NO130976B - - Google Patents
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- Publication number
- NO130976B NO130976B NO01091/72A NO109172A NO130976B NO 130976 B NO130976 B NO 130976B NO 01091/72 A NO01091/72 A NO 01091/72A NO 109172 A NO109172 A NO 109172A NO 130976 B NO130976 B NO 130976B
- Authority
- NO
- Norway
- Prior art keywords
- nitro
- acid
- furfurylidene
- sulfuric acid
- hydrazine
- Prior art date
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 14
- -1 ureido- Chemical class 0.000 claims description 10
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 7
- OAKJQQAXSVQMHS-UHFFFAOYSA-N hydrazine Substances NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 229910017604 nitric acid Inorganic materials 0.000 claims description 7
- 239000002244 precipitate Substances 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 239000011541 reaction mixture Substances 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims description 3
- 239000002253 acid Substances 0.000 description 12
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 10
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 9
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- SXINBFXPADXIEY-UHFFFAOYSA-N 5-Nitrofurfural Chemical compound [O-][N+](=O)C1=CC=C(C=O)O1 SXINBFXPADXIEY-UHFFFAOYSA-N 0.000 description 5
- 235000019441 ethanol Nutrition 0.000 description 4
- 238000006396 nitration reaction Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 2
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 239000007859 condensation product Substances 0.000 description 2
- 150000002240 furans Chemical class 0.000 description 2
- IAIWVQXQOWNYOU-FPYGCLRLSA-N nitrofural Chemical compound NC(=O)N\N=C\C1=CC=C([N+]([O-])=O)O1 IAIWVQXQOWNYOU-FPYGCLRLSA-N 0.000 description 2
- NXFQHRVNIOXGAQ-YCRREMRBSA-N nitrofurantoin Chemical compound O1C([N+](=O)[O-])=CC=C1\C=N\N1C(=O)NC(=O)C1 NXFQHRVNIOXGAQ-YCRREMRBSA-N 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- KVYKDNGUEZRPGJ-UHFFFAOYSA-N 1-Aminohydantoin Chemical compound NN1CC(=O)NC1=O KVYKDNGUEZRPGJ-UHFFFAOYSA-N 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- BAOXJBYPTRZNSH-XBXARRHUSA-N [(e)-furan-2-ylmethylideneamino]urea Chemical compound NC(=O)N\N=C\C1=CC=CO1 BAOXJBYPTRZNSH-XBXARRHUSA-N 0.000 description 1
- 239000002246 antineoplastic agent Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229940127089 cytotoxic agent Drugs 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229960004279 formaldehyde Drugs 0.000 description 1
- 235000019256 formaldehyde Nutrition 0.000 description 1
- PLHJDBGFXBMTGZ-WEVVVXLNSA-N furazolidone Chemical compound O1C([N+](=O)[O-])=CC=C1\C=N\N1C(=O)OCC1 PLHJDBGFXBMTGZ-WEVVVXLNSA-N 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 230000000802 nitrating effect Effects 0.000 description 1
- 229960001907 nitrofurazone Drugs 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
- B01J8/12—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by gravity in a downward flow
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D57/00—Separation, other than separation of solids, not fully covered by a single other group or subclass, e.g. B03C
- B01D57/02—Separation, other than separation of solids, not fully covered by a single other group or subclass, e.g. B03C by electrophoresis
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/416—Systems
- G01N27/447—Systems using electrophoresis
- G01N27/44756—Apparatus specially adapted therefor
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/416—Systems
- G01N27/447—Systems using electrophoresis
- G01N27/44756—Apparatus specially adapted therefor
- G01N27/44769—Continuous electrophoresis, i.e. the sample being continuously introduced, e.g. free flow electrophoresis [FFE]
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Analytical Chemistry (AREA)
- Physics & Mathematics (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Peptides Or Proteins (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7111180A FR2131859B1 (zh) | 1971-03-30 | 1971-03-30 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NO130976B true NO130976B (zh) | 1974-12-09 |
| NO130976C NO130976C (zh) | 1975-03-19 |
Family
ID=9074431
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO1091/72A NO130976C (zh) | 1971-03-30 | 1972-03-29 |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US3829370A (zh) |
| BE (1) | BE781424A (zh) |
| BR (1) | BR7201749D0 (zh) |
| CA (1) | CA985209A (zh) |
| CH (1) | CH543305A (zh) |
| DE (1) | DE2215761A1 (zh) |
| FR (1) | FR2131859B1 (zh) |
