PL3624940T3 - Metody regeneracji katalizatorów aromatyzacji z etapem odkoksowania między dodawaniem chloru i fluoru - Google Patents

Metody regeneracji katalizatorów aromatyzacji z etapem odkoksowania między dodawaniem chloru i fluoru

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Publication number
PL3624940T3
PL3624940T3 PL18731934T PL18731934T PL3624940T3 PL 3624940 T3 PL3624940 T3 PL 3624940T3 PL 18731934 T PL18731934 T PL 18731934T PL 18731934 T PL18731934 T PL 18731934T PL 3624940 T3 PL3624940 T3 PL 3624940T3
Authority
PL
Poland
Prior art keywords
chlorine
methods
fluorine addition
aromatization catalysts
decoking step
Prior art date
Application number
PL18731934T
Other languages
English (en)
Inventor
Gabriela ALVEZ-MANOLI
Original Assignee
Chevron Phillips Chemical Company Lp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chevron Phillips Chemical Company Lp filed Critical Chevron Phillips Chemical Company Lp
Publication of PL3624940T3 publication Critical patent/PL3624940T3/pl

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/42—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst using halogen-containing material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/12—Treating with free oxygen-containing gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/60—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the type L, as exemplified by patent document US3216789
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/60—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the type L, as exemplified by patent document US3216789
    • B01J29/61—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the type L, as exemplified by patent document US3216789 containing iron group metals, noble metals or copper
    • B01J29/62—Noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/90—Regeneration or reactivation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/42—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst using halogen-containing material
    • B01J38/44—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst using halogen-containing material and adding simultaneously or subsequently free oxygen; using oxyhalogen compound
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/42—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst using halogen-containing material
    • B01J38/46—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst using halogen-containing material fluorine-containing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/32—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen
    • C07C5/373—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen with simultaneous isomerisation
    • C07C5/393—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen with simultaneous isomerisation with cyclisation to an aromatic six-membered ring, e.g. dehydrogenation of n-hexane to benzene
    • C07C5/41—Catalytic processes
    • C07C5/412—Catalytic processes with metal oxides or metal sulfides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G35/00—Reforming naphtha
    • C10G35/04—Catalytic reforming
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G35/00—Reforming naphtha
    • C10G35/04—Catalytic reforming
    • C10G35/06—Catalytic reforming characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G35/00—Reforming naphtha
    • C10G35/04—Catalytic reforming
    • C10G35/06—Catalytic reforming characterised by the catalyst used
    • C10G35/085—Catalytic reforming characterised by the catalyst used containing platinum group metals or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G35/00—Reforming naphtha
    • C10G35/04—Catalytic reforming
    • C10G35/06—Catalytic reforming characterised by the catalyst used
    • C10G35/095—Catalytic reforming characterised by the catalyst used containing crystalline alumino-silicates, e.g. molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
    • C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C07C2529/064—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof containing iron group metals, noble metals or copper
    • C07C2529/068—Noble metals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
    • C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C07C2529/60—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the type L
    • C07C2529/61—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the type L containing iron group metals, noble metals or copper
    • C07C2529/62—Noble metals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/32—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen
    • C07C5/373—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen with simultaneous isomerisation
    • C07C5/393—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen with simultaneous isomerisation with cyclisation to an aromatic six-membered ring, e.g. dehydrogenation of n-hexane to benzene
    • C07C5/41—Catalytic processes
    • C07C5/415—Catalytic processes with metals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/32—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen
    • C07C5/373—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen with simultaneous isomerisation
    • C07C5/393—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen with simultaneous isomerisation with cyclisation to an aromatic six-membered ring, e.g. dehydrogenation of n-hexane to benzene
    • C07C5/41—Catalytic processes
    • C07C5/415—Catalytic processes with metals
    • C07C5/417—Catalytic processes with metals of the platinum group

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
PL18731934T 2017-05-17 2018-05-16 Metody regeneracji katalizatorów aromatyzacji z etapem odkoksowania między dodawaniem chloru i fluoru PL3624940T3 (pl)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US15/597,189 US10300476B2 (en) 2017-05-17 2017-05-17 Methods of regenerating aromatization catalysts with a decoking step between chlorine and fluorine addition
EP18731934.8A EP3624940B1 (en) 2017-05-17 2018-05-16 Methods of regenerating aromatization catalysts with a decoking step between chlorine and fluorine addition
PCT/US2018/032995 WO2018213466A1 (en) 2017-05-17 2018-05-16 Methods of regenerating aromatization catalysts with a decoking step between chlorine and fluorine addition

Publications (1)

Publication Number Publication Date
PL3624940T3 true PL3624940T3 (pl) 2022-03-21

Family

ID=62631160

Family Applications (1)

Application Number Title Priority Date Filing Date
PL18731934T PL3624940T3 (pl) 2017-05-17 2018-05-16 Metody regeneracji katalizatorów aromatyzacji z etapem odkoksowania między dodawaniem chloru i fluoru

Country Status (9)

