NO128092B - - Google Patents
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- Publication number
- NO128092B NO128092B NO04824/71A NO482471A NO128092B NO 128092 B NO128092 B NO 128092B NO 04824/71 A NO04824/71 A NO 04824/71A NO 482471 A NO482471 A NO 482471A NO 128092 B NO128092 B NO 128092B
- Authority
- NO
- Norway
- Prior art keywords
- tobacco
- impregnation
- compound
- zone
- temperature
- Prior art date
Links
- 241000208125 Nicotiana Species 0.000 claims description 153
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 153
- 238000005470 impregnation Methods 0.000 claims description 104
- 150000001875 compounds Chemical class 0.000 claims description 44
- 238000009835 boiling Methods 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 21
- CYRMSUTZVYGINF-UHFFFAOYSA-N trichlorofluoromethane Chemical compound FC(Cl)(Cl)Cl CYRMSUTZVYGINF-UHFFFAOYSA-N 0.000 claims description 12
- 229940029284 trichlorofluoromethane Drugs 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 6
- 230000001105 regulatory effect Effects 0.000 claims description 4
- 150000002894 organic compounds Chemical class 0.000 claims description 2
- 239000007788 liquid Substances 0.000 description 20
- 239000003795 chemical substances by application Substances 0.000 description 18
- 239000007789 gas Substances 0.000 description 15
- 239000012530 fluid Substances 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 238000011084 recovery Methods 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- 239000003570 air Substances 0.000 description 4
- 238000009833 condensation Methods 0.000 description 4
- 230000005494 condensation Effects 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- QWTDNUCVQCZILF-UHFFFAOYSA-N isopentane Chemical compound CCC(C)C QWTDNUCVQCZILF-UHFFFAOYSA-N 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 235000019504 cigarettes Nutrition 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- RGSFGYAAUTVSQA-UHFFFAOYSA-N Cyclopentane Chemical compound C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N Furan Chemical compound C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- GZUXJHMPEANEGY-UHFFFAOYSA-N bromomethane Chemical compound BrC GZUXJHMPEANEGY-UHFFFAOYSA-N 0.000 description 2
- AFABGHUZZDYHJO-UHFFFAOYSA-N dimethyl butane Natural products CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 150000008282 halocarbons Chemical class 0.000 description 2
- TZIHFWKZFHZASV-UHFFFAOYSA-N methyl formate Chemical compound COC=O TZIHFWKZFHZASV-UHFFFAOYSA-N 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- 238000009834 vaporization Methods 0.000 description 2
- 230000008016 vaporization Effects 0.000 description 2
- RDTZCQIUXDONLZ-UHFFFAOYSA-N 1,1,1-trichloro-2,2-difluoroethane Chemical compound FC(F)C(Cl)(Cl)Cl RDTZCQIUXDONLZ-UHFFFAOYSA-N 0.000 description 1
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 1
- NPNPZTNLOVBDOC-UHFFFAOYSA-N 1,1-difluoroethane Chemical compound CC(F)F NPNPZTNLOVBDOC-UHFFFAOYSA-N 0.000 description 1
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- DDMOUSALMHHKOS-UHFFFAOYSA-N 1,2-dichloro-1,1,2,2-tetrafluoroethane Chemical compound FC(F)(Cl)C(F)(F)Cl DDMOUSALMHHKOS-UHFFFAOYSA-N 0.000 description 1
- RFCAUADVODFSLZ-UHFFFAOYSA-N 1-Chloro-1,1,2,2,2-pentafluoroethane Chemical compound FC(F)(F)C(F)(F)Cl RFCAUADVODFSLZ-UHFFFAOYSA-N 0.000 description 1
