MX340839B - Particulas de compuestos de metal de transicion y metodos de produccion. - Google Patents
Particulas de compuestos de metal de transicion y metodos de produccion.Info
- Publication number
- MX340839B MX340839B MX2013007539A MX2013007539A MX340839B MX 340839 B MX340839 B MX 340839B MX 2013007539 A MX2013007539 A MX 2013007539A MX 2013007539 A MX2013007539 A MX 2013007539A MX 340839 B MX340839 B MX 340839B
- Authority
- MX
- Mexico
- Prior art keywords
- transition metal
- particles
- metal compound
- production
- methods
- Prior art date
Links
- 239000011817 metal compound particle Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 150000003623 transition metal compounds Chemical class 0.000 title abstract 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 4
- 239000002245 particle Substances 0.000 abstract 3
- 235000012538 ammonium bicarbonate Nutrition 0.000 abstract 2
- 150000001449 anionic compounds Chemical class 0.000 abstract 2
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 abstract 2
- 229910000357 manganese(II) sulfate Inorganic materials 0.000 abstract 2
- 239000012266 salt solution Substances 0.000 abstract 2
- 235000017550 sodium carbonate Nutrition 0.000 abstract 2
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 2
- 229910052723 transition metal Inorganic materials 0.000 abstract 2
- 150000003624 transition metals Chemical class 0.000 abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 125000000129 anionic group Chemical group 0.000 abstract 1
- 229910052791 calcium Inorganic materials 0.000 abstract 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 abstract 1
- 229910052804 chromium Inorganic materials 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 229910052733 gallium Inorganic materials 0.000 abstract 1
- 229910052732 germanium Inorganic materials 0.000 abstract 1
- 229910052738 indium Inorganic materials 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 229910052748 manganese Inorganic materials 0.000 abstract 1
- 239000011656 manganese carbonate Substances 0.000 abstract 1
- 235000006748 manganese carbonate Nutrition 0.000 abstract 1
- 229910000016 manganese(II) carbonate Inorganic materials 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 229910052698 phosphorus Inorganic materials 0.000 abstract 1
- 238000000527 sonication Methods 0.000 abstract 1
- 229910052712 strontium Inorganic materials 0.000 abstract 1
- 229910052718 tin Inorganic materials 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
- 229910052726 zirconium Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G45/00—Compounds of manganese
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G45/00—Compounds of manganese
- C01G45/006—Compounds containing, besides manganese, two or more other elements, with the exception of oxygen or hydrogen
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/60—Preparation of carbonates or bicarbonates in general
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/006—Compounds containing, besides nickel, two or more other elements, with the exception of oxygen or hydrogen
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/32—Spheres
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/11—Powder tap density
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Catalysts (AREA)
- Compounds Of Iron (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Battery Electrode And Active Subsutance (AREA)
Abstract
Se describe un método para la preparación de partículas de compuestos de metal de transición insolubles que comprende: proveer una sal de metal de transición que tiene la fórmula (TM) (S), en donde el componente de metal de transición TM es uno o más de Mn, Ni, Co, Mg, Zn, Ca, Sr, Cu, Zr, P, Fe, Al, Ga, In, Cr, Ge o Sn; proveer una fuente de compuesto aniónico a base de carbonato-, hidróxido-, fosfato-, oxihidróxido u óxido, en donde el componente aniónico, representado por S´ es reactivo con el componente de metal de transición para formar las partículas; agregar la sal de metal de transición y el compuesto aniónico a una cámara de reacción y someter la cámara a sonificación para formar partículas. En una modalidad ejemplar, la solución de sal de metal de transición comprende MnSO4, la fuente del compuesto aniónico comprende Na2CO3 y/o NH4HCO3, la proporción de MnSO4 a Na2CO3 y/o NH4HCO3 es de alrededor de1:1.5 a 1.5:1. Las partículas formadas que comprenden MnCO3 pueden tener una distribución de tamaño estrecha y una densidad de derivación de alrededor de 1.7 g/ml a alrededor de 2.3 g/ml.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201061428284P | 2010-12-30 | 2010-12-30 | |
