NO330674B1 - Fremgangsmate for fremstilling av en vanadylpyrofosfatkatalysator. - Google Patents
Fremgangsmate for fremstilling av en vanadylpyrofosfatkatalysator. Download PDFInfo
- Publication number
- NO330674B1 NO330674B1 NO20053128A NO20053128A NO330674B1 NO 330674 B1 NO330674 B1 NO 330674B1 NO 20053128 A NO20053128 A NO 20053128A NO 20053128 A NO20053128 A NO 20053128A NO 330674 B1 NO330674 B1 NO 330674B1
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- Norway
- Prior art keywords
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- 239000003054 catalyst Substances 0.000 title claims abstract description 30
- -1 vanadyl pyrophosphate Chemical compound 0.000 title claims description 16
- 235000011180 diphosphates Nutrition 0.000 title claims description 15
- 238000004519 manufacturing process Methods 0.000 title claims description 12
- 238000000034 method Methods 0.000 claims abstract description 31
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000001273 butane Substances 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims abstract description 16
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims abstract description 16
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims abstract description 16
- 230000003647 oxidation Effects 0.000 claims abstract description 16
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 16
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 238000001354 calcination Methods 0.000 claims abstract description 8
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 120
- 229910001868 water Inorganic materials 0.000 claims description 42
- 239000007787 solid Substances 0.000 claims description 40
- 239000000843 powder Substances 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 14
- 239000002002 slurry Substances 0.000 claims description 14
- 239000000243 solution Substances 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 7
- 238000005406 washing Methods 0.000 claims description 7
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 230000032683 aging Effects 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 238000001704 evaporation Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 235000011007 phosphoric acid Nutrition 0.000 claims description 3
- 239000011541 reaction mixture Substances 0.000 claims description 3
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 claims description 2
- 229910017912 NH2OH Inorganic materials 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 abstract description 7
- 229910017775 (VO)2P207 Inorganic materials 0.000 description 13
- 230000009466 transformation Effects 0.000 description 9
- 239000002243 precursor Substances 0.000 description 8
- 230000015572 biosynthetic process Effects 0.000 description 7
- 238000003786 synthesis reaction Methods 0.000 description 6
- 238000002441 X-ray diffraction Methods 0.000 description 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 3
- 230000003197 catalytic effect Effects 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 239000004094 surface-active agent Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 238000005033 Fourier transform infrared spectroscopy Methods 0.000 description 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
- WTDHULULXKLSOZ-UHFFFAOYSA-N Hydroxylamine hydrochloride Chemical compound Cl.ON WTDHULULXKLSOZ-UHFFFAOYSA-N 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000001027 hydrothermal synthesis Methods 0.000 description 2
- 230000001131 transforming effect Effects 0.000 description 2
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 1
- FALRKNHUBBKYCC-UHFFFAOYSA-N 2-(chloromethyl)pyridine-3-carbonitrile Chemical compound ClCC1=NC=CC=C1C#N FALRKNHUBBKYCC-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 229910017299 Mo—O Inorganic materials 0.000 description 1
