PL422573A1 - 3-[bis(hydroxyphosphinylmethyl)aminomethyl)-3,5,5-trimethylcyclohexylamine-bis(methylphosphinic) acid and method for producing it - Google Patents

3-[bis(hydroxyphosphinylmethyl)aminomethyl)-3,5,5-trimethylcyclohexylamine-bis(methylphosphinic) acid and method for producing it

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Publication number
PL422573A1
PL422573A1 PL422573A PL42257317A PL422573A1 PL 422573 A1 PL422573 A1 PL 422573A1 PL 422573 A PL422573 A PL 422573A PL 42257317 A PL42257317 A PL 42257317A PL 422573 A1 PL422573 A1 PL 422573A1
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PL
Poland
Prior art keywords
bis
acid
aminomethyl
hydroxyphosphinylmethyl
methylphosphinic
Prior art date
Application number
PL422573A
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Polish (pl)
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PL234794B1 (en
Inventor
Mirosław Soroka
Anna Brol
Łukasz Stala
Bartosz Jagusiak
Ciepacz Magdalena Klockar-
Original Assignee
Politechnika Wrocławska
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Politechnika Wrocławska filed Critical Politechnika Wrocławska
Priority to PL422573A priority Critical patent/PL234794B1/en
Publication of PL422573A1 publication Critical patent/PL422573A1/en
Publication of PL234794B1 publication Critical patent/PL234794B1/en

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Abstract

Zgłoszenie dotyczy kwasu 3-[bis(hydroksyfosfinylometylo)aminometylo)-3,5,5-trimetylocykloheksyloaminobis(metylofosfinowego) o wzorze 1. Kwas 3-[bis(hydroksyfosfinylome-tylo)aminometylo)-3,5,5-trimetylocykloheksyloaminobis(metylofosfinowy) jest przeznaczony do stosowania jako substrat do syntezy kwasu 3-[bis(fosfonometylo)aminometylo)-3,5,5-trimetylocykloheksyloaminobis(metylofosfonowego), a także innych produktów zawierających fragmenty strukturalne 5-amino-1,3,3-trimetylocykloheksanometanaminy i kwasu dimetylofosfinowego. Przedmiotem zgłoszenia jest też sposób wytwarzania kwasu 3-[bis(hydroksyfosfinylometylo)aminometylo)-3,5,5-trimetylocykloheksyloamino-bis(metylofosfinowego) polega na tym, że 5-amino-1,3,3-trimetylocykloheksanometanaminę poddaje się reakcji z co najmniej czterema częściami molowymi formaldehydu i co najmniej czterema częściami molowymi kwasu fosfinowego, a reakcję prowadzi się w temperaturze poniżej 330 K, aż do przereagowania substratów.The application relates to 3- [bis (hydroxyphosphinylmethyl) aminomethyl) -3,5,5-trimethylcyclohexylaminobis (methylphosphinic) acid of formula 1. 3- [Bis (hydroxyphosphinylmethyl) aminomethyl) -3,5,5-trimethylcyclohexylaminobis (methylphosphinic) acid is intended for use as a substrate for the synthesis of 3- [bis (phosphonomethyl) aminomethyl) -3,5,5-trimethylcyclohexylaminobis (methylphosphonic acid), as well as other products containing structural fragments of 5-amino-1,3,3-trimethylcyclohexanomethanamine and dimetylofosfinowego. The subject of the application is also a process for the production of 3- [bis (hydroxyphosphinylmethyl) aminomethyl) -3,5,5-trimethylcyclohexylamino-bis (methylphosphinic acid) in which 5-amino-1,3,3-trimethylcyclohexanomethanamine is reacted with with at least four mole parts of formaldehyde and at least four mole parts of phosphinic acid, and the reaction is carried out at a temperature below 330 K, until reactants react.

PL422573A 2017-08-16 2017-08-16 3-[bis(hydroxyphosphinylmethyl)aminomethyl)-3,5,5-trimethylcyclohexylamine-bis(methylphosphinic) acid and method for producing it PL234794B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL422573A PL234794B1 (en) 2017-08-16 2017-08-16 3-[bis(hydroxyphosphinylmethyl)aminomethyl)-3,5,5-trimethylcyclohexylamine-bis(methylphosphinic) acid and method for producing it

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL422573A PL234794B1 (en) 2017-08-16 2017-08-16 3-[bis(hydroxyphosphinylmethyl)aminomethyl)-3,5,5-trimethylcyclohexylamine-bis(methylphosphinic) acid and method for producing it

Publications (2)

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PL422573A1 true PL422573A1 (en) 2018-02-12
PL234794B1 PL234794B1 (en) 2020-04-30

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Family Applications (1)

Application Number Title Priority Date Filing Date
PL422573A PL234794B1 (en) 2017-08-16 2017-08-16 3-[bis(hydroxyphosphinylmethyl)aminomethyl)-3,5,5-trimethylcyclohexylamine-bis(methylphosphinic) acid and method for producing it

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PL (1) PL234794B1 (en)

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Publication number Publication date
PL234794B1 (en) 2020-04-30

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