NO116720B - - Google Patents
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- Publication number
- NO116720B NO116720B NO161680A NO16168066A NO116720B NO 116720 B NO116720 B NO 116720B NO 161680 A NO161680 A NO 161680A NO 16168066 A NO16168066 A NO 16168066A NO 116720 B NO116720 B NO 116720B
- Authority
- NO
- Norway
- Prior art keywords
- reaction
- temperature
- sulfate
- bis
- carried out
- Prior art date
Links
- 238000006243 chemical reaction Methods 0.000 claims description 24
- 238000000034 method Methods 0.000 claims description 8
- 230000035484 reaction time Effects 0.000 claims description 8
- 125000005270 trialkylamine group Chemical group 0.000 claims description 7
- 239000000376 reactant Substances 0.000 claims description 6
- 125000000217 alkyl group Chemical group 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
- 238000001704 evaporation Methods 0.000 claims description 3
- 230000008020 evaporation Effects 0.000 claims description 3
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 3
- 150000008050 dialkyl sulfates Chemical class 0.000 claims description 2
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 description 10
- 235000011130 ammonium sulphate Nutrition 0.000 description 8
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 7
- VAYGXNSJCAHWJZ-UHFFFAOYSA-N dimethyl sulfate Chemical compound COS(=O)(=O)OC VAYGXNSJCAHWJZ-UHFFFAOYSA-N 0.000 description 6
- 150000001412 amines Chemical class 0.000 description 5
- 239000007795 chemical reaction product Substances 0.000 description 5
- 238000002474 experimental method Methods 0.000 description 5
- 239000001166 ammonium sulphate Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
- -1 dialkyl sulfate ester Chemical class 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- KJFVITRRNTVAPC-UHFFFAOYSA-L tetramethylazanium;sulfate Chemical compound C[N+](C)(C)C.C[N+](C)(C)C.[O-]S([O-])(=O)=O KJFVITRRNTVAPC-UHFFFAOYSA-L 0.000 description 2
- RJFAYQIBOAGBLC-BYPYZUCNSA-N Selenium-L-methionine Chemical compound C[Se]CC[C@H](N)C(O)=O RJFAYQIBOAGBLC-BYPYZUCNSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000010931 ester hydrolysis Methods 0.000 description 1
- RHSSOBQGZQVTHC-UHFFFAOYSA-L ethyl(trimethyl)azanium;sulfate Chemical compound [O-]S([O-])(=O)=O.CC[N+](C)(C)C.CC[N+](C)(C)C RHSSOBQGZQVTHC-UHFFFAOYSA-L 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- TXBULBYASDPNNC-UHFFFAOYSA-L tetraethylazanium;sulfate Chemical compound [O-]S([O-])(=O)=O.CC[N+](CC)(CC)CC.CC[N+](CC)(CC)CC TXBULBYASDPNNC-UHFFFAOYSA-L 0.000 description 1
- YFTHZRPMJXBUME-UHFFFAOYSA-N tripropylamine Chemical compound CCCN(CCC)CCC YFTHZRPMJXBUME-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C211/00—Compounds containing amino groups bound to a carbon skeleton
- C07C211/62—Quaternary ammonium compounds
- C07C211/63—Quaternary ammonium compounds having quaternised nitrogen atoms bound to acyclic carbon atoms
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US432820A US3371117A (en) | 1965-02-15 | 1965-02-15 | Process for preparing bis-quaternary ammonium sulfates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO116720B true NO116720B (ko) | 1969-05-12 |
Family
ID=23717714
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO161680A NO116720B (ko) | 1965-02-15 | 1966-02-14 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3371117A (ko) |
| BE (1) | BE676493A (ko) |
| CH (1) | CH463527A (ko) |
| DE (1) | DE1543747C3 (ko) |
| DK (1) | DK117150B (ko) |
| GB (1) | GB1089029A (ko) |
| IL (1) | IL25174A (ko) |
| LU (1) | LU50449A1 (ko) |
| NL (2) | NL6601948A (ko) |
| NO (1) | NO116720B (ko) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102004010662A1 (de) * | 2004-03-04 | 2005-09-22 | Basf Ag | Verfahren zur Herstellung von Verbindungen mit quaternären sp2-hybridisierten Stickstoffatomen |
| EA200602043A1 (ru) * | 2004-05-28 | 2007-06-29 | Басф Акциенгезельшафт | Способ получения четвертичных аммониевых соединений |
| AR051007A1 (es) * | 2004-08-13 | 2006-12-13 | Basf Ag | Procedimiento para la preparacion de compuestos de amonio cuaternario a presion ambiental |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2569326A (en) * | 1948-07-30 | 1951-09-25 | J B Niederl & Associates Inc | Unsymmetrical quaternary ammonium alkyl sulfates |
-
0
- NL NL130981D patent/NL130981C/xx active
-
1965
- 1965-02-15 US US432820A patent/US3371117A/en not_active Expired - Lifetime
-
1966
- 1966-02-14 IL IL25174A patent/IL25174A/en unknown
- 1966-02-14 NO NO161680A patent/NO116720B/no unknown
- 1966-02-14 LU LU50449A patent/LU50449A1/xx unknown
- 1966-02-15 DE DE1543747A patent/DE1543747C3/de not_active Expired
- 1966-02-15 NL NL6601948A patent/NL6601948A/xx unknown
- 1966-02-15 BE BE676493D patent/BE676493A/xx unknown
- 1966-02-15 GB GB6638/66A patent/GB1089029A/en not_active Expired
- 1966-02-15 CH CH213066A patent/CH463527A/de unknown
- 1966-02-15 DK DK78766AA patent/DK117150B/da unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US3371117A (en) | 1968-02-27 |
| LU50449A1 (ko) | 1966-08-16 |
| DK117150B (da) | 1970-03-23 |
| NL130981C (ko) | 1900-01-01 |
| NL6601948A (ko) | 1966-08-16 |
| DE1543747B2 (de) | 1975-02-06 |
| DE1543747C3 (de) | 1975-09-25 |
| GB1089029A (en) | 1967-11-01 |
| DE1543747A1 (de) | 1969-12-11 |
| CH463527A (de) | 1968-10-15 |
| BE676493A (ko) | 1966-08-16 |
| IL25174A (en) | 1969-11-30 |
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