BR112018077082A2 - processos para fabricação de grânulos de sais e de tabletes, grânulo, uso de um grânulo - Google Patents

processos para fabricação de grânulos de sais e de tabletes, grânulo, uso de um grânulo

Info

Publication number
BR112018077082A2
BR112018077082A2 BR112018077082-5A BR112018077082A BR112018077082A2 BR 112018077082 A2 BR112018077082 A2 BR 112018077082A2 BR 112018077082 A BR112018077082 A BR 112018077082A BR 112018077082 A2 BR112018077082 A2 BR 112018077082A2
Authority
BR
Brazil
Prior art keywords
granules
glda
enantiomers
processes
alkali metal
Prior art date
Application number
BR112018077082-5A
Other languages
English (en)
Other versions
BR112018077082B1 (pt
Inventor
Reinoso Garcia Marta
Klemens MUELLER Michael
Sueling Carsten
Mormul Verena
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BR112018077082A2 publication Critical patent/BR112018077082A2/pt
Publication of BR112018077082B1 publication Critical patent/BR112018077082B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0073—Tablets
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/36—Racemisation of optical isomers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/02—Preparation in the form of powder by spray drying
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22—Organic compounds
    • C11D7/32—Organic compounds containing nitrogen
    • C11D7/3245—Aminoacids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Detergent Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

processo para a fabricação de grânulos de sais de pelo menos dois ácidos aminopolicarboxílicos (a), compreendendo as etapas de (a) fornecimento de uma solução aquosa de (a1) pelo menos um sal de metal alcalino de uma mistura de enantiômeros l e d de ácido metil glicina diacético (mgda), contendo a dita mistura predominantemente o respectivo isômero l com um excesso enantiomérico (ee) na faixa de 10 a 95%, (a2) pelo menos um sal de metal alcalino dos enantiômeros l e d de ácido diacético de ácido glutâmico (glda) ou de l-glda enantiomericamente puro, a razão em peso de (a1) e (a2) estando na faixa de 1:9 a 9:1, (b) granulação por aspersão da dita solução com uma temperatura de entrada de gás de pelo menos 125 °c. adicionalmente, a presente invenção refere-se aos grânulos e ao seu uso.
BR112018077082-5A 2016-07-15 2017-07-05 Processo para fabricação de grânulos de sais, grânulo, uso de um grânulo BR112018077082B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP16179707.1 2016-07-15
EP16179707 2016-07-15
PCT/EP2017/066705 WO2018011027A1 (en) 2016-07-15 2017-07-05 Process for manufacturing of mgda and glda containing granules, the granules and their use

Publications (2)

Publication Number Publication Date
BR112018077082A2 true BR112018077082A2 (pt) 2019-04-30
BR112018077082B1 BR112018077082B1 (pt) 2023-03-28

Family

ID=56511340

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112018077082-5A BR112018077082B1 (pt) 2016-07-15 2017-07-05 Processo para fabricação de grânulos de sais, grânulo, uso de um grânulo

Country Status (8)

Country Link
US (1) US10865362B2 (pt)
EP (1) EP3484988B1 (pt)
JP (1) JP6878564B2 (pt)
CN (1) CN109415663A (pt)
BR (1) BR112018077082B1 (pt)
MX (1) MX2019000662A (pt)
RU (1) RU2744632C2 (pt)
WO (1) WO2018011027A1 (pt)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA3069043A1 (en) * 2017-07-07 2019-01-10 Nouryon Chemicals International B.V. Sodium methyl glycine-n,n-diacetic acid compound, process to prepare it and use thereof
US20210040418A1 (en) * 2018-02-23 2021-02-11 Conopco Inc., D/B/A Unilever Detergent solid composition comprising aminopolycarboxylate and inorganic acid
US20210317392A1 (en) * 2018-09-27 2021-10-14 Basf Se Process for making a granule or powder
WO2020094480A1 (en) 2018-11-07 2020-05-14 Basf Se Process for manufacturing granules, and granules and their use
WO2020127349A1 (en) * 2018-12-21 2020-06-25 Nouryon Chemicals International B.V. Crumbly phase composition of methylglycine n,n diacetic acid
JP2020105440A (ja) 2018-12-28 2020-07-09 株式会社ダイセル 高純度３，４−エポキシシクロヘキシルメチルメタクリレート
PL3822335T3 (pl) * 2019-11-15 2023-03-13 Basf Se Kompozycje czyszczące i ich zastosowanie
WO2021115851A1 (en) * 2019-12-11 2021-06-17 Basf Se Granules of mgda and (meth)acrylic acid homo- or co-polymer; process for making the same
EP4168388A1 (en) * 2020-06-19 2023-04-26 Nouryon Chemicals International B.V. Process to prepare a co granule of methylglycine n,n diacetic acid salts employing a crumbly phase composition of methylglycine n,n diacetic acid salts
CN112010769B (zh) * 2020-09-01 2023-01-31 河南清水源科技股份有限公司 一种绿色螯合剂甲基甘氨酸二乙酸钠盐的制备方法
WO2022184551A1 (en) * 2021-03-04 2022-09-09 Basf Se Process for making a particulate coated organic salt, and particulate coated salt

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5200236A (en) * 1989-11-15 1993-04-06 Lever Brothers Company, Division Of Conopco, Inc. Method for wax encapsulating particles
US5837663A (en) 1996-12-23 1998-11-17 Lever Brothers Company, Division Of Conopco, Inc. Machine dishwashing tablets containing a peracid
DE19819187A1 (de) 1998-04-30 1999-11-11 Henkel Kgaa Festes maschinelles Geschirrspülmittel mit Phosphat und kristallinen schichtförmigen Silikaten
BRPI0911375A2 (pt) 2008-04-01 2015-12-29 Unilever Nv processo para a preparação de grânulos de fluxo livre de baixa higroscopicidade, e, usos de grânulos de fluxo livre
US9334232B2 (en) * 2009-06-05 2016-05-10 Akzo Nobel Chemicals International B.V. Process to prepare a chelating agent or precursor thereof using a cyanide salt
US8802894B2 (en) * 2011-04-04 2014-08-12 Basf Se Process for the preparation of aqueous solutions of methylglycine-N,N-diacetic acid trialkali metal salts
GB2491619B (en) 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation
US8813268B1 (en) * 2011-09-05 2014-08-26 Outdoor Cap Company, Inc. Lighted headwear with recessed light source and lens
US20130284210A1 (en) * 2012-04-25 2013-10-31 Basf Se Solid formulations, their preparation and use
KR102360294B1 (ko) 2013-09-13 2022-02-08 바스프 에스이 거울상이성질체의 혼합물, 및 이러한 혼합물의 제조 방법
JP6900193B2 (ja) 2014-02-13 2021-07-07 ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ 粉末及び顆粒、この粉末及び顆粒の製造方法、並びに、その使用方法

Also Published As

Publication number Publication date
RU2744632C2 (ru) 2021-03-12
US20200181537A1 (en) 2020-06-11
EP3484988B1 (en) 2020-09-09
WO2018011027A1 (en) 2018-01-18
RU2019104062A3 (pt) 2020-09-23
BR112018077082B1 (pt) 2023-03-28
RU2019104062A (ru) 2020-08-17
EP3484988A1 (en) 2019-05-22
JP2019525984A (ja) 2019-09-12
JP6878564B2 (ja) 2021-05-26
MX2019000662A (es) 2019-05-20
CN109415663A (zh) 2019-03-01
US10865362B2 (en) 2020-12-15

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Legal Events

Date Code Title Description
B06W Patent application suspended after preliminary examination (for patents with searches from other patent authorities) chapter 6.23 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 05/07/2017, OBSERVADAS AS CONDICOES LEGAIS