MX354639B - Procedimiento para la eliminacion de contaminantes a partir de una hidroclorofluoro-olefina mediante destilacion extractiva. - Google Patents
Procedimiento para la eliminacion de contaminantes a partir de una hidroclorofluoro-olefina mediante destilacion extractiva.Info
- Publication number
- MX354639B MX354639B MX2014010500A MX2014010500A MX354639B MX 354639 B MX354639 B MX 354639B MX 2014010500 A MX2014010500 A MX 2014010500A MX 2014010500 A MX2014010500 A MX 2014010500A MX 354639 B MX354639 B MX 354639B
- Authority
- MX
- Mexico
- Prior art keywords
- contaminant
- hydrochlorofhioroolefin
- extractive
- extractive distillation
- removal
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 5
- 238000000895 extractive distillation Methods 0.000 title abstract 4
- 239000000356 contaminant Substances 0.000 title abstract 3
- 239000002904 solvent Substances 0.000 abstract 3
- KYKAJFCTULSVSH-UHFFFAOYSA-N chloro(fluoro)methane Chemical compound F[C]Cl KYKAJFCTULSVSH-UHFFFAOYSA-N 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 2
- LDTMPQQAWUMPKS-OWOJBTEDSA-N (e)-1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)\C=C\Cl LDTMPQQAWUMPKS-OWOJBTEDSA-N 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- CYRMSUTZVYGINF-UHFFFAOYSA-N trichlorofluoromethane Chemical compound FC(Cl)(Cl)Cl CYRMSUTZVYGINF-UHFFFAOYSA-N 0.000 abstract 1
- 229940029284 trichlorofluoromethane Drugs 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
- C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/40—Extractive distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/07—Optical isomers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Un método para separar un contaminante de una hidroclorofluoro-olefina (tal como trans-1,1,1-trifluoro-3-cloro-2 -propeno (1233zd(E))) incluye extraer un clorofluorocarburo (tal como triclorofluorometano (R11)) de una mezcla que comprende la hidroclorofluoro-olefina y el clorofluorocarburo utilizando una destilación extractiva en presencia de un disolvente extractivo que comprende un compuesto dorado, para formar una hidroclorofluoro-olefina purificada. Este método de separación proporciona la eliminación de un contaminante tal como R11 a partir de una hidroclorofluoro-olefina tal como 1232zd(E), que no son separables por métodos de destilación convencionales. El método puede emplear un procedimiento que utilice dos columnas de destilación, por ejemplo una primera columna de destilación extractiva y una segunda columna de recuperación de disolvente, que permite el reciclaje del disolvente extractivo a la primera columna de destilación extractiva.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261605883P | 2012-03-02 | 2012-03-02 | |
| PCT/US2013/027205 WO2013130342A1 (en) | 2012-03-02 | 2013-02-22 | Process for the removal of contaminant from a hydrochlorofluoroolefin by extractive distillation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2014010500A MX2014010500A (es) | 2014-11-26 |
| MX354639B true MX354639B (es) | 2018-03-14 |
Family
ID=49083170
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2014010500A MX354639B (es) | 2012-03-02 | 2013-02-22 | Procedimiento para la eliminacion de contaminantes a partir de una hidroclorofluoro-olefina mediante destilacion extractiva. |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US9284241B2 (es) |
| EP (2) | EP3511312B1 (es) |
