NO129627B - - Google Patents
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- Publication number
- NO129627B NO129627B NO02643/71A NO264371A NO129627B NO 129627 B NO129627 B NO 129627B NO 02643/71 A NO02643/71 A NO 02643/71A NO 264371 A NO264371 A NO 264371A NO 129627 B NO129627 B NO 129627B
- Authority
- NO
- Norway
- Prior art keywords
- dicyandiamide
- ammonia
- melamine
- container
- pressure
- Prior art date
Links
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 372
- QGBSISYHAICWAH-UHFFFAOYSA-N dicyandiamide Chemical compound NC(N)=NC#N QGBSISYHAICWAH-UHFFFAOYSA-N 0.000 claims description 247
- 229910021529 ammonia Inorganic materials 0.000 claims description 166
- 229920000877 Melamine resin Polymers 0.000 claims description 130
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims description 128
- 239000002002 slurry Substances 0.000 claims description 76
- 238000006243 chemical reaction Methods 0.000 claims description 62
- 238000003860 storage Methods 0.000 claims description 57
- 239000000725 suspension Substances 0.000 claims description 43
- 239000013078 crystal Substances 0.000 claims description 28
- 239000007787 solid Substances 0.000 claims description 27
- 238000003756 stirring Methods 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 238000000926 separation method Methods 0.000 claims description 15
- 230000008021 deposition Effects 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 13
- 238000001816 cooling Methods 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 11
- 238000004090 dissolution Methods 0.000 claims description 9
- 239000000428 dust Substances 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- 238000000746 purification Methods 0.000 claims description 8
- 238000006073 displacement reaction Methods 0.000 claims description 7
- 229920006395 saturated elastomer Polymers 0.000 claims description 7
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims description 5
- 239000000356 contaminant Substances 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 3
- 150000002500 ions Chemical class 0.000 claims description 3
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- 238000007906 compression Methods 0.000 claims description 2
- 230000006835 compression Effects 0.000 claims description 2
- 239000006193 liquid solution Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 description 72
- 238000000034 method Methods 0.000 description 34
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 25
- 239000007789 gas Substances 0.000 description 23
- 230000015572 biosynthetic process Effects 0.000 description 13
- 238000009833 condensation Methods 0.000 description 7
- 230000005494 condensation Effects 0.000 description 7
- 238000001704 evaporation Methods 0.000 description 7
- 239000000203 mixture Substances 0.000 description 6
- 230000001105 regulatory effect Effects 0.000 description 6
- 239000012047 saturated solution Substances 0.000 description 6
- 230000008020 evaporation Effects 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 230000007306 turnover Effects 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- 230000008569 process Effects 0.000 description 4
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 230000001419 dependent effect Effects 0.000 description 3
- -1 at minus 27° C Chemical compound 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 230000029142 excretion Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 150000007974 melamines Chemical class 0.000 description 2
- 238000001953 recrystallisation Methods 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- YZEZMSPGIPTEBA-UHFFFAOYSA-N 2-n-(4,6-diamino-1,3,5-triazin-2-yl)-1,3,5-triazine-2,4,6-triamine Chemical compound NC1=NC(N)=NC(NC=2N=C(N)N=C(N)N=2)=N1 YZEZMSPGIPTEBA-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 230000001464 adherent effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000011437 continuous method Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 239000012527 feed solution Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- YSRVJVDFHZYRPA-UHFFFAOYSA-N melem Chemical compound NC1=NC(N23)=NC(N)=NC2=NC(N)=NC3=N1 YSRVJVDFHZYRPA-UHFFFAOYSA-N 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D243/00—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms
- C07D243/06—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4
- C07D243/10—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4 condensed with carbocyclic rings or ring systems
- C07D243/14—1,4-Benzodiazepines; Hydrogenated 1,4-benzodiazepines
- C07D243/16—1,4-Benzodiazepines; Hydrogenated 1,4-benzodiazepines substituted in position 5 by aryl radicals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US521539A US3413346A (en) | 1966-01-19 | 1966-01-19 | 2-(2-haloethylamino)-5-halo-benzophenones |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO129627B true NO129627B (sv) | 1974-05-06 |
Family
ID=24077140
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO02643/71A NO129627B (sv) | 1966-01-19 | 1971-07-09 |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US3413346A (sv) |
| AT (2) | AT279588B (sv) |
| BE (1) | BE692377A (sv) |
| CH (1) | CH474528A (sv) |
| DE (1) | DE1693070A1 (sv) |
| DK (1) | DK138370B (sv) |
| ES (1) | ES335790A1 (sv) |
| FI (1) | FI47370C (sv) |
| FR (1) | FR1508035A (sv) |
| GB (1) | GB1122962A (sv) |
| GR (1) | GR35175B (sv) |
| IL (1) | IL27108A (sv) |
| MY (1) | MY6900175A (sv) |
| NL (3) | NL6700665A (sv) |
| NO (1) | NO129627B (sv) |
| OA (1) | OA02300A (sv) |
| SE (3) | SE335986B (sv) |
| YU (1) | YU31793B (sv) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3927010A (en) * | 1969-10-17 | 1975-12-16 | Hoffmann La Roche | Diarylmethane derivatives and processes for their preparation |
| US3709898A (en) * | 1971-02-09 | 1973-01-09 | Upjohn Co | Process for the production of triazolobenzodiazepines and intermediates |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3182054A (en) * | 1965-05-04 | Benzodiazepine - compounds | ||
| US3121077A (en) * | 1961-10-20 | 1964-02-11 | Hoffmann La Roche | Substituted-1, 4-benzodiazepine-2-one compounds |
-
1966
- 1966-01-19 US US521539A patent/US3413346A/en not_active Expired - Lifetime
- 1966-12-15 CH CH1792666A patent/CH474528A/de not_active IP Right Cessation
- 1966-12-17 DE DE19661693070 patent/DE1693070A1/de active Pending
- 1966-12-19 AT AT01625/68A patent/AT279588B/de active
- 1966-12-19 AT AT01624/68A patent/AT279587B/de not_active IP Right Cessation
- 1966-12-21 IL IL27108A patent/IL27108A/xx unknown
-
1967
- 1967-01-10 BE BE692377D patent/BE692377A/xx unknown
- 1967-01-11 OA OA52722A patent/OA02300A/xx unknown
- 1967-01-11 GB GB1579/67A patent/GB1122962A/en not_active Expired
- 1967-01-11 SE SE00376/67A patent/SE335986B/xx unknown
- 1967-01-11 FI FI670066A patent/FI47370C/sv active
- 1967-01-11 SE SE7003731A patent/SE379343B/xx unknown
- 1967-01-11 YU YU0040/67A patent/YU31793B/xx unknown
- 1967-01-16 NL NL6700665A patent/NL6700665A/xx unknown
- 1967-01-17 GR GR670135175A patent/GR35175B/el unknown
- 1967-01-18 ES ES335790A patent/ES335790A1/es not_active Expired
- 1967-01-18 FR FR91529A patent/FR1508035A/fr not_active Expired
- 1967-01-18 DK DK30067AA patent/DK138370B/da not_active IP Right Cessation
-
1969
- 1969-12-30 MY MY175/69A patent/MY6900175A/xx unknown
-
1970
- 1970-03-19 SE SE7003733A patent/SE379757B/xx unknown
-
1971
- 1971-05-04 NL NL7106074A patent/NL7106074A/xx unknown
- 1971-05-04 NL NL7106075A patent/NL7106075A/xx unknown
- 1971-07-09 NO NO02643/71A patent/NO129627B/no unknown
Also Published As
| Publication number | Publication date |
|---|---|
| SE379343B (sv) | 1975-10-06 |
| DE1693070A1 (de) | 1971-12-09 |
| IL27108A (en) | 1971-02-25 |
| YU4067A (en) | 1973-06-30 |
| FR1508035A (fr) | 1967-12-29 |
| OA02300A (fr) | 1970-05-05 |
| NL7106074A (sv) | 1971-08-25 |
| DK138370B (da) | 1978-08-21 |
| CH474528A (de) | 1969-06-30 |
| MY6900175A (en) | 1969-12-31 |
| SE379757B (sv) | 1975-10-20 |
| DK138370C (sv) | 1979-02-05 |
| NL6700665A (sv) | 1967-07-20 |
| AT279588B (de) | 1970-03-10 |
| GB1122962A (en) | 1968-08-07 |
| BE692377A (sv) | 1967-07-10 |
| ES335790A1 (es) | 1968-03-16 |
| SE335986B (sv) | 1971-06-21 |
| GR35175B (el) | 1968-08-22 |
| NL7106075A (sv) | 1971-08-25 |
| US3413346A (en) | 1968-11-26 |
| FI47370B (sv) | 1973-07-31 |
| AT279587B (de) | 1970-03-10 |
| FI47370C (sv) | 1974-11-29 |
| YU31793B (en) | 1973-12-31 |
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