MX2024014792A - Formas cristalinas del compuesto fungicida picolinamida - Google Patents

Formas cristalinas del compuesto fungicida picolinamida

Info

Publication number
MX2024014792A
MX2024014792A MX2024014792A MX2024014792A MX2024014792A MX 2024014792 A MX2024014792 A MX 2024014792A MX 2024014792 A MX2024014792 A MX 2024014792A MX 2024014792 A MX2024014792 A MX 2024014792A MX 2024014792 A MX2024014792 A MX 2024014792A
Authority
MX
Mexico
Prior art keywords
compound
organic solvent
mixture
crystalline forms
fungicide compound
Prior art date
Application number
MX2024014792A
Other languages
English (en)
Inventor
Caroline Long
Adriane Miller
Mark P Muehlfeld
Nicola Webb
Xiaowen Zhao
Original Assignee
Corteva Agriscience Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Corteva Agriscience Llc filed Critical Corteva Agriscience Llc
Publication of MX2024014792A publication Critical patent/MX2024014792A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/81—Amides; Imides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0018—Evaporation of components of the mixture to be separated
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0036—Crystallisation on to a bed of product crystals; Seeding

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyridine Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

La presente tecnología se refiere a procesos útiles para preparar (3-acetoxi-4-metoxipicolinoil)-L-alaninato de (S)-1,1-bis(4-fluorofenil)propan-2-ilo Compuesto (I) que comprenden: destilar una mezcla que comprende: un disolvente orgánico aprótico, un disolvente orgánico prótico, el Compuesto (I) y una semilla del Compuesto (I), o que comprenden: destilar una mezcla que comprende: un disolvente orgánico aprótico y el Compuesto (I), y cristalizar el Compuesto (I) creando una segunda mezcla que comprende: un disolvente orgánico prótico, el Compuesto (I) y una semilla del Compuesto (I). Los procesos divulgados en el presente documento describen preparados más estables, compatibles con el almacenamiento del Compuesto (I). También se divulgan preparados del Compuesto (I) que tienen menos impurezas (trazas).
MX2024014792A 2022-05-31 2024-11-28 Formas cristalinas del compuesto fungicida picolinamida MX2024014792A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US202263365532P 2022-05-31 2022-05-31
PCT/US2023/022639 WO2023235153A1 (en) 2022-05-31 2023-05-18 Crystalline forms of picolinamide fungicide compound

Publications (1)

Publication Number Publication Date
MX2024014792A true MX2024014792A (es) 2025-01-09

Family

ID=89025477

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2024014792A MX2024014792A (es) 2022-05-31 2024-11-28 Formas cristalinas del compuesto fungicida picolinamida

Country Status (10)

Country Link
US (1) US20260049058A1 (es)
EP (1) EP4532068A1 (es)
JP (1) JP2025518760A (es)
CN (1) CN119255852A (es)
AU (1) AU2023278798A1 (es)
CA (1) CA3257491A1 (es)
CL (1) CL2024003629A1 (es)
MX (1) MX2024014792A (es)
WO (1) WO2023235153A1 (es)
ZA (1) ZA202408600B (es)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2025151697A1 (en) * 2024-01-12 2025-07-17 Corteva Agriscience Llc Fungicidal sc formulations

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL8105170A (nl) * 1980-12-10 1982-07-01 Thomae Gmbh Dr K Nieuwe fenylalkylaminen, werkwijze ter bereiding daarvan en de toepassing daarvan als geneesmiddelen.
US7834176B2 (en) * 2006-01-26 2010-11-16 Sandoz Ag Polymorph E of Olanzapine and preparation of anhydrous non-solvated crystalline polymorphic Form I of 2-methyl-4(4-methyl-1-piperazinyl)-10H-thieno[2,3-b][1,5] benzodiazepine (Olanzapine Form I) from the polymorphic Olanzapine Form E
WO2008058278A2 (en) * 2006-11-09 2008-05-15 Wyeth POLYMORPHS OF N2-(1, 1' - BIPHENYL - 4 - YLCARBONYL) - N1- [2- (4 - FLUOROPHENYL) -1, 1 - DIMETHYLETHYL]- L - α -GLUTAMINE
US10100060B2 (en) * 2016-06-16 2018-10-16 Xenon Pharmaceuticals Inc. Asymmetric synthesis of funapide
CA3030551C (en) * 2016-07-07 2025-05-06 Corteva Agriscience Llc PROCESSES FOR PREPARATION OF 4-ALCOXY-3-(ACYL OR ALKYL)OXYPICOLINAMIDES
CN113614079A (zh) * 2019-03-15 2021-11-05 日产化学株式会社 杂环酰胺化合物的结晶及其制造方法
MX2021012248A (es) * 2019-04-11 2022-03-11 Mei Pharma Inc Polimorfos de voruciclib y metodos de elaboracion y uso de los mismos.
TWI912287B (zh) * 2020-03-11 2026-01-21 美商富曼西公司 殺真菌劑混合物

Also Published As

Publication number Publication date
ZA202408600B (en) 2026-01-28
EP4532068A1 (en) 2025-04-09
AU2023278798A1 (en) 2024-12-05
CL2024003629A1 (es) 2025-03-14
CN119255852A (zh) 2025-01-03
US20260049058A1 (en) 2026-02-19
CA3257491A1 (en) 2023-12-07
WO2023235153A1 (en) 2023-12-07
JP2025518760A (ja) 2025-06-19

Similar Documents

Publication Publication Date Title
DE69426692T2 (de) Methode zur herstellung von taxan-diterpen und methode zum einten von kulturzellen, die taxan-diterpen in hohen ausbeuten herstellen
MX2024014792A (es) Formas cristalinas del compuesto fungicida picolinamida
MX2023013978A (es) Composicion fungicida que contiene compuestos de oxadiazol.
EP3519396B1 (en) New strigolactone analogs and their usage in plant control
JPWO2021005970A5 (es)
CN108349886B (zh) 新型含杂环氨基酸化合物和其用途
TW200744450A (en) Method of promoting thickening growth of agricultural or horticultural crop
Khodanitska et al. Physiological activity of plant growth stimulators
US10920248B2 (en) Method for mass-producing viniferin using stevioside from cell culture of grapevine tissue
DE3004177A1 (de) Optisch aktive alpha -cyan-3-(4-halogenphenoxy)-benzyl-2-(4-chlorphenyl)-isovalerat-derivate, verfahren zu ihrer herstellung und ihre verwendung
FR2558834A1 (fr) Fongicides a groupes triazole et oligoether
JP2020080682A (ja) 葉物野菜の生産方法
EP0335806A1 (fr) Composés beta-phénoxynitrile
FR2561239A1 (fr) Arylthio-pyridinyl-alcanols
JP7090261B2 (ja) ヤマブシタケ由来新規化合物
EP0555485A1 (en) Antitumor compound nsc-lsc1 and production thereof
MY203688A (en) Bioavailable nitrogen composition and methods
Han et al. Synthesis and bioactivity of novel 3-(1-hydroxyethylidene)-5-substituted-pyrrolidine-2, 4-dione derivatives
EP4674266A3 (en) Penetration enhancer
CN1160327C (zh) 邻-取代苯(烷)硫基苯甲酸植物生长调节剂
CN114249714B (zh) 吡唑胺类化合物及其制备方法和应用
WO2018143140A1 (ja) フシコクシン化合物
CN112079800B (zh) 被取代的烯胺羰基化合物及其制备方法和应用
EP3952651B1 (fr) Utilisation de derives de benzoxepine a titre d'herbicide
KR101093415B1 (ko) 식물세포주를 이용한 비스유제놀 합성 방법