| JP (1) | JP6230548B2 (es) |
| KR (1) | KR102029667B1 (es) |
| CN (2) | CN104144900A (es) |
| BR (1) | BR112014021670B1 (es) |
| CA (1) | CA2866326C (es) |
| ES (2) | ES2811226T3 (es) |
| HU (2) | HUE043143T2 (es) |
| IN (1) | IN2014DN07237A (es) |
| MX (1) | MX354639B (es) |
| PL (2) | PL3511312T3 (es) |
| TR (1) | TR201902296T4 (es) |
| TW (1) | TWI606028B (es) |
| WO (1) | WO2013130342A1 (es) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6668254B2 (ja) * | 2014-01-13 | 2020-03-18 | アルケマ フランス | １，１，３，３−テトラクロロプロペンからｅ−１−クロロ−３，３，３−トリフルオロプロペンを製造する方法 |
| FR3032706B1 (fr) * | 2015-02-17 | 2019-10-11 | Arkema France | Procede de separation du 2-chloro-1,1-difluoroethane et du trans-dichloroethylene |
| CN105601471B (zh) * | 2015-10-22 | 2017-08-25 | 北京宇极科技发展有限公司 | 3,3,4,4,5,5‑六氟环戊烯的提纯方法 |
| CN106631683A (zh) * | 2016-11-16 | 2017-05-10 | 西安近代化学研究所 | 一种提纯1,1,1,3,3‑五氟丙烷的方法 |
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| DE2403310A1 (de) * | 1973-01-29 | 1974-08-08 | Lummus Co | Erzeugung von chlorfluormethanen |
| JPS49134609A (es) * | 1973-05-08 | 1974-12-25 | ||
| JPS606337B2 (ja) * | 1979-05-24 | 1985-02-18 | 株式会社トクヤマ | 塩素化炭化水素の精製方法 |
| GB9018372D0 (en) * | 1990-08-21 | 1990-10-03 | Ici Plc | Separation process |
| JPH04316525A (ja) * | 1991-04-16 | 1992-11-06 | Showa Denko Kk | １，１，１，２−テトラフルオロエタンの精製方法 |
| ES2134446T3 (es) * | 1994-02-07 | 1999-10-01 | Du Pont | Procedimiento para separar pentafluoroetano de una mezcla que comprende hidrocarburos halogenados y cloropentafluoroetano. |
| EP0729932A1 (en) * | 1995-03-03 | 1996-09-04 | Central Glass Company, Limited | Method of producing halopropane |
| JPH11209316A (ja) * | 1998-01-27 | 1999-08-03 | Central Glass Co Ltd | １，１，１，３，３−ペンタフルオロプロパンの分離方法 |
| JPH10310541A (ja) * | 1997-03-11 | 1998-11-24 | Central Glass Co Ltd | １，１，１，３，３−ペンタフルオロプロパンの分離方法 |
| DE69807962T2 (de) * | 1997-03-11 | 2003-01-30 | Central Glass Co., Ltd. | Verfahren zur Reinigung von rohem 1,1,1,3,3-Pentafluorpropan |
| US7371309B2 (en) * | 1997-08-12 | 2008-05-13 | E. I. Du Pont De Nemours And Company | Purification of difluoromethane by extractive distillation |
| US6264399B1 (en) | 1999-10-14 | 2001-07-24 | The Lubrizol Corporation | Method to remediate soil using a surfactant of a salt of an acrylamidoalkanesulfonic acid-amine reaction product |
| JP4225736B2 (ja) * | 2002-03-11 | 2009-02-18 | 昭和電工株式会社 | フルオロエタンの製造方法およびその用途 |
| US7423103B2 (en) * | 2004-06-21 | 2008-09-09 | Exxonmobil Chemical Patents Inc. | Low fouling and high activity polymerization process |
| CN101583582B (zh) * | 2006-09-08 | 2013-09-11 | 纳幕尔杜邦公司 | 包含1,1,1,2,3-五氟丙烯和氟化氢的共沸组合物及其用途 |
| US7981312B2 (en) * | 2006-10-31 | 2011-07-19 | E. I. Du Pont De Nemours And Company | Processes for producing and compositions comprising 2,3,3,3-tetrafluoropropene and/or 1,2,3,3-tetrafluoropropene |
| KR20100017987A (ko) * | 2007-09-13 | 2010-02-16 | 알케마 인코포레이티드 | 하이드로플루오로올레핀의 ｚ 및 ｅ 입체이성체의 조합물을 함유하는 조성물 |
| WO2010009090A2 (en) * | 2008-07-16 | 2010-01-21 | Honeywell International Inc. | Hfo-1234ze mixed isomers with hfc-245fa as a blowing agent, aerosol, and solvent |
| CN105646135A (zh) * | 2008-11-19 | 2016-06-08 | 阿科玛股份有限公司 | 用于制造氢氯氟烯烃的方法 |
| US8217208B2 (en) * | 2008-12-12 | 2012-07-10 | Honeywell International, Inc. | Isomerization of 1-chloro-3,3,3-trifluoropropene |