- CXBDYQVECUFKRK-UHFFFAOYSA-N 1-methoxybutane Chemical compound CCCCOC CXBDYQVECUFKRK-UHFFFAOYSA-N 0.000 description 1
- BSPCSKHALVHRSR-UHFFFAOYSA-N 2-chlorobutane Chemical compound CCC(C)Cl BSPCSKHALVHRSR-UHFFFAOYSA-N 0.000 description 1
- VOPWNXZWBYDODV-UHFFFAOYSA-N Chlorodifluoromethane Chemical compound FC(F)Cl VOPWNXZWBYDODV-UHFFFAOYSA-N 0.000 description 1
- 239000004340 Chloropentafluoroethane Substances 0.000 description 1
- PMPVIKIVABFJJI-UHFFFAOYSA-N Cyclobutane Chemical compound C1CCC1 PMPVIKIVABFJJI-UHFFFAOYSA-N 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- 239000004338 Dichlorodifluoromethane Substances 0.000 description 1
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical class CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 1
- XOBKSJJDNFUZPF-UHFFFAOYSA-N Methoxyethane Chemical compound CCOC XOBKSJJDNFUZPF-UHFFFAOYSA-N 0.000 description 1
- 239000004341 Octafluorocyclobutane Substances 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 1
- -1 aliphatic alcohols Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
- 239000012080 ambient air Substances 0.000 description 1
- RDHPKYGYEGBMSE-UHFFFAOYSA-N bromoethane Chemical compound CCBr RDHPKYGYEGBMSE-UHFFFAOYSA-N 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 1
- 235000019406 chloropentafluoroethane Nutrition 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 150000004292 cyclic ethers Chemical class 0.000 description 1
- PXBRQCKWGAHEHS-UHFFFAOYSA-N dichlorodifluoromethane Chemical compound FC(F)(Cl)Cl PXBRQCKWGAHEHS-UHFFFAOYSA-N 0.000 description 1
- 235000019404 dichlorodifluoromethane Nutrition 0.000 description 1
- NKDDWNXOKDWJAK-UHFFFAOYSA-N dimethoxymethane Chemical compound COCOC NKDDWNXOKDWJAK-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229960003750 ethyl chloride Drugs 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- WBJINCZRORDGAQ-UHFFFAOYSA-N formic acid ethyl ester Natural products CCOC=O WBJINCZRORDGAQ-UHFFFAOYSA-N 0.000 description 1
- DMEGYFMYUHOHGS-UHFFFAOYSA-N heptamethylene Natural products C1CCCCCC1 DMEGYFMYUHOHGS-UHFFFAOYSA-N 0.000 description 1
- ULYZAYCEDJDHCC-UHFFFAOYSA-N isopropyl chloride Chemical compound CC(C)Cl ULYZAYCEDJDHCC-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229940102396 methyl bromide Drugs 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- SNMVRZFUUCLYTO-UHFFFAOYSA-N n-propyl chloride Chemical compound CCCCl SNMVRZFUUCLYTO-UHFFFAOYSA-N 0.000 description 1
- BCCOBQSFUDVTJQ-UHFFFAOYSA-N octafluorocyclobutane Chemical compound FC1(F)C(F)(F)C(F)(F)C1(F)F BCCOBQSFUDVTJQ-UHFFFAOYSA-N 0.000 description 1
- 235000019407 octafluorocyclobutane Nutrition 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- RKSOPLXZQNSWAS-UHFFFAOYSA-N tert-butyl bromide Chemical compound CC(C)(C)Br RKSOPLXZQNSWAS-UHFFFAOYSA-N 0.000 description 1
- NBRKLOOSMBRFMH-UHFFFAOYSA-N tert-butyl chloride Chemical compound CC(C)(C)Cl NBRKLOOSMBRFMH-UHFFFAOYSA-N 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/18—Other treatment of leaves, e.g. puffing, crimpling, cleaning
- A24B3/182—Puffing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S131/00—Tobacco
- Y10S131/901—Organic liquid employed in puffing tobacco
Landscapes
- Manufacture Of Tobacco Products (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13803971A | 1971-04-28 | 1971-04-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO128092B true NO128092B (fi) | 1973-10-01 |
Family
ID=22480163
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO04824/71A NO128092B (fi) | 1971-04-28 | 1971-12-23 |
Country Status (27)
| Country | Link |
|---|---|
| US (1) | US3693631A (fi) |
| JP (1) | JPS5119039B1 (fi) |
| AU (1) | AU432710B2 (fi) |
| BE (1) | BE777252R (fi) |
| BR (1) | BR7108611D0 (fi) |
| CA (1) | CA955490A (fi) |
| CH (1) | CH580393A5 (fi) |
| CS (1) | CS197343B2 (fi) |
| DE (1) | DE2203105C3 (fi) |
| DK (1) | DK134501B (fi) |
| ES (1) | ES401456A2 (fi) |
| FI (1) | FI52011C (fi) |
| GB (1) | GB1356065A (fi) |
| GT (1) | GT197122835A (fi) |
| HU (1) | HU163923B (fi) |
| IE (1) | IE35925B1 (fi) |
| IL (1) | IL38444A0 (fi) |
| IT (1) | IT1008520B (fi) |
| LU (1) | LU64556A1 (fi) |
| NL (1) | NL152159B (fi) |
| NO (1) | NO128092B (fi) |
| PL (1) | PL83373B1 (fi) |
| RO (1) | RO66356A (fi) |
| SE (1) | SE383952B (fi) |
| SU (1) | SU661994A3 (fi) |
| YU (1) | YU34236B (fi) |
| ZA (1) | ZA717885B (fi) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| USRE29298E (en) * | 1971-11-30 | 1977-07-12 | Brown & Williamson Tobacco Corporation | Deposition of vaporized flavorant on tobacco |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3870053A (en) * | 1972-06-06 | 1975-03-11 | Brown & Williamson Tobacco | Enhancement of flavor and aroma by microwave treatment |
| GB8315987D0 (en) * | 1983-06-10 | 1983-07-13 | British American Tobacco Co | Expansion of tobacco |
| GB8416084D0 (en) * | 1984-06-23 | 1984-07-25 | British American Tobacco Co | Expansion of tobacco |
| EP0242418B1 (de) * | 1986-04-23 | 1989-01-04 | R.J. Reynolds Tobacco GmbH | Verfahren zur Behandlung von Tabak und ähnlichen organischen Materialien |
| US4870980A (en) * | 1987-04-10 | 1989-10-03 | R. J. Reynolds Tobacco Company | Tobacco expansion process and apparatus |
| CA1328064C (en) * | 1987-07-27 | 1994-03-29 | Masao Kobari | Apparatus for expanding material for foodstuffs, favorite items and the like |
| US5056537A (en) * | 1989-09-29 | 1991-10-15 | R. J. Reynolds Tobacco Company | Cigarette |
| US5095922A (en) * | 1990-04-05 | 1992-03-17 | R. J. Reynolds Tobacco Company | Process for increasing the filling power of tobacco material |
| ATE185051T1 (de) * | 1995-06-10 | 1999-10-15 | Rudolf Bichsel | Verfahren und vorrichtung zum puffen von nahrungsmitteln |
| US5657771A (en) * | 1995-07-10 | 1997-08-19 | R. J. Reynolds Tobacco Company | Process and apparatus for tobacco batch preparation and expansion |
| US6586661B1 (en) | 1997-06-12 | 2003-07-01 | North Carolina State University | Regulation of quinolate phosphoribosyl transferase expression by transformation with a tobacco quinolate phosphoribosyl transferase nucleic acid |
| US6209546B1 (en) | 1998-11-30 | 2001-04-03 | Truman W. Ellison | Apparatus and method for improved hydrate formation and improved efficiency of recovery of expansion agent in processes for expanding tobacco and other agricultural products |
| HUP0400161A2 (hu) | 2001-06-08 | 2004-08-30 | Vector Tobacco Ltd., | Módosított nikotin- és nitrozamintartalmú dohány |
| US7556047B2 (en) * | 2003-03-20 | 2009-07-07 | R.J. Reynolds Tobacco Company | Method of expanding tobacco using steam |
| GB201104311D0 (en) | 2011-03-15 | 2011-04-27 | British American Tobacco Co | Method and apparatus for impregnating tobacco industry products with sensate constituents of botanicals |
| CN105595402A (zh) * | 2016-02-24 | 2016-05-25 | 福建中烟工业有限责任公司 | 烟梗处理系统及方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3144871A (en) * | 1962-06-04 | 1964-08-18 | Imp Tobacco Co Ltd | Treatment of tobacco with organic solvents in the vapour phase |
| US3524451A (en) * | 1968-04-10 | 1970-08-18 | Reynolds Tobacco Co R | Process for increasing the filling capacity of tobacco |
| US3612066A (en) * | 1970-02-05 | 1971-10-12 | Reynolds Tobacco Co R | Denicotinizing process |
-
1971
- 1971-04-28 US US138039A patent/US3693631A/en not_active Expired - Lifetime
- 1971-11-18 GT GT197122835A patent/GT197122835A/es unknown
- 1971-11-23 ZA ZA717885A patent/ZA717885B/xx unknown
- 1971-12-23 IE IE1647/71A patent/IE35925B1/xx unknown
- 1971-12-23 NO NO04824/71A patent/NO128092B/no unknown
- 1971-12-23 GB GB6008371A patent/GB1356065A/en not_active Expired
- 1971-12-24 AU AU37352/71A patent/AU432710B2/en not_active Expired
- 1971-12-24 BE BE777252A patent/BE777252R/xx active
- 1971-12-24 IL IL38444A patent/IL38444A0/xx unknown
- 1971-12-27 SE SE7116635A patent/SE383952B/xx unknown
- 1971-12-27 IT IT55020/71A patent/IT1008520B/it active
- 1971-12-27 DK DK634771AA patent/DK134501B/da not_active IP Right Cessation
- 1971-12-28 BR BR008611/71A patent/BR7108611D0/pt unknown
-
1972
- 1972-01-04 NL NL727200074A patent/NL152159B/xx unknown
- 1972-01-06 LU LU64556D patent/LU64556A1/xx unknown
- 1972-01-11 CS CS72165A patent/CS197343B2/cs unknown
- 1972-01-11 JP JP47005020A patent/JPS5119039B1/ja active Pending
- 1972-01-19 CA CA132,781A patent/CA955490A/en not_active Expired
- 1972-01-20 DE DE2203105A patent/DE2203105C3/de not_active Expired
- 1972-01-26 PL PL1972153116A patent/PL83373B1/pl unknown
- 1972-01-28 RO RO7269575A patent/RO66356A/ro unknown
- 1972-01-28 YU YU203/72A patent/YU34236B/xx unknown
- 1972-01-28 HU HURE514A patent/HU163923B/hu unknown
- 1972-02-11 CH CH197072A patent/CH580393A5/xx not_active IP Right Cessation
- 1972-02-22 FI FI720477A patent/FI52011C/fi active
- 1972-04-04 ES ES401456A patent/ES401456A2/es not_active Expired
- 1972-04-14 SU SU721772591A patent/SU661994A3/ru active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| USRE29298E (en) * | 1971-11-30 | 1977-07-12 | Brown & Williamson Tobacco Corporation | Deposition of vaporized flavorant on tobacco |
Also Published As
| Publication number | Publication date |
|---|---|
| FI52011C (fi) | 1977-06-10 |
| AU432710B2 (en) | 1973-03-08 |
| CA955490A (en) | 1974-10-01 |
| DE2203105A1 (de) | 1972-11-02 |
| RO66356A (ro) | 1980-07-15 |
| YU34236B (en) | 1979-04-30 |
| IE35925L (en) | 1972-10-28 |
| ES401456A2 (es) | 1975-02-16 |
| FI52011B (fi) | 1977-02-28 |
| ZA717885B (en) | 1972-08-30 |
| BR7108611D0 (pt) | 1973-09-06 |
| PL83373B1 (en) | 1975-12-31 |
| LU64556A1 (fi) | 1972-08-23 |
| JPS5119039B1 (fi) | 1976-06-14 |
| AU3735271A (en) | 1973-03-08 |
| SU661994A3 (ru) | 1979-05-05 |
| DK134501C (fi) | 1977-04-18 |
| DE2203105C3 (de) | 1978-12-07 |
| IL38444A0 (en) | 1972-02-29 |
| CS197343B2 (en) | 1980-04-30 |
| IT1008520B (it) | 1976-11-30 |
| DK134501B (da) | 1976-11-22 |
| DE2203105B2 (de) | 1978-03-09 |
| SE383952B (sv) | 1976-04-12 |
| BE777252R (fi) | 1972-06-26 |
| HU163923B (fi) | 1973-11-28 |
| GB1356065A (en) | 1974-06-12 |
| NL7200074A (fi) | 1972-10-31 |
| GT197122835A (es) | 1973-05-11 |
| YU20372A (en) | 1978-09-18 |
| IE35925B1 (en) | 1976-06-23 |
| CH580393A5 (fi) | 1976-10-15 |
| NL152159B (nl) | 1977-02-15 |
| US3693631A (en) | 1972-09-26 |
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