnosci teoretycz¬ nej) estru 0-etylo-S-n-propyloU(2-bromu-4-cyja- nofenylowego) kwasu tionotiolofosforowego o wzo¬ rze 1 w postaci zóltego oleju o wspólczynniku za¬ lamania swiatla n^ =1,5802 60 6593 670 /P-o-f ycN n-C3H7S x=/ Wzór 1 C2H5°\? )P-Hal n-C3H75 Br ho-\2ycu Wzór 2 Wzór 3 0-P(0C2H5)j C2H5°\? /^\ -C3HrS /r 3H5^_0 HCln-C3H7S/ Schemat OZGraf. Lz. 1420 (100+25 egz.) Cena 10 zl PL PL
PL1974175326A 1973-11-06 1974-11-04 PL93670B1 (pl)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19732355442 DE2355442A1 (de) 1973-11-06 1973-11-06 0-aethyl-s-n-propyl-0-(2-brom-4-cyanophenyl)-thionothiolphosphorsaeureester, verfahren zu seiner herstellung und seine verwendung als insektizid und akarizid

Publications (1)

Publication Number Publication Date
PL93670B1 true PL93670B1 (pl) 1977-06-30

Family

ID=5897329

Family Applications (1)

Application Number Title Priority Date Filing Date
PL1974175326A PL93670B1 (pl) 1973-11-06 1974-11-04

Country Status (25)

Country Link
US (1) US3966850A (pl)
JP (2) JPS5077349A (pl)
AT (1) AT327221B (pl)
AU (1) AU7502474A (pl)
BE (1) BE821871A (pl)
BR (1) BR7409233A (pl)
CA (1) CA1034588A (pl)
CH (1) CH575428A5 (pl)
CS (1) CS181277B2 (pl)
DD (1) DD116047A5 (pl)
DE (1) DE2355442A1 (pl)
DK (1) DK138654C (pl)
EG (1) EG11253A (pl)
ES (1) ES431664A1 (pl)
FR (1) FR2249620B1 (pl)
GB (1) GB1438748A (pl)
HU (1) HU169828B (pl)
IE (1) IE40101B1 (pl)
IL (1) IL45992A (pl)
LU (1) LU71233A1 (pl)
NL (1) NL7414362A (pl)
PL (1) PL93670B1 (pl)
SU (1) SU559618A3 (pl)
TR (1) TR17857A (pl)
ZA (1) ZA747093B (pl)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06347523A (ja) * 1993-06-04 1994-12-22 Nec Corp バッテリ状態検出装置

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4924656B1 (pl) * 1970-03-13 1974-06-25

Also Published As

Publication number Publication date
JPS5077349A (pl) 1975-06-24
DD116047A5 (pl) 1975-11-05
JPS5071833A (pl) 1975-06-14
AT327221B (de) 1976-01-26
IE40101B1 (en) 1979-03-14
FR2249620A1 (pl) 1975-05-30
EG11253A (en) 1977-08-15
NL7414362A (nl) 1975-05-09
IE40101L (en) 1975-05-06
HU169828B (pl) 1977-02-28
GB1438748A (en) 1976-06-09
DK138654C (da) 1979-03-12
TR17857A (tr) 1976-05-12
BE821871A (fr) 1975-05-05
DE2355442A1 (de) 1975-05-07
BR7409233A (pt) 1976-05-11
CA1034588A (en) 1978-07-11
FR2249620B1 (pl) 1978-02-24
US3966850A (en) 1976-06-29
CH575428A5 (pl) 1976-05-14
CS181277B2 (en) 1978-03-31
ZA747093B (en) 1975-11-26
ES431664A1 (es) 1976-11-16
SU559618A3 (ru) 1977-05-25
AU7502474A (en) 1976-05-06
DK138654B (da) 1978-10-09
DK575774A (pl) 1975-07-07
IL45992A (en) 1977-11-30
LU71233A1 (pl) 1975-08-20
ATA881874A (de) 1975-04-15
IL45992A0 (en) 1975-02-10

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