Country Link
US (1) US10300476B2 (pl)
EP (1) EP3624940B1 (pl)
JP (1) JP6801127B2 (pl)
KR (1) KR102143731B1 (pl)
ES (1) ES2916198T3 (pl)
PL (1) PL3624940T3 (pl)
RU (1) RU2720230C1 (pl)
SA (1) SA519410547B1 (pl)
WO (1) WO2018213466A1 (pl)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10307740B2 (en) * 2017-05-17 2019-06-04 Chevron Phillips Chemical Company Lp Methods of regenerating aromatization catalysts with a decoking step between chlorine and fluorine addition
CN110252420B (zh) * 2019-07-09 2022-01-18 河北工业大学 一种中毒蜂窝催化剂的再生方法以及一种中毒蜂窝催化剂的再生装置
US12533650B2 (en) 2022-08-18 2026-01-27 Chevron Phillips Chemical Company Lp Use of a continuous catalyst regeneration type reformer for the aromax® catalyst process
WO2024197245A1 (en) * 2023-03-22 2024-09-26 Chevron Phillips Chemical Company Lp Methods for releasing at least a portion of a halide from a surface
US12473498B2 (en) 2023-04-10 2025-11-18 Chevron Phillips Chemical Company Lp In-reactor activation of a high chloride aromatization catalyst
US20250050323A1 (en) * 2023-08-11 2025-02-13 Chevron Phillips Chemical Company Lp Methods for improving metal dispersion of a catalyst

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US4851380A (en) * 1986-12-19 1989-07-25 Chevron Research Company Process for regenerating sulfur contaminated reforming catalysts
US4855269A (en) 1986-12-19 1989-08-08 Chevron Research Company Process for regenerating a monofunctional large-pore zeolite catalyst having high selectivity for paraffin dehydrocyclization
US4937215A (en) 1987-11-13 1990-06-26 Research Association For Utilization Of Light Oil Process for restoring deactivated catalysts
JPH084748B2 (ja) * 1987-11-13 1996-01-24 出光興産株式会社 失活触媒の再生方法
US4810683A (en) 1988-01-25 1989-03-07 Uop Inc. Regeneration of a platinum-containing zeolite
US5021377A (en) * 1990-06-05 1991-06-04 Phillips Petroleum Company Demetallization and passivation of spent cracking catalysts
SA05260056B1 (ar) 1991-03-08 2008-03-26 شيفرون فيليبس كيميكال كمبني ال بي جهاز لمعالجة الهيدروكربون hydrocarbon
JP2606991B2 (ja) 1991-10-03 1997-05-07 出光興産株式会社 失活触媒の再生方法
US5401386A (en) 1992-07-24 1995-03-28 Chevron Research And Technology Company Reforming process for producing high-purity benzene
CA2146759A1 (en) 1992-10-28 1994-05-11 George T. Chen High purity benzene production using extractive distillation
US5389235A (en) 1992-12-02 1995-02-14 Uop Catalytic reaction zone for sulfur contaminant sensitive catalyst
SA94150056B1 (ar) 1993-01-04 2005-10-15 شيفرون ريسيرتش أند تكنولوجي كمبني عمليات لإزالة الألكلة الهيدروجينية hydrodealkylation
BR9810013A (pt) 1997-06-12 2000-09-12 Idemitsu Kosan Co Catalisador contendo halogênio, processo para sua preparação, e, processo para a produção de hidrocarbonetos aromáticos a partir de hidrocarbonetos não aromáticos
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US6121180A (en) * 1998-01-09 2000-09-19 Uop Llc Precombustion of halogen-containing compounds in catalyst regeneration processes
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US7153801B2 (en) 2003-06-18 2006-12-26 Chevron Phillips Chemical Company Lp Aromatization catalyst and methods of making and using same
US7582272B2 (en) 2004-03-12 2009-09-01 Chevron Phillips Chemical Company Lp Method of treating a catalytic reactor system prior to reactor servicing
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DE102008015406A1 (de) * 2008-03-22 2009-09-24 Bayer Materialscience Ag Verfahren zur Regeneration eines mit Schwefel in Form von Schwefelverbindungen vergifteten, Ruthenium oder Rutheniumverbindungen enthaltenden Katalysators
US8664144B2 (en) * 2008-12-23 2014-03-04 Chevron Phillips Chemical Company Lp Methods of reactivating an aromatization catalyst
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US8912108B2 (en) * 2012-03-05 2014-12-16 Chevron Phillips Chemical Company Lp Methods of regenerating aromatization catalysts
US8716161B2 (en) * 2012-03-05 2014-05-06 Chevron Phillips Chemical Company Methods of regenerating aromatization catalysts
JP6129931B2 (ja) * 2015-11-05 2017-05-17 アルケマ フランス 気相触媒フッ素化
MY193455A (en) * 2016-09-08 2022-10-14 Chevron Phillips Chemical Co Lp Acid aromatization catalyst with improved activity and stability
US10118167B2 (en) * 2016-12-20 2018-11-06 Chevron Phillips Chemical Company Lp Methods for regenerating sulfur-contaminated aromatization catalysts
US10307740B2 (en) * 2017-05-17 2019-06-04 Chevron Phillips Chemical Company Lp Methods of regenerating aromatization catalysts with a decoking step between chlorine and fluorine addition

Also Published As

Publication number Publication date
JP2020520795A (ja) 2020-07-16
RU2720230C1 (ru) 2020-04-28
EP3624940A1 (en) 2020-03-25
US10300476B2 (en) 2019-05-28
KR20200009049A (ko) 2020-01-29
EP3624940B1 (en) 2021-12-01
KR102143731B1 (ko) 2020-08-13
WO2018213466A1 (en) 2018-11-22
SA519410547B1 (ar) 2022-09-21
US20180333713A1 (en) 2018-11-22
JP6801127B2 (ja) 2020-12-16
ES2916198T3 (es) 2022-06-29

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