MX374656B - Método para determinar una concentración de un inhibidor de incrustaciones en una muestra. - Google Patents
Método para determinar una concentración de un inhibidor de incrustaciones en una muestra.Info
- Publication number
- MX374656B MX374656B MX2016006512A MX2016006512A MX374656B MX 374656 B MX374656 B MX 374656B MX 2016006512 A MX2016006512 A MX 2016006512A MX 2016006512 A MX2016006512 A MX 2016006512A MX 374656 B MX374656 B MX 374656B
- Authority
- MX
- Mexico
- Prior art keywords
- sample
- scale inhibitor
- concentration
- determining
- signal
- Prior art date
Links
- 239000002455 scale inhibitor Substances 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 3
- 229910052747 lanthanoid Inorganic materials 0.000 abstract 2
- 150000002602 lanthanoids Chemical class 0.000 abstract 2
- 239000003153 chemical reaction reagent Substances 0.000 abstract 1
- 238000007865 diluting Methods 0.000 abstract 1
- 230000005284 excitation Effects 0.000 abstract 1
- 238000004020 luminiscence type Methods 0.000 abstract 1
- 238000005259 measurement Methods 0.000 abstract 1
- 150000002894 organic compounds Chemical class 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/64—Fluorescence; Phosphorescence
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/64—Fluorescence; Phosphorescence
- G01N21/6408—Fluorescence; Phosphorescence with measurement of decay time, time resolved fluorescence
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/34—Purifying; Cleaning
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/38—Diluting, dispersing or mixing samples
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/75—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
- G01N21/77—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/64—Fluorescence; Phosphorescence
- G01N2021/6417—Spectrofluorimetric devices
- G01N2021/6419—Excitation at two or more wavelengths
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/64—Fluorescence; Phosphorescence
- G01N2021/6417—Spectrofluorimetric devices
- G01N2021/6421—Measuring at two or more wavelengths
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/75—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
- G01N21/77—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
- G01N2021/7769—Measurement method of reaction-produced change in sensor
- G01N2021/7786—Fluorescence
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pathology (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Engineering & Computer Science (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Plasma & Fusion (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biomedical Technology (AREA)
- Molecular Biology (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Abstract
La invención se refiere a un método para determinar la concentración de un inhibidor de incrustaciones en una muestra que comprende por lo menos un primer inhibidor de incrustaciones, que es un compuesto orgánico sintético que incluye por lo menos un grupo ionizado. El método comprende, opcionalmente, diluir y/o purificar la muestra y permitir que la muestra interactúe con un reactivo que comprende un ión lantánido (III). La muestra es activada mediante una primera longitud de onda de activación y una señal de muestra que se deriva del ión lantánido (III) es detectada a una longitud de onda de señal utilizando una medición de luminiscencia de tiempo resuelto y se determina la concentración de por lo menos un primer inhibidor de incrustaciones en la muestra utilizando la señal de muestra detectada.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI20136151A FI125102B (en) | 2013-11-19 | 2013-11-19 | Method for the determination of an antifouling agent in a sample |
| PCT/FI2014/050877 WO2015075308A1 (en) | 2013-11-19 | 2014-11-18 | Method for determining a scale inhibitor concentration in a sample |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2016006512A MX2016006512A (es) | 2016-08-05 |
| MX374656B true MX374656B (es) | 2025-03-06 |
Family
ID=52002990
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2016006512A MX374656B (es) | 2013-11-19 | 2014-11-18 | Método para determinar una concentración de un inhibidor de incrustaciones en una muestra. |
Country Status (12)
| Country | Link |
|---|---|
| US (2) | US9958389B2 (es) |
| EP (1) | EP3071949B1 (es) |
| CN (1) | CN105917214B (es) |
| AR (1) | AR098472A1 (es) |
| CA (1) | CA2928989C (es) |
| DK (1) | DK3071949T3 (es) |
| ES (1) | ES2687596T3 (es) |
| FI (1) | FI125102B (es) |
| HU (1) | HUE039925T2 (es) |
| MX (1) | MX374656B (es) |
| PL (1) | PL3071949T3 (es) |
| WO (1) | WO2015075308A1 (es) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI125111B (en) * | 2013-11-19 | 2015-06-15 | Kemira Oyj | A method for analyzing a sample comprising first and second anticaking agents |
| FI125102B (en) * | 2013-11-19 | 2015-06-15 | Kemira Oyj | Method for the determination of an antifouling agent in a sample |
| FI127399B (en) | 2016-02-19 | 2018-05-15 | Kemira Oyj | Procedure for handling liquid samples |
| FR3062480B1 (fr) * | 2017-01-31 | 2019-06-07 | S.P.C.M. Sa | Methode de determination de la densite de charge anionique d'un polymere |
| FR3064364A1 (fr) * | 2017-03-27 | 2018-09-28 | S.P.C.M. Sa | Methode de dosage de polymeres cationiques |
| CA3113136A1 (en) * | 2018-10-01 | 2020-04-09 | Kemira Oyj | A method for determining hydrolysis degree and charge density of polyelectrolytes and phosphonates |
| BR112021005427B1 (pt) | 2018-10-01 | 2023-12-26 | Kemira Oyj | Método para determinação da concentração de polieletrólitos e fosfonatos e uso do mesmo |
| US10739269B2 (en) | 2018-10-18 | 2020-08-11 | Baker Hughes, A Ge Company, Llc | Detection of trace chemicals in oil and gas applications |
| WO2020260684A1 (en) | 2019-06-28 | 2020-12-30 | Københavns Universitet | An optical sensor |
| CN114059968A (zh) * | 2021-11-11 | 2022-02-18 | 中国海洋石油集团有限公司 | 一种油田固体防垢块投放装置及井下投放方法 |
| WO2025152095A1 (en) * | 2024-01-18 | 2025-07-24 | Saudi Arabian Oil Company | Methods for determining polymeric scale inhibitor concentrations in produced waters |
Family Cites Families (38)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US3962110A (en) | 1970-10-19 | 1976-06-08 | Texaco Inc. | Process and composition for preventing scale build-up |
| US4416785A (en) | 1982-05-17 | 1983-11-22 | Uop Inc. | Scale-inhibiting compositions of matter |
| SE8301395L (sv) * | 1983-03-15 | 1984-09-16 | Wallac Oy | Kelatiserande foreningar med funktionella grupper vilka tillater kovalent koppling till bio-organiska molekyler |
| EP0533333A3 (en) * | 1991-09-19 | 1993-07-28 | Texaco Development Corporation | Optical photometry system |
| US5411889A (en) * | 1994-02-14 | 1995-05-02 | Nalco Chemical Company | Regulating water treatment agent dosage based on operational system stresses |
| US5389548A (en) * | 1994-03-29 | 1995-02-14 | Nalco Chemical Company | Monitoring and in-system concentration control of polyelectrolytes using fluorochromatic dyes |
| CN1069162C (zh) * | 1994-05-02 | 2001-08-08 | 诺尔科化学公司 | 用作改进的抗微生物剂的荧光杀生物剂组合物 |
| US5658798A (en) * | 1996-02-08 | 1997-08-19 | Nalco Chemical Company | Detection of process components in food process streams by fluorescence |
| TWI227323B (en) * | 1998-03-11 | 2005-02-01 | Sensors For Med & Science Inc | Detection of analytes by fluorescent lanthanide metal chelate complexes containing substituted ligands |
| JP4218133B2 (ja) | 1999-06-15 | 2009-02-04 | オルガノ株式会社 | ポリカルボン酸類の選択的検出方法 |
| US6329205B1 (en) * | 1999-08-31 | 2001-12-11 | Molecular Probes, Inc. | Detection method using luminescent europium-based protein stains |
| US6312644B1 (en) * | 1999-12-16 | 2001-11-06 | Nalco Chemical Company | Fluorescent monomers and polymers containing same for use in industrial water systems |
| US6645428B1 (en) * | 2000-04-27 | 2003-11-11 | Ondeo Nalco Company | Fluorescent monomers and tagged treatment polymers containing same for use in industrial water systems |
| DE10042498A1 (de) * | 2000-08-30 | 2002-04-11 | Bayer Ag | Polyasparaginsäure-Konzentrationsbestimmung mittels Fluorometrie |
| US6790664B2 (en) * | 2001-12-28 | 2004-09-14 | Nalco Company | Fluorometric monitoring and control of soluble hardness of water used in industrial water systems |
| ATE393294T1 (de) | 2003-06-25 | 2008-05-15 | Rhodia Chimie Sa | Verfahren zur stimulierung einer ölbohrung durch verwendung verschiedener ablagerungsinhibitoren |
| US20050036903A1 (en) * | 2003-06-26 | 2005-02-17 | Patrick Colclasure | Pewitt analyzer |
| US7179384B2 (en) * | 2004-04-30 | 2007-02-20 | Nalco Company | Control of cooling water system using rate of consumption of fluorescent polymer |
| US7772009B2 (en) * | 2005-11-22 | 2010-08-10 | SCR Research, LLC | Room temperature phosphorescence apparatus and methods |
| US7532321B2 (en) * | 2006-09-08 | 2009-05-12 | Strategic Diagnostics Inc. | Compositions and methods for the detection of water treatment polymers |
