NO129141B - - Google Patents
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- Publication number
- NO129141B NO129141B NO05074/69A NO507469A NO129141B NO 129141 B NO129141 B NO 129141B NO 05074/69 A NO05074/69 A NO 05074/69A NO 507469 A NO507469 A NO 507469A NO 129141 B NO129141 B NO 129141B
- Authority
- NO
- Norway
- Prior art keywords
- sodium triphosphate
- steam
- sodium
- triphosphate
- stated
- Prior art date
Links
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 81
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 claims description 77
- 238000000034 method Methods 0.000 claims description 29
- 239000003599 detergent Substances 0.000 claims description 23
- 238000004519 manufacturing process Methods 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 239000012159 carrier gas Substances 0.000 claims description 10
- 239000000843 powder Substances 0.000 description 22
- 239000002002 slurry Substances 0.000 description 19
- 239000013078 crystal Substances 0.000 description 14
- 239000000203 mixture Substances 0.000 description 14
- 150000004687 hexahydrates Chemical class 0.000 description 12
- 239000003795 chemical substances by application Substances 0.000 description 10
- 230000036571 hydration Effects 0.000 description 10
- 238000006703 hydration reaction Methods 0.000 description 10
- 238000003860 storage Methods 0.000 description 9
- -1 alkali metal salts Chemical class 0.000 description 8
- 125000000129 anionic group Chemical group 0.000 description 7
- 239000000344 soap Substances 0.000 description 7
- 150000001875 compounds Chemical class 0.000 description 5
- 238000009833 condensation Methods 0.000 description 5
- 230000005494 condensation Effects 0.000 description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 5
- 229910019142 PO4 Inorganic materials 0.000 description 4
- 230000002209 hydrophobic effect Effects 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 235000021317 phosphate Nutrition 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 238000001694 spray drying Methods 0.000 description 4
- 239000000271 synthetic detergent Substances 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
- 229910052783 alkali metal Inorganic materials 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000007859 condensation product Substances 0.000 description 3
- 230000001627 detrimental effect Effects 0.000 description 3
- FGXJOKTYAQIFRP-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate;hexahydrate Chemical compound O.O.O.O.O.O.[Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O FGXJOKTYAQIFRP-UHFFFAOYSA-I 0.000 description 3
- 239000010452 phosphate Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 230000001105 regulatory effect Effects 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 125000002947 alkylene group Chemical group 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- XPPKVPWEQAFLFU-UHFFFAOYSA-J diphosphate(4-) Chemical compound [O-]P([O-])(=O)OP([O-])([O-])=O XPPKVPWEQAFLFU-UHFFFAOYSA-J 0.000 description 2
- 235000011180 diphosphates Nutrition 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- HSCXJVOGIGDDMR-UHFFFAOYSA-I pentasodium [oxido(phosphonatooxy)phosphoryl] phosphate hydrate Chemical class [O-]P([O-])(=O)OP(=O)([O-])OP(=O)([O-])[O-].O.[Na+].[Na+].[Na+].[Na+].[Na+] HSCXJVOGIGDDMR-UHFFFAOYSA-I 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 235000011178 triphosphate Nutrition 0.000 description 2
- 239000001226 triphosphate Substances 0.000 description 2
- UNXRWKVEANCORM-UHFFFAOYSA-N triphosphoric acid Chemical compound OP(O)(=O)OP(O)(=O)OP(O)(O)=O UNXRWKVEANCORM-UHFFFAOYSA-N 0.000 description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N 1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylic acid Chemical compound C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- 206010039509 Scab Diseases 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000007046 ethoxylation reaction Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 125000001165 hydrophobic group Chemical group 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 150000004668 long chain fatty acids Chemical class 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 125000005608 naphthenic acid group Chemical group 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 description 1
