PL54176B1 - - Google Patents
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- Publication number
- PL54176B1 PL54176B1 PL108225A PL10822565A PL54176B1 PL 54176 B1 PL54176 B1 PL 54176B1 PL 108225 A PL108225 A PL 108225A PL 10822565 A PL10822565 A PL 10822565A PL 54176 B1 PL54176 B1 PL 54176B1
- Authority
- PL
- Poland
- Prior art keywords
- mixture
- benzene
- acetone
- methanol
- extracted
- Prior art date
Links
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 50
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 42
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 36
- 239000000203 mixture Substances 0.000 claims description 26
- 229930182470 glycoside Natural products 0.000 claims description 22
- 150000002338 glycosides Chemical class 0.000 claims description 22
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 21
- 239000002904 solvent Substances 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 15
- QBILRDAMJUPXCX-UHFFFAOYSA-N Corchoroside A Chemical compound C1C(O)C(O)C(C)OC1OC1CC2(O)CCC3C4(O)CCC(C=5COC(=O)C=5)C4(C)CCC3C2(C=O)CC1 QBILRDAMJUPXCX-UHFFFAOYSA-N 0.000 claims description 12
- HKNQDCBTAOHPIM-UHFFFAOYSA-N Helveticosid Natural products CC1OCC(CC(O)C1O)OC2CCC3(C=O)C4CCC5(C)C(CCC5(O)C4CCC3(O)C2)C6=CC(=O)OC6 HKNQDCBTAOHPIM-UHFFFAOYSA-N 0.000 claims description 12
- 239000012071 phase Substances 0.000 claims description 11
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000000284 extract Substances 0.000 claims description 6
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 claims description 6
- DQTACWJQVHJQDY-UHFFFAOYSA-N O.OC.CCOC(C)=O.C1=CC=CC=C1 Chemical compound O.OC.CCOC(C)=O.C1=CC=CC=C1 DQTACWJQVHJQDY-UHFFFAOYSA-N 0.000 claims description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 5
- 239000008346 aqueous phase Substances 0.000 claims description 5
- 238000002955 isolation Methods 0.000 claims description 5
- 239000011780 sodium chloride Substances 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- 238000000605 extraction Methods 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- 239000012074 organic phase Substances 0.000 claims description 3
- 238000004821 distillation Methods 0.000 claims description 2
- 238000010828 elution Methods 0.000 claims description 2
- YNQLUTRBYVCPMQ-UHFFFAOYSA-N alpha-methyl toluene Natural products CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 claims 1
- 230000001166 anti-perspirative effect Effects 0.000 claims 1
- 239000003213 antiperspirant Substances 0.000 claims 1
- 229910052593 corundum Inorganic materials 0.000 claims 1
- 238000010790 dilution Methods 0.000 claims 1
- 239000012895 dilution Substances 0.000 claims 1
- 239000004615 ingredient Substances 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 239000011877 solvent mixture Substances 0.000 claims 1
- 229910001845 yogo sapphire Inorganic materials 0.000 claims 1
- 239000000395 magnesium oxide Substances 0.000 description 3
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 3
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 241000146985 Erysimum perofskianum Species 0.000 description 2
- ZHNUHDYFZUAESO-UHFFFAOYSA-N Formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- DWCBZUWYUAIEEP-UHFFFAOYSA-N 2-bromo-n-ethylbenzamide Chemical compound CCNC(=O)C1=CC=CC=C1Br DWCBZUWYUAIEEP-UHFFFAOYSA-N 0.000 description 1
- 229930192810 Corchoroside Natural products 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000286783 Erysimum canescens Species 0.000 description 1
- 206010027406 Mesothelioma Diseases 0.000 description 1
- 241000283984 Rodentia Species 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 239000006286 aqueous extract Substances 0.000 description 1
- TXHIDIHEXDFONW-UHFFFAOYSA-N benzene;propan-2-one Chemical compound CC(C)=O.C1=CC=CC=C1 TXHIDIHEXDFONW-UHFFFAOYSA-N 0.000 description 1
- LRHPLDYGYMQRHN-UHFFFAOYSA-N butyl alcohol Substances CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 1
- 230000000747 cardiac effect Effects 0.000 description 1
- 230000003177 cardiotonic effect Effects 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 239000003480 eluent Substances 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 239000000401 methanolic extract Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 230000003389 potentiating effect Effects 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 238000004809 thin layer chromatography Methods 0.000 description 1
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR55614A FR1473587A (fr) | 1965-04-02 | 1966-03-30 | Procédé d'extraction de l'hevéticoside et du corchoroside alpha |
| NL6604384A NL6604384A (OSRAM) | 1965-04-02 | 1966-04-01 | |
| DE19661617553 DE1617553A1 (de) | 1965-04-02 | 1966-04-01 | Verfahren zur Isolierung von Helvetikosid und Korchorosid A |
| GB1469866A GB1139466A (en) | 1965-04-02 | 1966-04-01 | Method of extracting helveticoside and corchoroside a |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL54176B1 true PL54176B1 (OSRAM) | 1967-10-25 |
Family
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