NL2025805B1 - Method for increasing resistance and yield of resistant dextrin - Google Patents
Method for increasing resistance and yield of resistant dextrin Download PDFInfo
- Publication number
- NL2025805B1 NL2025805B1 NL2025805A NL2025805A NL2025805B1 NL 2025805 B1 NL2025805 B1 NL 2025805B1 NL 2025805 A NL2025805 A NL 2025805A NL 2025805 A NL2025805 A NL 2025805A NL 2025805 B1 NL2025805 B1 NL 2025805B1
- Authority
- NL
- Netherlands
- Prior art keywords
- enzymolysis
- resistant dextrin
- added
- yield
- resistance
- Prior art date
Links
- 229920001353 Dextrin Polymers 0.000 title claims abstract description 155
- 239000004375 Dextrin Substances 0.000 title claims abstract description 96
- 235000019425 dextrin Nutrition 0.000 title claims abstract description 96
- 238000000034 method Methods 0.000 title claims abstract description 42
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 59
- 108010028688 Isoamylase Proteins 0.000 claims abstract description 43
- 239000004382 Amylase Substances 0.000 claims abstract description 41
- 230000002255 enzymatic effect Effects 0.000 claims abstract description 36
- 238000001556 precipitation Methods 0.000 claims abstract description 3
- 229920002472 Starch Polymers 0.000 claims description 65
- 239000008107 starch Substances 0.000 claims description 65
- 235000019698 starch Nutrition 0.000 claims description 65
- 239000002253 acid Substances 0.000 claims description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- 238000002386 leaching Methods 0.000 claims description 20
- 102000004190 Enzymes Human genes 0.000 claims description 15
- 108090000790 Enzymes Proteins 0.000 claims description 15
- 238000000967 suction filtration Methods 0.000 claims description 13
- 238000001914 filtration Methods 0.000 claims description 11
- 238000002156 mixing Methods 0.000 claims description 11
- 239000002244 precipitate Substances 0.000 claims description 11
- 230000000694 effects Effects 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 2
- 239000000413 hydrolysate Substances 0.000 abstract description 31
- 238000002360 preparation method Methods 0.000 abstract description 15
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 abstract description 11
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 abstract description 10
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 abstract description 10
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 abstract description 10
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 abstract description 10
- 239000008103 glucose Substances 0.000 abstract description 10
- 235000013325 dietary fiber Nutrition 0.000 abstract description 8
- 239000000047 product Substances 0.000 abstract description 6
- 108060008539 Transglutaminase Proteins 0.000 description 35
- 102000003601 transglutaminase Human genes 0.000 description 35
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 18
- 229920002261 Corn starch Polymers 0.000 description 11
- 239000008120 corn starch Substances 0.000 description 11
- 238000004458 analytical method Methods 0.000 description 10
- 238000004364 calculation method Methods 0.000 description 10
- 230000009471 action Effects 0.000 description 9
- 238000001035 drying Methods 0.000 description 9
- 238000000197 pyrolysis Methods 0.000 description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 238000006911 enzymatic reaction Methods 0.000 description 6
- 238000007086 side reaction Methods 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 229920001503 Glucan Polymers 0.000 description 3
- 239000003929 acidic solution Substances 0.000 description 3
- 230000003247 decreasing effect Effects 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 108010065511 Amylases Proteins 0.000 description 2
- 102000013142 Amylases Human genes 0.000 description 2
- 108010009736 Protein Hydrolysates Proteins 0.000 description 2
- 235000019418 amylase Nutrition 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 102000003925 1,4-alpha-Glucan Branching Enzyme Human genes 0.000 description 1
- 108090000344 1,4-alpha-Glucan Branching Enzyme Proteins 0.000 description 1
- ZCLAHGAZPPEVDX-UHFFFAOYSA-N D-panose Natural products OC1C(O)C(O)C(OC(C(O)CO)C(O)C(O)C=O)OC1COC1C(O)C(O)C(O)C(CO)O1 ZCLAHGAZPPEVDX-UHFFFAOYSA-N 0.000 description 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- AYRXSINWFIIFAE-SCLMCMATSA-N Isomaltose Natural products OC[C@H]1O[C@H](OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O)[C@@H](O)[C@@H](O)[C@@H]1O AYRXSINWFIIFAE-SCLMCMATSA-N 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 102000038379 digestive enzymes Human genes 0.000 description 1
- 108091007734 digestive enzymes Proteins 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- DLRVVLDZNNYCBX-RTPHMHGBSA-N isomaltose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)C(O)O1 DLRVVLDZNNYCBX-RTPHMHGBSA-N 0.000 description 1
- TWNIBLMWSKIRAT-VFUOTHLCSA-N levoglucosan Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@H]2CO[C@@H]1O2 TWNIBLMWSKIRAT-VFUOTHLCSA-N 0.000 description 1
- 238000010606 normalization Methods 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- ZCLAHGAZPPEVDX-MQHGYYCBSA-N panose Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@@H](O[C@H]([C@H](O)CO)[C@H](O)[C@@H](O)C=O)O[C@@H]1CO[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 ZCLAHGAZPPEVDX-MQHGYYCBSA-N 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 235000021067 refined food Nutrition 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/04—Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
- C12P19/08—Dextran
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/14—Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910571371.8A CN110295208B (zh) | 2019-06-28 | 2019-06-28 | 一种提升抗性糊精抗性和产量的方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NL2025805A NL2025805A (en) | 2021-01-26 |
| NL2025805B1 true NL2025805B1 (en) | 2022-08-17 |
Family
ID=68029272
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NL2025805A NL2025805B1 (en) | 2019-06-28 | 2020-06-10 | Method for increasing resistance and yield of resistant dextrin |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN110295208B (zh) |
| NL (1) | NL2025805B1 (zh) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112725312B (zh) * | 2021-01-25 | 2023-06-30 | 浙江大学 | 一种复合酶及抗性糊精的制备方法 |
| CN115053965B (zh) * | 2022-07-11 | 2023-09-08 | 山东省食品发酵工业研究设计院 | 一种利用超高压处理制备难消化性更强的抗性糊精的方法 |
| CN115181189A (zh) * | 2022-07-26 | 2022-10-14 | 河南飞天生物科技股份有限公司 | 一种抗性糊精联产戊聚糖的方法及其系统 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AR053259A1 (es) * | 2005-05-02 | 2007-04-25 | Nippon Flour Mills | Trigo con nuevo almidon y metodo para producirlo |
| CN104403009B (zh) * | 2014-11-21 | 2016-08-17 | 广东省食品工业研究所 | 一种抗性糊精的制备方法 |
| CN104762346B (zh) * | 2015-03-19 | 2018-04-10 | 江苏省奥谷生物科技有限公司 | β‑环糊精和超高麦芽糖浆联产制备工艺 |
| CN106318991A (zh) * | 2016-08-19 | 2017-01-11 | 山东百龙创园生物科技有限公司 | 一种抗性糊精及其制备方法 |
| CN109182417B (zh) * | 2018-09-18 | 2022-06-17 | 山东百龙创园生物科技股份有限公司 | 一种还原性抗性糊精的制备方法 |
-
2019
- 2019-06-28 CN CN201910571371.8A patent/CN110295208B/zh active Active
-
2020
- 2020-06-10 NL NL2025805A patent/NL2025805B1/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| CN110295208B (zh) | 2023-04-18 |
| CN110295208A (zh) | 2019-10-01 |
| NL2025805A (en) | 2021-01-26 |
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| Date | Code | Title | Description |
|---|---|---|---|
| MM | Lapsed because of non-payment of the annual fee |
Effective date: 20230701 |