| US20080169243A1 (en) * | 2007-01-11 | 2008-07-17 | Dave Bhasker B | Method of inhibiting scale formation and deposition in desalination systems |
| US7985318B2 (en) * | 2007-05-10 | 2011-07-26 | Nalco Company | Method of monitoring and inhibiting scale deposition in pulp mill evaporators and concentrators |
| US20090101587A1 (en) * | 2007-10-22 | 2009-04-23 | Peter Blokker | Method of inhibiting scale formation and deposition in desalination systems |
| BRPI0820943A2 (pt) * | 2007-12-17 | 2015-06-30 | Lux Innovate Ltd | Composições e métodos para monitorização de fluxo através de sistemas de condução e contenção de fluido |
| US20110027803A1 (en) * | 2007-12-17 | 2011-02-03 | Artin Moussavi | Compositions and Methods for Maintenance of Fluid Conducting and Containment Systems |
| US20120032093A1 (en) * | 2010-08-03 | 2012-02-09 | Kemira Chemicals Inc. | Tagged scale inhibitor compositions and methods of inhibiting scale |
| CN102455291B (zh) * | 2010-10-20 | 2017-04-12 | 纳尔科公司 | 使用荧光技术检测污染的方法 |
| RU2550625C2 (ru) | 2011-01-19 | 2015-05-10 | Родиа Операсьон | Семейства ингибиторов солевых отложений, имеющих отличные профили поглощения, и их применение в нефтяном промысле |
| AR092855A1 (es) * | 2012-07-10 | 2015-05-06 | Kemira Oyj | Composiciones polimericas de inhibicion de incrustaciones marcadas y metodos para inhibir la formacion de incrustaciones |
| US9086383B2 (en) * | 2012-09-14 | 2015-07-21 | Halliburton Energy Services, Inc. | Systems and methods for monitoring chemical processes |
| US20140100142A1 (en) * | 2012-10-05 | 2014-04-10 | Meadwestvaco Corporation | Traceable polymeric scale inhibitors and methods of using such scale inhibitors |
| US9751789B2 (en) * | 2012-12-28 | 2017-09-05 | Ecolab Usa Inc. | Fluorescent monomers and tagged treatment polymers containing same for use in industrial water systems |
| US9028747B2 (en) * | 2012-12-28 | 2015-05-12 | Ecolab Usa Inc. | Corrosion and fouling mitigation using non-phosphorus based additives |
| US9804076B2 (en) * | 2013-03-13 | 2017-10-31 | Baker Hughes, A Ge Company, Llc | Use of detection techniques for contaminant and corrosion control in industrial processes |
| US9169164B2 (en) * | 2013-04-05 | 2015-10-27 | Ecolab Usa Inc. | Polymers useful in agricultural applications |
| FI125111B (en) * | 2013-11-19 | 2015-06-15 | Kemira Oyj | A method for analyzing a sample comprising first and second anticaking agents |
| FI125102B (en) * | 2013-11-19 | 2015-06-15 | Kemira Oyj | Method for the determination of an antifouling agent in a sample |
| FR3015547B1 (fr) * | 2013-12-20 | 2016-01-01 | Total Sa | Methode pour ajuster le taux d'inhibiteurs dans un puits de petrole ou de gaz |
-
2013
- 2013-11-19 FI FI20136151A patent/FI125102B/en active IP Right Grant
-
2014
- 2014-11-18 CA CA2928989A patent/CA2928989C/en active Active
- 2014-11-18 EP EP14805964.5A patent/EP3071949B1/en active Active
- 2014-11-18 PL PL14805964T patent/PL3071949T3/pl unknown
- 2014-11-18 CN CN201480073517.1A patent/CN105917214B/zh not_active Expired - Fee Related
- 2014-11-18 WO PCT/FI2014/050877 patent/WO2015075308A1/en not_active Ceased
- 2014-11-18 HU HUE14805964A patent/HUE039925T2/hu unknown
- 2014-11-18 ES ES14805964.5T patent/ES2687596T3/es active Active
- 2014-11-18 US US15/037,680 patent/US9958389B2/en active Active
- 2014-11-18 MX MX2016006512A patent/MX374656B/es active IP Right Grant
- 2014-11-18 DK DK14805964.5T patent/DK3071949T3/en active
- 2014-11-19 AR ARP140104346A patent/AR098472A1/es active IP Right Grant
-
2018
- 2018-03-21 US US15/928,056 patent/US10914679B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP3071949B1 (en) | 2018-06-27 |
| EP3071949A1 (en) | 2016-09-28 |
| CN105917214B (zh) | 2019-05-07 |
| AR098472A1 (es) | 2016-06-01 |
| CN105917214A (zh) | 2016-08-31 |
| HUE039925T2 (hu) | 2019-02-28 |
| FI125102B (en) | 2015-06-15 |
| US9958389B2 (en) | 2018-05-01 |
| ES2687596T3 (es) | 2018-10-26 |
| PL3071949T3 (pl) | 2018-11-30 |
| US20180284022A1 (en) | 2018-10-04 |
| DK3071949T3 (en) | 2018-10-15 |
| US20160290923A1 (en) | 2016-10-06 |
| WO2015075308A1 (en) | 2015-05-28 |
| FI20136151A7 (fi) | 2015-05-20 |
| MX2016006512A (es) | 2016-08-05 |
| US10914679B2 (en) | 2021-02-09 |
| CA2928989A1 (en) | 2015-05-28 |
| CA2928989C (en) | 2022-05-10 |
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Legal Events
| Date | Code | Title | Description |
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| FG | Grant or registration |