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- XPPKVPWEQAFLFU-UHFFFAOYSA-J diphosphate(4-) Chemical compound [O-]P([O-])(=O)OP([O-])([O-])=O XPPKVPWEQAFLFU-UHFFFAOYSA-J 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000921 elemental analysis Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000001630 malic acid Substances 0.000 description 1
- 235000011090 malic acid Nutrition 0.000 description 1
- 230000000877 morphologic effect Effects 0.000 description 1
- WHQSYGRFZMUQGQ-UHFFFAOYSA-N n,n-dimethylformamide;hydrate Chemical compound O.CN(C)C=O WHQSYGRFZMUQGQ-UHFFFAOYSA-N 0.000 description 1
- 235000012736 patent blue V Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000011877 solvent mixture Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229940014800 succinic anhydride Drugs 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- IHIXIJGXTJIKRB-UHFFFAOYSA-N trisodium vanadate Chemical compound [Na+].[Na+].[Na+].[O-][V]([O-])([O-])=O IHIXIJGXTJIKRB-UHFFFAOYSA-N 0.000 description 1
- 229920006305 unsaturated polyester Polymers 0.000 description 1
Landscapes
- Catalysts (AREA)
- Furan Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/IB2003/000016 WO2004060558A1 (en) | 2003-01-03 | 2003-01-03 | Process for preparing vanadyl pyrophosphate catalyst |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO20053128D0 NO20053128D0 (no) | 2005-06-27 |
| NO20053128L NO20053128L (no) | 2005-09-22 |
| NO330674B1 true NO330674B1 (no) | 2011-06-06 |
Family
ID=34362332
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO20053128A NO330674B1 (no) | 2003-01-03 | 2005-06-27 | Fremgangsmate for fremstilling av en vanadylpyrofosfatkatalysator. |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP1581340B1 (de) |
| JP (1) | JP4242842B2 (de) |
| CN (1) | CN100434171C (de) |
| AT (1) | ATE499154T1 (de) |
| AU (1) | AU2003200849B2 (de) |
| DE (1) | DE60336173D1 (de) |
| NO (1) | NO330674B1 (de) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MY153933A (en) * | 2007-10-22 | 2015-04-15 | Huntsman Petrochemical Llc | Improved oxidation catalyst for maleic anhydride production |
| US8658557B2 (en) * | 2011-10-25 | 2014-02-25 | Ineos Usa Llc | Catalyst for n-butane oxidation to maleic anhydride |
| CN103539099B (zh) * | 2013-10-30 | 2016-04-06 | 渤海大学 | 一种焦磷酸镍微米纤维的制备方法 |
| CN103539098B (zh) * | 2013-10-30 | 2015-09-23 | 渤海大学 | 一种片状形貌焦磷酸锰微晶的制备方法 |
| CN105709790B (zh) * | 2014-12-03 | 2018-01-23 | 中国石油化工股份有限公司 | 纳米结构正丁烷氧化制顺酐催化剂制备方法及其催化剂 |
| CN109261221A (zh) * | 2018-11-08 | 2019-01-25 | 中触媒新材料股份有限公司 | 一种用于去除钒银钼磷酸盐催化剂中还原性有机物的方法 |
| CN113274951B (zh) * | 2021-05-21 | 2022-12-20 | 济南隆凯能源科技有限公司 | 一种双蒸气引射循环烃部分氧化系统及方法 |
| CN113527233A (zh) * | 2021-08-18 | 2021-10-22 | 上海师范大学 | 一种连续生产丁二酸酐的方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05103990A (ja) * | 1991-10-17 | 1993-04-27 | Tosoh Corp | 酸化触媒の製造方法 |
| EP0986434B1 (de) * | 1997-06-04 | 2001-10-24 | Sasol Technology (Proprietary) Limited | Verfahren zur herstellung eines vanadium-phosphoroxide-katalysators |
-
2003
- 2003-01-03 EP EP03700020A patent/EP1581340B1/de not_active Expired - Lifetime
- 2003-01-03 JP JP2004564355A patent/JP4242842B2/ja not_active Expired - Fee Related
- 2003-01-03 AT AT03700020T patent/ATE499154T1/de not_active IP Right Cessation
- 2003-01-03 CN CNB038257548A patent/CN100434171C/zh not_active Expired - Fee Related
- 2003-01-03 AU AU2003200849A patent/AU2003200849B2/en not_active Ceased
- 2003-01-03 DE DE60336173T patent/DE60336173D1/de not_active Expired - Lifetime
-
2005
- 2005-06-27 NO NO20053128A patent/NO330674B1/no not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| JP4242842B2 (ja) | 2009-03-25 |
| CN100434171C (zh) | 2008-11-19 |
| EP1581340B1 (de) | 2011-02-23 |
| CN1750877A (zh) | 2006-03-22 |
| EP1581340A1 (de) | 2005-10-05 |
| ATE499154T1 (de) | 2011-03-15 |
| DE60336173D1 (de) | 2011-04-07 |
| AU2003200849B2 (en) | 2006-10-19 |
| NO20053128L (no) | 2005-09-22 |
| NO20053128D0 (no) | 2005-06-27 |
| AU2003200849A1 (en) | 2004-07-29 |
| JP2006512196A (ja) | 2006-04-13 |
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| MM1K | Lapsed by not paying the annual fees |