NO129677B - - Google Patents
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- Publication number
- NO129677B NO129677B NO01726/70A NO172670A NO129677B NO 129677 B NO129677 B NO 129677B NO 01726/70 A NO01726/70 A NO 01726/70A NO 172670 A NO172670 A NO 172670A NO 129677 B NO129677 B NO 129677B
- Authority
- NO
- Norway
- Prior art keywords
- chloride
- reaction
- sulfur
- trichloromethanesulfenyl
- disulfur dichloride
- Prior art date
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 28
- 238000006243 chemical reaction Methods 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 24
- RYFZYYUIAZYQLC-UHFFFAOYSA-N perchloromethyl mercaptan Chemical compound ClSC(Cl)(Cl)Cl RYFZYYUIAZYQLC-UHFFFAOYSA-N 0.000 claims description 24
- PXJJSXABGXMUSU-UHFFFAOYSA-N disulfur dichloride Chemical compound ClSSCl PXJJSXABGXMUSU-UHFFFAOYSA-N 0.000 claims description 21
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 20
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 239000005864 Sulphur Substances 0.000 claims description 6
- QSUDTRSBIJFXJE-UHFFFAOYSA-N chloroform chlorosulfanyl thiohypochlorite Chemical compound S(SCl)Cl.ClC(Cl)Cl QSUDTRSBIJFXJE-UHFFFAOYSA-N 0.000 claims description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 16
- 229910052717 sulfur Inorganic materials 0.000 description 14
- 239000011593 sulfur Substances 0.000 description 14
- 239000011541 reaction mixture Substances 0.000 description 9
- 238000004821 distillation Methods 0.000 description 6
- 239000003054 catalyst Substances 0.000 description 5
- NTOLLCFJWFCTMH-UHFFFAOYSA-N trichloro-(trichloromethyldisulfanyl)methane Chemical compound ClC(Cl)(Cl)SSC(Cl)(Cl)Cl NTOLLCFJWFCTMH-UHFFFAOYSA-N 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 239000006227 byproduct Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 4
- HEWWCALXHMTHHM-UHFFFAOYSA-N trichloro-(trichloromethyltrisulfanyl)methane Chemical compound ClC(Cl)(Cl)SSSC(Cl)(Cl)Cl HEWWCALXHMTHHM-UHFFFAOYSA-N 0.000 description 4
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 3
- GJEAMHAFPYZYDE-UHFFFAOYSA-N [C].[S] Chemical compound [C].[S] GJEAMHAFPYZYDE-UHFFFAOYSA-N 0.000 description 3
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 238000005660 chlorination reaction Methods 0.000 description 2
- 238000004587 chromatography analysis Methods 0.000 description 2
- 238000003776 cleavage reaction Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- -1 hexachloride methyl trisulfide Chemical compound 0.000 description 2
- 229910052740 iodine Inorganic materials 0.000 description 2
- 239000011630 iodine Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 230000007017 scission Effects 0.000 description 2
- ZWZVWGITAAIFPS-UHFFFAOYSA-N thiophosgene Chemical compound ClC(Cl)=S ZWZVWGITAAIFPS-UHFFFAOYSA-N 0.000 description 2
- 230000007306 turnover Effects 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- QZRGKCOWNLSUDK-UHFFFAOYSA-N Iodochlorine Chemical class ICl QZRGKCOWNLSUDK-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- YQCIWBXEVYWRCW-UHFFFAOYSA-N methane;sulfane Chemical compound C.S YQCIWBXEVYWRCW-UHFFFAOYSA-N 0.000 description 1
- 230000000590 parasiticidal effect Effects 0.000 description 1
- 239000002297 parasiticide Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- FWMUJAIKEJWSSY-UHFFFAOYSA-N sulfur dichloride Chemical compound ClSCl FWMUJAIKEJWSSY-UHFFFAOYSA-N 0.000 description 1
- DQWPFSLDHJDLRL-UHFFFAOYSA-N triethyl phosphate Chemical compound CCOP(=O)(OCC)OCC DQWPFSLDHJDLRL-UHFFFAOYSA-N 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C381/00—Compounds containing carbon and sulfur and having functional groups not covered by groups C07C301/00 - C07C337/00
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691933242 DE1933242A1 (de) | 1969-07-01 | 1969-07-01 | Verfahren zur Herstellung von Trichlormethanthiosulfenylchlorid mehrstufiger Schmierpumpen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO129677B true NO129677B (pt) | 1974-05-13 |
Family
ID=5738477
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO01726/70A NO129677B (pt) | 1969-07-01 | 1970-05-06 |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US3790627A (pt) |
| JP (1) | JPS4817263B1 (pt) |
| AT (1) | AT296239B (pt) |
| BE (1) | BE750988A (pt) |
| BG (1) | BG17440A3 (pt) |
| CH (1) | CH525200A (pt) |
| DE (1) | DE1933242A1 (pt) |
| DK (1) | DK124478B (pt) |
| ES (1) | ES379845A1 (pt) |
| FR (1) | FR2056435A5 (pt) |
| GB (1) | GB1256844A (pt) |
| IE (1) | IE34189B1 (pt) |
| LU (1) | LU61206A1 (pt) |
| NL (1) | NL7008047A (pt) |
| NO (1) | NO129677B (pt) |
| RO (1) | RO57535A (pt) |
| SE (1) | SE351423B (pt) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IL53443A (en) * | 1976-12-22 | 1983-03-31 | Stauffer Chemical Co | Production of perchloromethyl mercaptan |
| US4340762A (en) * | 1980-12-15 | 1982-07-20 | Allied Corporation | Gas phase synthesis of bis(trifluoromethyl) disulfide |
-
1969
- 1969-07-01 DE DE19691933242 patent/DE1933242A1/de active Pending
-
1970
- 1970-04-28 IE IE539/70A patent/IE34189B1/xx unknown
- 1970-05-06 NO NO01726/70A patent/NO129677B/no unknown
- 1970-05-11 SE SE06432/70A patent/SE351423B/xx unknown
- 1970-05-11 DK DK237170AA patent/DK124478B/da unknown
- 1970-05-15 GB GB1256844D patent/GB1256844A/en not_active Expired
- 1970-05-20 RO RO63407A patent/RO57535A/ro unknown
- 1970-05-20 ES ES379845A patent/ES379845A1/es not_active Expired
- 1970-05-25 CH CH768870A patent/CH525200A/de not_active IP Right Cessation
- 1970-05-27 BE BE750988D patent/BE750988A/xx unknown
- 1970-06-03 NL NL7008047A patent/NL7008047A/xx unknown
- 1970-06-10 AT AT521470A patent/AT296239B/de not_active IP Right Cessation
- 1970-06-26 LU LU61206D patent/LU61206A1/xx unknown
- 1970-06-29 US US00050919A patent/US3790627A/en not_active Expired - Lifetime
- 1970-06-30 FR FR7024238A patent/FR2056435A5/fr not_active Expired
- 1970-07-01 BG BG15071A patent/BG17440A3/xx unknown
- 1970-07-01 JP JP45056990A patent/JPS4817263B1/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US3790627A (en) | 1974-02-05 |
| GB1256844A (pt) | 1971-12-15 |
| CH525200A (de) | 1972-07-15 |
| BG17440A3 (pt) | 1973-11-10 |
| DE1933242A1 (de) | 1971-01-21 |
| IE34189L (en) | 1971-01-01 |
| IE34189B1 (en) | 1975-03-05 |
| JPS4817263B1 (pt) | 1973-05-28 |
| AT296239B (de) | 1972-02-10 |
| SE351423B (pt) | 1972-11-27 |
| LU61206A1 (pt) | 1970-06-26 |
| BE750988A (fr) | 1970-11-03 |
| DK124478B (da) | 1972-10-23 |
| RO57535A (pt) | 1975-01-15 |
| FR2056435A5 (pt) | 1971-05-14 |
| ES379845A1 (es) | 1972-09-16 |
| NL7008047A (pt) | 1971-01-05 |
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