| US8075797B2 (en) * | 2009-01-29 | 2011-12-13 | Honeywell International Inc. | Azeotrope-like compositions of pentafluoropropane, chlorotrifluoropropene, and hydrogen fluoride |
| JP5477011B2 (ja) * | 2009-02-03 | 2014-04-23 | セントラル硝子株式会社 | （ｚ）−１−クロロ−３，３，３−トリフルオロプロペンの精製方法 |
| PL2411353T3 (pl) * | 2009-03-24 | 2019-01-31 | Arkema Inc. | Oddzielanie R-1233 od fluorowodoru |
| US8486293B2 (en) * | 2009-10-30 | 2013-07-16 | E I Du Pont De Nemours And Company | Hydrogen fluoride-HFC-254eb azeotrope and its uses |
| US9045386B2 (en) * | 2010-02-18 | 2015-06-02 | Honeywell International Inc. | Integrated process and methods of producing (E)-1-chloro-3,3,3-trifluoropropene |
| US8293954B2 (en) * | 2010-03-10 | 2012-10-23 | Honeywell International Inc. | Catalyst life improvement for the vapor phase manufacture of 1-chloro-3,3,3-trifluoropropene |
| EP2550247B1 (en) * | 2010-07-23 | 2014-08-20 | Daikin Industries, Ltd. | Purification method of 2,3,3,3-tetrafluoropropene |
-
2013
- 2013-02-22 BR BR112014021670-3A patent/BR112014021670B1/pt active IP Right Grant
- 2013-02-22 CN CN201380012242.6A patent/CN104144900A/zh active Pending
- 2013-02-22 WO PCT/US2013/027205 patent/WO2013130342A1/en not_active Ceased
- 2013-02-22 EP EP19152628.4A patent/EP3511312B1/en active Active
- 2013-02-22 US US14/381,011 patent/US9284241B2/en active Active
- 2013-02-22 HU HUE13754019A patent/HUE043143T2/hu unknown
- 2013-02-22 HU HUE19152628A patent/HUE050404T2/hu unknown
- 2013-02-22 CA CA2866326A patent/CA2866326C/en active Active
- 2013-02-22 IN IN7237DEN2014 patent/IN2014DN07237A/en unknown
- 2013-02-22 KR KR1020147024526A patent/KR102029667B1/ko active Active
- 2013-02-22 TR TR2019/02296T patent/TR201902296T4/tr unknown
- 2013-02-22 ES ES19152628T patent/ES2811226T3/es active Active
- 2013-02-22 CN CN201810601276.3A patent/CN108863713B/zh active Active
- 2013-02-22 MX MX2014010500A patent/MX354639B/es active IP Right Grant
- 2013-02-22 PL PL19152628T patent/PL3511312T3/pl unknown
- 2013-02-22 JP JP2014559928A patent/JP6230548B2/ja active Active
- 2013-02-22 PL PL13754019T patent/PL2819980T3/pl unknown
- 2013-02-22 ES ES13754019T patent/ES2711134T3/es active Active
- 2013-02-22 EP EP13754019.1A patent/EP2819980B1/en active Active
- 2013-03-01 TW TW102107390A patent/TWI606028B/zh active
Also Published As
| Publication number | Publication date |
|---|---|
| IN2014DN07237A (es) | 2015-04-24 |
| EP2819980A1 (en) | 2015-01-07 |
| JP6230548B2 (ja) | 2017-11-15 |
| TW201336807A (zh) | 2013-09-16 |
| KR102029667B1 (ko) | 2019-10-08 |
| CN108863713B (zh) | 2024-05-07 |
| TR201902296T4 (tr) | 2019-03-21 |
| US20150005539A1 (en) | 2015-01-01 |
| HUE050404T2 (hu) | 2020-12-28 |
| EP2819980A4 (en) | 2015-11-25 |
| CN104144900A (zh) | 2014-11-12 |
| MX2014010500A (es) | 2014-11-26 |
| BR112014021670B1 (pt) | 2020-09-29 |
| HUE043143T2 (hu) | 2019-08-28 |
| JP2015511955A (ja) | 2015-04-23 |
| TWI606028B (zh) | 2017-11-21 |
| EP3511312A1 (en) | 2019-07-17 |
| KR20140132351A (ko) | 2014-11-17 |
| ES2811226T3 (es) | 2021-03-11 |
| CA2866326A1 (en) | 2013-09-06 |
| CA2866326C (en) | 2020-01-07 |
| US9284241B2 (en) | 2016-03-15 |
| EP3511312B1 (en) | 2020-07-15 |
| PL3511312T3 (pl) | 2020-11-30 |
| WO2013130342A1 (en) | 2013-09-06 |
| EP2819980B1 (en) | 2019-01-23 |
| CN108863713A (zh) | 2018-11-23 |
| ES2711134T3 (es) | 2019-04-30 |
| PL2819980T3 (pl) | 2019-05-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |