NO20076225L - Fremstilling av fosforoksyklorid som biprodukt fra fosforpentaklorid og DMF og dens anvendelse for kloreringsreaksjon ved omdanning til Vilsmeier-Haack-reagens - Google Patents
Fremstilling av fosforoksyklorid som biprodukt fra fosforpentaklorid og DMF og dens anvendelse for kloreringsreaksjon ved omdanning til Vilsmeier-Haack-reagensInfo
- Publication number
- NO20076225L NO20076225L NO20076225A NO20076225A NO20076225L NO 20076225 L NO20076225 L NO 20076225L NO 20076225 A NO20076225 A NO 20076225A NO 20076225 A NO20076225 A NO 20076225A NO 20076225 L NO20076225 L NO 20076225L
- Authority
- NO
- Norway
- Prior art keywords
- vilsmeier
- dmf
- product
- phosphorus
- conversion
- Prior art date
Links
- ZMXDDKWLCZADIW-UHFFFAOYSA-N Vilsmeier-Haack reagent Natural products CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 title abstract 10
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 title abstract 4
- UHZYTMXLRWXGPK-UHFFFAOYSA-N phosphorus pentachloride Chemical compound ClP(Cl)(Cl)(Cl)Cl UHZYTMXLRWXGPK-UHFFFAOYSA-N 0.000 title abstract 3
- 239000006227 byproduct Substances 0.000 title abstract 2
- 238000006243 chemical reaction Methods 0.000 title abstract 2
- 238000005660 chlorination reaction Methods 0.000 title 1
- QQVDYSUDFZZPSU-UHFFFAOYSA-M chloromethylidene(dimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)=CCl QQVDYSUDFZZPSU-UHFFFAOYSA-M 0.000 abstract 3
- 238000000034 method Methods 0.000 abstract 2
- AFHCRQREQZIDSI-OVUASUNJSA-N [(2r,3s,4s,5r,6r)-6-[(2s,3s,4s,5r)-3,4-dihydroxy-2,5-bis(hydroxymethyl)oxolan-2-yl]oxy-3,4,5-trihydroxyoxan-2-yl]methyl benzoate Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](COC(=O)C=2C=CC=CC=2)O1 AFHCRQREQZIDSI-OVUASUNJSA-N 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
- AFHCRQREQZIDSI-UHFFFAOYSA-N sucrose-6-benzoate Natural products OC1C(O)C(CO)OC1(CO)OC1C(O)C(O)C(O)C(COC(=O)C=2C=CC=CC=2)O1 AFHCRQREQZIDSI-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/02—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton containing imino groups
- C07C251/30—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton containing imino groups having nitrogen atoms of imino groups quaternised
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/10—Halides or oxyhalides of phosphorus
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B39/00—Halogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/02—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of compounds containing imino groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/09—Esters of phosphoric acids
- C07F9/14—Esters of phosphoric acids containing P(=O)-halide groups
- C07F9/1403—Esters of phosphoric acids containing P(=O)-halide groups containing the structure Hal-P(=O)-O-unsaturated acyclic group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
- C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Genetics & Genomics (AREA)
- Inorganic Chemistry (AREA)
- Saccharide Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IN545MU2005 | 2005-05-04 | ||
| PCT/IN2006/000151 WO2007017891A2 (en) | 2005-05-04 | 2006-04-28 | Generation of phosphorus oxychloride as by-product from phosphorus pentachloride and dmf and its use for chlorination reaction by converting into vilsmeier-haack reagent. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO20076225L true NO20076225L (no) | 2007-12-04 |
Family
ID=37727715
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO20076225A NO20076225L (no) | 2005-05-04 | 2007-12-04 | Fremstilling av fosforoksyklorid som biprodukt fra fosforpentaklorid og DMF og dens anvendelse for kloreringsreaksjon ved omdanning til Vilsmeier-Haack-reagens |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US20090131653A1 (es) |
| EP (1) | EP1888611A4 (es) |
| JP (1) | JP2008542199A (es) |
| KR (1) | KR20080007347A (es) |
| CN (1) | CN101490070A (es) |
| AU (1) | AU2006277556A1 (es) |
| BR (1) | BRPI0612344A2 (es) |
| CA (1) | CA2606487A1 (es) |
| EA (1) | EA200702148A1 (es) |
| IL (1) | IL186985A0 (es) |
| LV (1) | LV13683B (es) |
| MX (1) | MX2007013689A (es) |
| NO (1) | NO20076225L (es) |
| NZ (1) | NZ562849A (es) |
| WO (1) | WO2007017891A2 (es) |
| ZA (1) | ZA200709833B (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012025937A1 (en) * | 2010-08-25 | 2012-03-01 | Ramamohan Rao Davuluri | Improved process for preparation of sugammadex |
| EP2643338B1 (en) | 2010-11-23 | 2016-04-06 | Lexington Pharmaceuticals Laboratories, LLC | Low temperature chlorination of carbohydrates |
| CA2823961C (en) | 2011-10-14 | 2020-10-06 | Lexington Pharmaceuticals Laboratories, Llc | Chlorination of carbohydrates and carbohydrate derivatives |
| CN103058883B (zh) * | 2013-01-18 | 2015-01-21 | 山东凯盛新材料有限公司 | 固体(氯亚甲基)二甲基氯化铵的制备工艺 |
| CN106554345B (zh) * | 2015-09-29 | 2018-11-30 | 杭州杜易科技有限公司 | 一种五氯化磷氯化副产物的回收和利用的方法 |
| CN109678651B (zh) * | 2018-12-28 | 2021-11-12 | 瑞孚信江苏药业股份有限公司 | 一种高纯度α,α-二氯乙基环丙烷的制备方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3062467D1 (en) * | 1979-12-20 | 1983-04-28 | Tate & Lyle Plc | Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
| GB8316790D0 (en) * | 1983-06-21 | 1983-07-27 | Tate & Lyle Plc | Chemical process |
| US4614806A (en) * | 1983-12-23 | 1986-09-30 | American Home Products Corporation | Process for the asymmetric synthesis of chiral indoline-2-carboxylic acids |
| US4980463A (en) * | 1989-07-18 | 1990-12-25 | Noramco, Inc. | Sucrose-6-ester chlorination |
| CN101175762A (zh) * | 2005-01-03 | 2008-05-07 | 法马德医疗保险私人有限公司 | 通过氯化试剂的共-加入进行蔗糖-6-酯的氯化 |
| BRPI0711237A2 (pt) * | 2006-05-23 | 2011-08-23 | Vb Medicare Pvt Ltd | processo de purificação e recuperação de uma amida terciária a partir de uma composição lìquida aquosa |
-
2006
- 2006-04-28 US US11/919,826 patent/US20090131653A1/en not_active Abandoned
- 2006-04-28 AU AU2006277556A patent/AU2006277556A1/en not_active Abandoned
- 2006-04-28 WO PCT/IN2006/000151 patent/WO2007017891A2/en active Application Filing
- 2006-04-28 CA CA002606487A patent/CA2606487A1/en not_active Abandoned
- 2006-04-28 EA EA200702148A patent/EA200702148A1/ru unknown
- 2006-04-28 CN CNA2006800151931A patent/CN101490070A/zh active Pending
- 2006-04-28 EP EP06809914A patent/EP1888611A4/en not_active Withdrawn
- 2006-04-28 JP JP2008509577A patent/JP2008542199A/ja not_active Abandoned
- 2006-04-28 MX MX2007013689A patent/MX2007013689A/es unknown
- 2006-04-28 KR KR1020077025559A patent/KR20080007347A/ko not_active Application Discontinuation
- 2006-04-28 BR BRPI0612344-9A patent/BRPI0612344A2/pt not_active IP Right Cessation
- 2006-04-28 NZ NZ562849A patent/NZ562849A/en not_active IP Right Cessation
-
2007
- 2007-10-29 IL IL186985A patent/IL186985A0/en unknown
- 2007-10-30 ZA ZA200709833A patent/ZA200709833B/xx unknown
- 2007-11-06 LV LVP-07-127A patent/LV13683B/lv unknown
- 2007-12-04 NO NO20076225A patent/NO20076225L/no not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| JP2008542199A (ja) | 2008-11-27 |
| MX2007013689A (es) | 2009-02-17 |
| IL186985A0 (en) | 2008-06-05 |
| EP1888611A4 (en) | 2011-04-13 |
| WO2007017891A2 (en) | 2007-02-15 |
| US20090131653A1 (en) | 2009-05-21 |
| KR20080007347A (ko) | 2008-01-18 |
| AU2006277556A1 (en) | 2007-02-15 |
| CN101490070A (zh) | 2009-07-22 |
| CA2606487A1 (en) | 2007-02-15 |
| BRPI0612344A2 (pt) | 2010-11-03 |
| LV13683B (lv) | 2009-01-20 |
| ZA200709833B (en) | 2009-07-29 |
| EP1888611A2 (en) | 2008-02-20 |
| EA200702148A1 (ru) | 2009-02-27 |
| WO2007017891A3 (en) | 2009-04-09 |
| NZ562849A (en) | 2009-11-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FC2A | Withdrawal, rejection or dismissal of laid open patent application |