PL416807A1 - 1,3-cyclohexane-diylbis[metylene-nitrilobis(metylene)]-tetrakisphosphonic acid and method for producing it - Google Patents

1,3-cyclohexane-diylbis[metylene-nitrilobis(metylene)]-tetrakisphosphonic acid and method for producing it

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Publication number
PL416807A1
PL416807A1 PL416807A PL41680716A PL416807A1 PL 416807 A1 PL416807 A1 PL 416807A1 PL 416807 A PL416807 A PL 416807A PL 41680716 A PL41680716 A PL 41680716A PL 416807 A1 PL416807 A1 PL 416807A1
Authority
PL
Poland
Prior art keywords
methylene
acid
metylene
cyclohexanediylbis
nitrilobis
Prior art date
Application number
PL416807A
Other languages
Polish (pl)
Other versions
PL233314B1 (en
Inventor
Mirosław Soroka
Anna Brol
Bartłomiej Kobiałka
Aleksander Grabka
Łukasz Stala
Magdalena Klacar-Ciepacz
Original Assignee
Politechnika Wrocławska
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Wrocławska filed Critical Politechnika Wrocławska
Priority to PL416807A priority Critical patent/PL233314B1/en
Publication of PL416807A1 publication Critical patent/PL416807A1/en
Publication of PL233314B1 publication Critical patent/PL233314B1/en

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Abstract

Zgłoszenie dotyczy kwasu 1,3-cykloheksanodiylbis[metylenonitrilobis(metyleno)]tetrakisfosfinowego o wzorze 1. Kwas 1,3-cykloheksanodiylbis[metylenonitrilobis(metyleno)]tetrakisfosfinowy jest przeznaczony do stosowania jako substrat do syntez, zwłaszcza kwasu 1,3-cykloheksanodiylbis[metylenonitrilobis(metyleno)]tetrakisfosfonowego, a także innych produktów zawierających fragmenty strukturalne 1,3-cykloheksanobis(metyloaminy) i kwasu dimetylofosfinowego. Zgłoszenie dotyczy również sposobu wytwarzania kwasu 1,3-cykloheksanodiylbis[metylenonitrilobis(metyleno)]tetrakisfosfinowego, który polega na tym, że 1,3-cykloheksanobis(metyloaminę) poddaje się reakcji z co najmniej czterema częściami molowymi kwasu fosfinowego i co najmniej czterema częściami molowymi formaldehydu zawartego w substancji wybranej z grupy formalina, trioksan, paraform, a reakcję prowadzi się w temperaturze poniżej 300K, w wodzie, aż do przereagowania substratów i utworzenia się produktu.The application relates to 1,3-cyclohexanediylbis [methylene nitrile (methylene)] tetrakisphosphinic acid of formula 1. 1,3-cyclohexanediylbis [methylene nitrile (methylene)] tetracisphosphinic acid is intended to be used as a synthesis substrate, especially 1,3-cyclohexanediylbisis [methylene (methylene)] tetrakisphosphonic acid, as well as other products containing structural fragments of 1,3-cyclohexanobis (methylamine) and dimethylphosphinic acid. The application also relates to a method for producing 1,3-cyclohexanediylbis [methylene nitrilobis (methylene)] tetrakisphosphinic acid, which consists in reacting 1,3-cyclohexanobis (methylamine) with at least four molar parts of phosphinic acid and at least four molar parts formaldehyde contained in a substance selected from the group formalin, trioxane, paraform, and the reaction is carried out at a temperature below 300K, in water, until reactants react and the product forms.

PL416807A 2016-04-11 2016-04-11 1,3-cyclohexane-diylbis[metylene-nitrilobis(metylene)]-tetrakisphosphonic acid and method for producing it PL233314B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL416807A PL233314B1 (en) 2016-04-11 2016-04-11 1,3-cyclohexane-diylbis[metylene-nitrilobis(metylene)]-tetrakisphosphonic acid and method for producing it

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL416807A PL233314B1 (en) 2016-04-11 2016-04-11 1,3-cyclohexane-diylbis[metylene-nitrilobis(metylene)]-tetrakisphosphonic acid and method for producing it

Publications (2)

Publication Number Publication Date
PL416807A1 true PL416807A1 (en) 2017-01-02
PL233314B1 PL233314B1 (en) 2019-09-30

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PL416807A PL233314B1 (en) 2016-04-11 2016-04-11 1,3-cyclohexane-diylbis[metylene-nitrilobis(metylene)]-tetrakisphosphonic acid and method for producing it

Country Status (1)

Country Link
PL (1) PL233314B1 (en)

Also Published As

Publication number Publication date
PL233314B1 (en) 2019-09-30

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