- 239000003784 tall oil Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/06—Phosphates, including polyphosphates
- C11D3/062—Special methods concerning phosphates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/38—Condensed phosphates
- C01B25/40—Polyphosphates
- C01B25/41—Polyphosphates of alkali metals
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/38—Condensed phosphates
- C01B25/40—Polyphosphates
- C01B25/41—Polyphosphates of alkali metals
- C01B25/418—After-treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19681816839 DE1816839B2 (de) | 1968-12-24 | 1968-12-24 | Fuer die herstellung von waschmitteln geeignetes, partiell hydratisiertes alkalitripolyphosphat und verfahren zu seiner herstellung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO129141B true NO129141B (enrdf_load_stackoverflow) | 1974-03-04 |
Family
ID=5717297
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO05074/69A NO129141B (enrdf_load_stackoverflow) | 1968-12-24 | 1969-12-22 |
Country Status (15)
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3954939A (en) * | 1974-05-21 | 1976-05-04 | Stauffer Chemical Company | Method for preparing monocalcium phosphate compositions with reduced caking tendencies |
| US4251498A (en) * | 1979-01-02 | 1981-02-17 | Fmc Corporation | Preparation of granular sodium tripolyphosphate products from screen undersize sodium tripolyphosphate particles |
| US4315898A (en) * | 1980-06-30 | 1982-02-16 | Fmc Corportion | Preparation of granular sodium tripolyphosphate hexahydrate with low friability |
| FR2565574B1 (fr) * | 1984-06-08 | 1988-04-22 | Rhone Poulenc Chim Base | Procede de preparation d'un tripolyphosphate de sodium hexahydrate a haut pouvoir absorbant et tripolyphosphate ainsi prepare |
| US5232620A (en) * | 1991-02-28 | 1993-08-03 | Fmc Corporation | Sodium tripolyphosphate composition and method of producing it |
| WO1999033945A1 (en) * | 1997-12-29 | 1999-07-08 | The Procter & Gamble Company | A process for making a phosphate material |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1054637B (de) * | 1956-01-14 | 1959-04-09 | Procter & Gamble | Verfahren zur Herstellung von Waschmitteln |
| US3394986A (en) * | 1965-04-19 | 1968-07-30 | Monsanto Co | Production of finely divided sodium tripolyphosphate |
| ZA663029B (enrdf_load_stackoverflow) * | 1965-06-25 | |||
| FR1537276A (fr) * | 1966-09-01 | 1968-08-23 | Knapsack Ag | Procédé de préparation de détersifs contenant du tripolyphosphate de sodium |
-
1968
- 1968-12-24 DE DE19681816839 patent/DE1816839B2/de not_active Withdrawn
-
1969
- 1969-12-18 CA CA070242A patent/CA931323A/en not_active Expired
- 1969-12-19 GB GB1295658D patent/GB1295658A/en not_active Expired
- 1969-12-22 ES ES374799A patent/ES374799A1/es not_active Expired
- 1969-12-22 ZA ZA698848*A patent/ZA698848B/xx unknown
- 1969-12-22 NO NO05074/69A patent/NO129141B/no unknown
- 1969-12-22 AT AT1193069A patent/AT300729B/de not_active IP Right Cessation
- 1969-12-22 DK DK679769A patent/DK132529C/da not_active IP Right Cessation
- 1969-12-22 US US887258A patent/US3672826A/en not_active Expired - Lifetime
- 1969-12-22 NL NL6919163.A patent/NL156373B/xx not_active IP Right Cessation
- 1969-12-23 SE SE17889/69A patent/SE358619B/xx unknown
- 1969-12-23 FR FR6944693A patent/FR2030955A5/fr not_active Expired
- 1969-12-23 JP JP44103708A patent/JPS5130037B1/ja active Pending
- 1969-12-23 BE BE743638D patent/BE743638A/xx not_active IP Right Cessation
- 1969-12-24 CH CH1925169A patent/CH544724A/de not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DK132529C (da) | 1976-05-24 |
| ES374799A1 (es) | 1972-04-16 |
| SE358619B (enrdf_load_stackoverflow) | 1973-08-06 |
| FR2030955A5 (enrdf_load_stackoverflow) | 1970-11-13 |
| AT300729B (de) | 1972-08-10 |
| CA931323A (en) | 1973-08-07 |
| GB1295658A (enrdf_load_stackoverflow) | 1972-11-08 |
| JPS5130037B1 (enrdf_load_stackoverflow) | 1976-08-28 |
| DE1816839A1 (de) | 1970-11-12 |
| BE743638A (enrdf_load_stackoverflow) | 1970-06-23 |
| ZA698848B (en) | 1971-08-25 |
| CH544724A (de) | 1973-11-30 |
| NL156373B (nl) | 1978-04-17 |
| NL6919163A (enrdf_load_stackoverflow) | 1970-06-26 |
| DE1816839B2 (de) | 1977-04-14 |
| US3672826A (en) | 1972-06-27 |
| DK132529B (da) | 1975-12-22 |
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