MX2019000662A - Proceso para la fabricacion de granulos que contienen mgda y glda, los granulos y su uso. - Google Patents

Proceso para la fabricacion de granulos que contienen mgda y glda, los granulos y su uso.

Info

Publication number
MX2019000662A
MX2019000662A MX2019000662A MX2019000662A MX2019000662A MX 2019000662 A MX2019000662 A MX 2019000662A MX 2019000662 A MX2019000662 A MX 2019000662A MX 2019000662 A MX2019000662 A MX 2019000662A MX 2019000662 A MX2019000662 A MX 2019000662A
Authority
MX
Mexico
Prior art keywords
granules
glda
mgda
manufacturing
enantiomers
Prior art date
Application number
MX2019000662A
Other languages
English (en)
Inventor
Reinoso Garcia Marta
Sueling Carsten
Klemens MUELLER Michael
Mormul Verena
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2019000662A publication Critical patent/MX2019000662A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047Detergents in the form of bars or tablets
    • C11D17/0065Solid detergents containing builders
    • C11D17/0073Tablets
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/36Racemisation of optical isomers
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
    • C11D11/02Preparation in the form of powder by spray drying
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06Powder; Flakes; Free-flowing mixtures; Sheets
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/26Organic compounds containing nitrogen
    • C11D3/33Amino carboxylic acids
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22Organic compounds
    • C11D7/32Organic compounds containing nitrogen
    • C11D7/3245Aminoacids

Abstract

Un proceso para la fabricación de gránulos de sales de al menos dos ácidos aminopolicarboxílicos (A), que comprende las etapas de (a) proporcionar una solución acuosa de (A1) al menos una sal de metal alcalino de una mezcla de L- y D-enantiómeros del ácido me-tilglicinadiacético (MGDA), donde dicha mezcla contiene predominantemente el L-isómero respectivo con un exceso enantiomérico (ee) en el intervalo de 10 a 95%, (A2) al menos una sal de metal alcalino de L- y D-enantiómeros de ácido glutámico ácido dia-cético (GLDA) o de L-GLDA enantioméricamente puro, la relación en peso de (A1) y (A2) en el intervalo de 1:9 a 9:1, (b) granular por pulverización dicha solución con una temperatura de entrada de gas de al menos 125°C. Adicionalmente, la presente invención se refiere a gránulos y a su uso.
MX2019000662A 2016-07-15 2017-07-05 Proceso para la fabricacion de granulos que contienen mgda y glda, los granulos y su uso. MX2019000662A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP16179707 2016-07-15
PCT/EP2017/066705 WO2018011027A1 (en) 2016-07-15 2017-07-05 Process for manufacturing of mgda and glda containing granules, the granules and their use

Publications (1)

Publication Number Publication Date
MX2019000662A true MX2019000662A (es) 2019-05-20

Family

ID=56511340

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019000662A MX2019000662A (es) 2016-07-15 2017-07-05 Proceso para la fabricacion de granulos que contienen mgda y glda, los granulos y su uso.

Country Status (8)

Country Link
US (1) US10865362B2 (es)
EP (1) EP3484988B1 (es)
JP (1) JP6878564B2 (es)
CN (1) CN109415663A (es)
BR (1) BR112018077082B1 (es)
MX (1) MX2019000662A (es)
RU (1) RU2744632C2 (es)
WO (1) WO2018011027A1 (es)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6773934B2 (ja) * 2017-07-07 2020-10-21 ヌーリオン ケミカルズ インターナショナル ベスローテン フェノーツハップNouryon Chemicals International B.V. メチルグリシン−n,n−二酢酸ナトリウム化合物、これを調製する方法、およびその使用
ES2902628T3 (es) * 2018-02-23 2022-03-29 Unilever Ip Holdings B V Producto de detergente de dosis unitaria con una parte sólida transparente
EP3856881A1 (en) * 2018-09-27 2021-08-04 Basf Se Process for making a granule or powder
WO2020094480A1 (en) 2018-11-07 2020-05-14 Basf Se Process for manufacturing granules, and granules and their use
WO2020127349A1 (en) * 2018-12-21 2020-06-25 Nouryon Chemicals International B.V. Crumbly phase composition of methylglycine n,n diacetic acid
JP2020105440A (ja) 2018-12-28 2020-07-09 株式会社ダイセル 高純度3,4−エポキシシクロヘキシルメチルメタクリレート
EP3822335B1 (en) * 2019-11-15 2022-10-12 Basf Se Cleaning compositions and their use
EP4073217A1 (en) * 2019-12-11 2022-10-19 Basf Se Granules of mgda and (meth)acrylic acid homo- or co-polymer; process for making the same
EP4168388A1 (en) * 2020-06-19 2023-04-26 Nouryon Chemicals International B.V. Process to prepare a co granule of methylglycine n,n diacetic acid salts employing a crumbly phase composition of methylglycine n,n diacetic acid salts
CN112010769B (zh) * 2020-09-01 2023-01-31 河南清水源科技股份有限公司 一种绿色螯合剂甲基甘氨酸二乙酸钠盐的制备方法
CN116761671A (zh) * 2021-03-04 2023-09-15 巴斯夫欧洲公司 制备颗粒状的经涂覆有机盐的方法和颗粒状的经涂覆盐

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5200236A (en) * 1989-11-15 1993-04-06 Lever Brothers Company, Division Of Conopco, Inc. Method for wax encapsulating particles
US5837663A (en) 1996-12-23 1998-11-17 Lever Brothers Company, Division Of Conopco, Inc. Machine dishwashing tablets containing a peracid
DE19819187A1 (de) 1998-04-30 1999-11-11 Henkel Kgaa Festes maschinelles Geschirrspülmittel mit Phosphat und kristallinen schichtförmigen Silikaten
EP3061744B1 (en) 2008-04-01 2018-05-09 Unilever N.V. Preparation of free flowing granules of methylglycine diacetic acid
WO2010139755A1 (en) * 2009-06-05 2010-12-09 Akzo Nobel Chemicals International B.V. Process to prepare a chelating agent or precursor thereof using a cyanide salt
US8802894B2 (en) * 2011-04-04 2014-08-12 Basf Se Process for the preparation of aqueous solutions of methylglycine-N,N-diacetic acid trialkali metal salts
GB2491619B (en) 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation
US8813268B1 (en) * 2011-09-05 2014-08-26 Outdoor Cap Company, Inc. Lighted headwear with recessed light source and lens
US20130284210A1 (en) * 2012-04-25 2013-10-31 Basf Se Solid formulations, their preparation and use
EP3044202B1 (en) * 2013-09-13 2017-08-09 Basf Se Mixtures of enantiomers, and process for making such mixtures
EP3105309B1 (en) 2014-02-13 2019-04-10 Basf Se Powder and granule, process for making such powder and granule, and use thereof

Also Published As

Publication number Publication date
RU2744632C2 (ru) 2021-03-12
EP3484988A1 (en) 2019-05-22
WO2018011027A1 (en) 2018-01-18
RU2019104062A3 (es) 2020-09-23
JP6878564B2 (ja) 2021-05-26
BR112018077082A2 (pt) 2019-04-30
RU2019104062A (ru) 2020-08-17
US10865362B2 (en) 2020-12-15
EP3484988B1 (en) 2020-09-09
CN109415663A (zh) 2019-03-01
JP2019525984A (ja) 2019-09-12
US20200181537A1 (en) 2020-06-11
BR112018077082B1 (pt) 2023-03-28

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