| US201161542974P | 2011-10-04 | 2011-10-04 | |
| PCT/CA2011/050780 WO2012088604A1 (en) | 2010-12-30 | 2011-12-16 | Transition metal compound particles and methods of production |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2013007539A MX2013007539A (es) | 2013-12-02 |
| MX340839B true MX340839B (es) | 2016-07-27 |
Family
ID=46382133
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2013007539A MX340839B (es) | 2010-12-30 | 2011-12-16 | Particulas de compuestos de metal de transicion y metodos de produccion. |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US9278867B2 (es) |
| EP (1) | EP2658811B1 (es) |
| JP (1) | JP6151189B2 (es) |
| CN (1) | CN103517878B (es) |
| AU (1) | AU2011350062B2 (es) |
| MX (1) | MX340839B (es) |
| WO (1) | WO2012088604A1 (es) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10149826B2 (en) * | 2015-01-20 | 2018-12-11 | Hyalo Technologies, LLC | Method of preparing microspheres |
| WO2018029715A1 (en) * | 2016-08-09 | 2018-02-15 | Consiglio Nazionale Delle Ricerche | A method and relative apparatus for the production of beer |
| CL2017002221A1 (es) * | 2017-09-01 | 2018-01-19 | Univ Antofagasta | Espinela de manganeso dopada con magnesio, material catódico que la comprende, método de preparación, y batería de ion litio que la comprende |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5321099A (en) * | 1976-08-10 | 1978-02-27 | Agency Of Ind Science & Technol | Fine spherical porovs cobalt ( ) carbonate particles and production thereof |
| US5905003A (en) * | 1995-06-26 | 1999-05-18 | Energy Conversion Devices, Inc. | Beta to gamma phase cycleable electrochemically active nickel hydroxide material |
| US5788943A (en) * | 1996-09-05 | 1998-08-04 | The Hall Chemical Company | Battery-grade nickel hydroxide and method for its preparation |
| GB9828721D0 (en) | 1998-12-24 | 1999-02-17 | Glaxo Group Ltd | Novel apparatus and process |
| JP2002030212A (ja) | 2000-06-29 | 2002-01-31 | Three M Innovative Properties Co | 熱伝導性シート |
| DK1409101T3 (da) | 2001-05-05 | 2006-07-31 | Accentus Plc | Dannelse af små krystaller |
| US6576205B2 (en) * | 2001-09-04 | 2003-06-10 | Inco Limited | Method for reducing the crystallinity of nickel hydroxide powders |
| KR100688732B1 (ko) | 2005-03-30 | 2007-03-02 | 에스케이 주식회사 | 구형 망간탄산화물의 제조방법 및 그 제조물 |
| CN100452488C (zh) * | 2005-10-28 | 2009-01-14 | 比亚迪股份有限公司 | 三元复合锂离子电池正极材料的制备方法 |
| CN101443273B (zh) * | 2006-02-17 | 2014-05-07 | 株式会社Lg化学 | 锂-金属复合氧化物的制备方法 |
| GB0705159D0 (en) | 2007-03-19 | 2007-04-25 | Prosonix Ltd | Process for making crystals |
| DE102007039471A1 (de) * | 2007-08-21 | 2009-02-26 | H.C. Starck Gmbh | Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in Lithium-Sekundärbatterien |
| JP4968944B2 (ja) * | 2008-02-01 | 2012-07-04 | 日本化学工業株式会社 | 複合炭酸塩およびその製造方法 |
| CN101637727B (zh) * | 2008-08-01 | 2011-07-20 | 北京大学 | 过渡金属-磁性氧化铁纳米复合物及其制备方法与应用 |
| JP2010082776A (ja) * | 2008-10-01 | 2010-04-15 | Tohoku Univ | 有機溶媒ソノケミストリーによるナノ粒子合成法 |
| US8618009B2 (en) * | 2008-11-10 | 2013-12-31 | Stc.Unm | Conjugated polyelectrolyte capsules: light activated antimicrobials |
-
2011
- 2011-12-16 US US13/976,623 patent/US9278867B2/en not_active Expired - Fee Related
- 2011-12-16 CN CN201180067760.9A patent/CN103517878B/zh not_active Expired - Fee Related
- 2011-12-16 MX MX2013007539A patent/MX340839B/es active IP Right Grant
- 2011-12-16 JP JP2013546535A patent/JP6151189B2/ja not_active Expired - Fee Related
- 2011-12-16 WO PCT/CA2011/050780 patent/WO2012088604A1/en active Application Filing
- 2011-12-16 AU AU2011350062A patent/AU2011350062B2/en not_active Ceased
- 2011-12-16 EP EP11852395.0A patent/EP2658811B1/en not_active Not-in-force
Also Published As
| Publication number | Publication date |
|---|---|
| EP2658811B1 (en) | 2019-06-12 |
| CN103517878A (zh) | 2014-01-15 |
| EP2658811A4 (en) | 2016-07-13 |
| CN103517878B (zh) | 2017-04-12 |
| MX2013007539A (es) | 2013-12-02 |
| AU2011350062B2 (en) | 2015-09-03 |
| US9278867B2 (en) | 2016-03-08 |
| WO2012088604A1 (en) | 2012-07-05 |
| EP2658811A1 (en) | 2013-11-06 |
| US20130272949A1 (en) | 2013-10-17 |
| AU2011350062A1 (en) | 2013-05-02 |
| JP2014504581A (ja) | 2014-02-24 |
| JP6151189B2 (ja) | 2017-06-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |