MX2018016289A - Polvos y granulos, y proceso para preparar tales polvos y granulos. - Google Patents
Polvos y granulos, y proceso para preparar tales polvos y granulos.Info
- Publication number
- MX2018016289A MX2018016289A MX2018016289A MX2018016289A MX2018016289A MX 2018016289 A MX2018016289 A MX 2018016289A MX 2018016289 A MX2018016289 A MX 2018016289A MX 2018016289 A MX2018016289 A MX 2018016289A MX 2018016289 A MX2018016289 A MX 2018016289A
- Authority
- MX
- Mexico
- Prior art keywords
- spray
- granules
- lumps
- fines
- powder
- Prior art date
Links
- 239000008187 granular material Substances 0.000 title abstract 6
- 239000000843 powder Substances 0.000 title abstract 6
- 238000000034 method Methods 0.000 title abstract 3
- 239000002738 chelating agent Substances 0.000 abstract 4
- 239000002245 particle Substances 0.000 abstract 3
- PQHYOGIRXOKOEJ-UHFFFAOYSA-N 2-(1,2-dicarboxyethylamino)butanedioic acid Chemical compound OC(=O)CC(C(O)=O)NC(C(O)=O)CC(O)=O PQHYOGIRXOKOEJ-UHFFFAOYSA-N 0.000 abstract 2
- CIEZZGWIJBXOTE-UHFFFAOYSA-N 2-[bis(carboxymethyl)amino]propanoic acid Chemical compound OC(=O)C(C)N(CC(O)=O)CC(O)=O CIEZZGWIJBXOTE-UHFFFAOYSA-N 0.000 abstract 2
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Chemical class OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- -1 alkali metal salts Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000004220 glutamic acid Chemical class 0.000 abstract 1
- 235000013922 glutamic acid Nutrition 0.000 abstract 1
- 238000005469 granulation Methods 0.000 abstract 1
- 230000003179 granulation Effects 0.000 abstract 1
- 238000003801 milling Methods 0.000 abstract 1
- 239000002002 slurry Substances 0.000 abstract 1
- 239000007921 spray Substances 0.000 abstract 1
- 238000001694 spray drying Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/44—Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
- C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
- C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/40—Specific cleaning or washing processes
- C11D2111/44—Multi-step processes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Medicinal Preparation (AREA)
- Glanulating (AREA)
Abstract
Proceso para elaborar un polvo o gránulo que contiene al menos un agente quelante seleccionado de sales de metales alcalinos de ácido metilglicindiacetico (MGDA). diacetato de ácido glutámico (GLDA) y ácido iminodisuccinico (IDS), dicho proceso comprende las etapas de (a) introducir una solución acuosa o suspensión acuosa del agente quelante respectivo (A) en un secador por pulverización o granulador por pulverización, y remover la mayor parte de dicha agua mediante secado por pulverización o granulación por pulverización usando un gas con una temperatura de entrada de 125 a 250°C, (b) retirar el polvo o los gránulos, respectivamente, del secador por pulverización o granulador por pulverización, respectivamente, (c) separar los finos de dicho polvo o gránulos, en donde dichos finos tienen un diámetro de partícula máximo de 350 pm, (d) separar los grumos de dicho polvo o gránulos, en donde dichos grumos tienen un diámetro de partícula de 1500 pm o más, (e) moler dichos grumos hasta alcanzar un diámetro de particula máximo de 500 pm, (f) reintroducir dichos finos de la Etapa (c) y los grumos molidos de la Etapa (e) en el secador por pulverización o en el granulador por pulverización, en donde la porción de finos está en el rango de 0.5 a 20% en peso del agente quelante total (A) retirado en la Etapa (b) y la porción de grumos molidos está en el rango de 5 a 60% en peso del agente quelante total (A) retirado en la Etapa (b).
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP16175240 | 2016-06-20 | ||
EP17167683 | 2017-04-24 | ||
PCT/EP2017/063285 WO2017220308A1 (en) | 2016-06-20 | 2017-06-01 | Powders and granules and process for making such powders and granules |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2018016289A true MX2018016289A (es) | 2019-09-16 |
Family
ID=59021485
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2018016289A MX2018016289A (es) | 2016-06-20 | 2017-06-01 | Polvos y granulos, y proceso para preparar tales polvos y granulos. |
Country Status (8)
Country | Link |
---|---|
US (1) | US11028350B2 (es) |
EP (1) | EP3472294B1 (es) |
JP (1) | JP6878471B2 (es) |
CN (1) | CN109415662A (es) |
BR (1) | BR112018075476B1 (es) |
MX (1) | MX2018016289A (es) |
RU (1) | RU2742268C2 (es) |
WO (1) | WO2017220308A1 (es) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2019211170A1 (en) * | 2018-05-04 | 2019-11-07 | Basf Se | Granules or powders and methods for their manufacture |
WO2020064379A1 (en) * | 2018-09-27 | 2020-04-02 | Basf Se | Process for making a granule or powder |
WO2020104231A1 (en) * | 2018-11-19 | 2020-05-28 | Basf Se | Powders and granules containing a chelating agent and an enzyme |