| GB (1) | GB1338543A (zh) |
| IT (1) | IT959581B (zh) |
| LU (1) | LU65075A1 (zh) |
| NL (1) | NL7203835A (zh) |
| NO (1) | NO130976C (zh) |
| SU (1) | SU487476A3 (zh) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3935092A (en) * | 1971-12-14 | 1976-01-27 | Rhone-Poulenc-Textile | Purification of a chloride solution |
| US3994799A (en) * | 1973-04-17 | 1976-11-30 | Yao Shang J | Blood and tissue detoxification apparatus |
| US3989613A (en) * | 1973-05-16 | 1976-11-02 | The Dow Chemical Company | Continuous balanced flow fixed boundary electrophoresis |
| US3972791A (en) * | 1974-05-06 | 1976-08-03 | Harold Stern | Fractionation of proteins by electrical means |
| US3923426A (en) * | 1974-08-15 | 1975-12-02 | Alza Corp | Electroosmotic pump and fluid dispenser including same |
| US4115225A (en) * | 1977-07-22 | 1978-09-19 | Ionics, Inc. | Electrodialysis cell electrode reversal and anolyte recirculation system |
| US4276140A (en) * | 1980-01-10 | 1981-06-30 | Ionics Inc. | Electrodialysis apparatus and process for fractionating protein mixtures |
| DE3040470A1 (de) * | 1980-10-27 | 1982-06-03 | Siemens AG, 1000 Berlin und 8000 München | Verfahren und vorrichtung zur indirekten oxidation von harnstoff |
| JPS58147639A (ja) * | 1982-02-26 | 1983-09-02 | Hideyuki Nishizawa | 連続電気泳動分離法および装置 |
| US4394246A (en) * | 1982-05-24 | 1983-07-19 | Mcdonnell Douglas Corporation | Electrophoresis apparatus with flow control |
| DE3337669C2 (de) * | 1983-10-17 | 1989-09-21 | Carl Schleicher & Schuell Gmbh & Co Kg, 3352 Einbeck | Gerät zur Elektroelution elektrisch geladener Makromoleküle |
| DE3337668C2 (de) * | 1983-10-17 | 1985-12-05 | Carl Schleicher & Schuell Gmbh & Co Kg, 3352 Einbeck | Verfahren zur Elektroelution elektrisch geladener Makromoleküle |
| FR2567914B1 (fr) * | 1984-07-19 | 1989-04-07 | Univ Languedoc | Procede de recuperation de cations metalliques en continu a partir de solutions diluees et appareil pour sa mise en oeuvre |
| FR2568485B1 (fr) * | 1984-08-06 | 1990-03-23 | Rhone Poulenc Rech | Appareil de fractionnement par electrophorese de solutions contenant des proteines, utilisable notamment pour le fractionnement du plasma humain |
| US4668361A (en) * | 1985-05-24 | 1987-05-26 | Dorr-Oliver Incorporated | Dialyzing electrofilter with improved electrode |
| US4834862A (en) * | 1988-09-12 | 1989-05-30 | Duke University | Ampholyte separation method and apparatus |
| GB2225339A (en) * | 1988-11-15 | 1990-05-30 | Aligena Ag | Separating electrically charged macromolecular compounds by forced-flow membrane electrophoresis |
| US5336387A (en) * | 1990-09-11 | 1994-08-09 | Bioseparations, Inc. | Electrical separator apparatus and method of counterflow gradient focusing |
| US5662813A (en) * | 1994-10-21 | 1997-09-02 | Bioseparations, Inc. | Method for separation of nucleated fetal erythrocytes from maternal blood samples |
| AUPP790898A0 (en) * | 1998-12-23 | 1999-01-28 | Life Therapeutics Limited | Renal dialysis |
| DE10063097B4 (de) * | 2000-12-18 | 2007-04-19 | Becton, Dickinson And Co. | Elektrophoresevorrichtung |
| EP3474006A1 (en) * | 2017-10-19 | 2019-04-24 | Université de Liège | Microchip for free flow electrophoresis |
-
1971
- 1971-03-30 FR FR7111180A patent/FR2131859B1/fr not_active Expired
-
1972
- 1972-03-22 NL NL7203835A patent/NL7203835A/xx unknown
- 1972-03-24 BR BR1749/72A patent/BR7201749D0/pt unknown
- 1972-03-27 SU SU1762202A patent/SU487476A3/ru active
- 1972-03-28 US US00238764A patent/US3829370A/en not_active Expired - Lifetime
- 1972-03-28 GB GB1445972A patent/GB1338543A/en not_active Expired
- 1972-03-29 LU LU65075D patent/LU65075A1/xx unknown
- 1972-03-29 CA CA138,533A patent/CA985209A/en not_active Expired
- 1972-03-29 CH CH468072A patent/CH543305A/fr not_active IP Right Cessation
- 1972-03-29 BE BE781424A patent/BE781424A/xx unknown
- 1972-03-29 NO NO1091/72A patent/NO130976C/no unknown
- 1972-03-30 IT IT22647/72A patent/IT959581B/it active
- 1972-03-30 DE DE19722215761 patent/DE2215761A1/de active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| CH543305A (fr) | 1973-10-31 |
| FR2131859B1 (zh) | 1974-03-08 |
| NO130976C (zh) | 1975-03-19 |
| LU65075A1 (zh) | 1972-12-07 |
| BR7201749D0 (pt) | 1973-11-01 |
| CA985209A (en) | 1976-03-09 |
| GB1338543A (en) | 1973-11-28 |
| SU487476A3 (ru) | 1975-10-05 |
| FR2131859A1 (zh) | 1972-11-17 |
| US3829370A (en) | 1974-08-13 |
| BE781424A (fr) | 1972-09-29 |
| IT959581B (it) | 1973-11-10 |
| DE2215761A1 (de) | 1972-10-12 |
| NL7203835A (zh) | 1972-10-03 |
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