US20220073842A1 (en) | 2018-12-21 | 2022-03-10 | Nouryon Chemicals International B.V. | Crumbly phase composition of methylglycine n,n diacetic acid |
WO2020200836A1 (en) * | 2019-04-01 | 2020-10-08 | Basf Se | Process for making a granule or powder |
EP4263775A1 (en) * | 2020-12-17 | 2023-10-25 | Basf Se | Process for making a solid alkali metal salt of an aminocarboxylate complexing agent |
EP4301504A1 (en) * | 2021-03-04 | 2024-01-10 | Basf Se | Process for making a particulate coated organic salt, and particulate coated salt |
CN117858938A (zh) | 2021-08-25 | 2024-04-09 | 巴斯夫欧洲公司 | 用于制造含有络合剂的粒料或粉末的方法 |
WO2023110611A1 (en) | 2021-12-17 | 2023-06-22 | Basf Se | Process for making granules and powders |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
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ZA739198B (en) | 1972-12-11 | 1975-07-30 | Lilly Co Eli | Herbicidal combinations for soybeans |
CA1101641A (en) * | 1977-06-09 | 1981-05-26 | Anton Niks | Urea granulation |
JPS61153132A (ja) | 1984-12-26 | 1986-07-11 | Mitsui Toatsu Chem Inc | 尿素の造粒方法 |
US5837663A (en) | 1996-12-23 | 1998-11-17 | Lever Brothers Company, Division Of Conopco, Inc. | Machine dishwashing tablets containing a peracid |
NZ331531A (en) | 1997-09-04 | 2000-01-28 | Toyo Engineering Corp | method for granulation and granulator |
DE19819187A1 (de) | 1998-04-30 | 1999-11-11 | Henkel Kgaa | Festes maschinelles Geschirrspülmittel mit Phosphat und kristallinen schichtförmigen Silikaten |
MX2010010779A (es) * | 2008-04-01 | 2010-12-21 | Unilever Nv | Preparacion de granulos que fluyen libres de acido metilglicina diacetico. |
MY153903A (en) * | 2009-05-20 | 2015-04-15 | Basf Se | Method for producing a spray powder containing one or more glycine-n,n-diacetic acid derivatives and use of the spray powder to produce compression agglomerates |
DE102009038951A1 (de) * | 2009-08-26 | 2011-03-03 | Inprotec Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
BR112012006281A2 (pt) * | 2009-09-25 | 2019-09-24 | Novozymes As | "composição detergente de particulado,uso da composição detergente, e ,métodos para preparar uma composição detergente e para remover sujeira contendo ovo de um artigo sujo." |
AU2010305833A1 (en) * | 2009-10-12 | 2012-04-19 | Basf Se | Method for producing a powder containing one or more complexing agent salts |
DE102009060814A1 (de) * | 2009-12-30 | 2011-07-07 | inprotec AG, 79423 | Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält |
KR101897991B1 (ko) * | 2010-09-27 | 2018-09-12 | 바스프 에스이 | 하나 이상의 착화제 염을 포함하는 과립의 제조 방법 |
GB2491619B (en) | 2011-06-09 | 2014-10-01 | Pq Silicas Bv | Builder granules and process for their preparation |
ES2612342T3 (es) | 2012-04-25 | 2017-05-16 | Basf Se | Formulaciones, su uso como o para la preparación de detergentes lavavajillas y su preparación |
US20130284210A1 (en) * | 2012-04-25 | 2013-10-31 | Basf Se | Solid formulations, their preparation and use |
WO2013160132A1 (de) * | 2012-04-25 | 2013-10-31 | Basf Se | Feste formulierungen, ihre herstellung und verwendung |
WO2014090943A1 (en) * | 2012-12-14 | 2014-06-19 | Akzo Nobel Chemicals International B.V. | Crystalline particles of salts of glutamic acid n,n-diacetic acid |
EP2774913B1 (en) * | 2013-03-08 | 2015-09-09 | Basf Se | Process for working up an aqueous solution or slurry of a complexing agent |
PL3105309T3 (pl) | 2014-02-13 | 2019-11-29 | Basf Se | Proszek i granulka, sposób wytwarzania takiego proszku i granulki oraz ich zastosowanie |
JP6426758B2 (ja) | 2014-05-13 | 2018-11-21 | アクゾ ノーベル ケミカルズ インターナショナル ベスローテン フエンノートシャップAkzo Nobel Chemicals International B.V. | キレート剤を結晶化するプロセス |
-
2017
- 2017-06-01 MX MX2018016289A patent/MX2018016289A/es unknown
- 2017-06-01 BR BR112018075476-5A patent/BR112018075476B1/pt active IP Right Grant
- 2017-06-01 WO PCT/EP2017/063285 patent/WO2017220308A1/en unknown
- 2017-06-01 CN CN201780038113.2A patent/CN109415662A/zh active Pending
- 2017-06-01 EP EP17728506.1A patent/EP3472294B1/en active Active
- 2017-06-01 US US16/309,339 patent/US11028350B2/en active Active
- 2017-06-01 JP JP2018566944A patent/JP6878471B2/ja active Active
- 2017-06-01 RU RU2019101363A patent/RU2742268C2/ru active
Also Published As
Publication number | Publication date |
---|---|
JP6878471B2 (ja) | 2021-05-26 |
US20190119611A1 (en) | 2019-04-25 |
US11028350B2 (en) | 2021-06-08 |
EP3472294B1 (en) | 2020-07-22 |
JP2019527741A (ja) | 2019-10-03 |
CN109415662A (zh) | 2019-03-01 |
RU2742268C2 (ru) | 2021-02-04 |
EP3472294A1 (en) | 2019-04-24 |
WO2017220308A1 (en) | 2017-12-28 |
RU2019101363A3 (es) | 2020-09-04 |
BR112018075476A2 (pt) | 2019-03-19 |
BR112018075476B1 (pt) | 2022-10-04 |
RU2019101363A (ru) | 2020-07-23 |
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