MX2015012041A - Metodo para reducir la formacion de compuestos de alto punto de ebullicion durante la deshidrocloracion de 1,1,1,3-tetracloropropa no. - Google Patents
Metodo para reducir la formacion de compuestos de alto punto de ebullicion durante la deshidrocloracion de 1,1,1,3-tetracloropropa no.Info
- Publication number
- MX2015012041A MX2015012041A MX2015012041A MX2015012041A MX2015012041A MX 2015012041 A MX2015012041 A MX 2015012041A MX 2015012041 A MX2015012041 A MX 2015012041A MX 2015012041 A MX2015012041 A MX 2015012041A MX 2015012041 A MX2015012041 A MX 2015012041A
- Authority
- MX
- Mexico
- Prior art keywords
- hcc
- tetrachloropropane
- dehydrochlorination
- formation
- high boiling
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
- C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
- C07C17/275—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/04—Chloro-alkenes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
- C07C17/263—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
- C07C17/269—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions of only halogenated hydrocarbons
Abstract
Esta invención se refiere a un método para mejorar la selectividad de 1,1,3-tricloropropeno (HCC-1240za) y/o 3,3,3-tricloropropeno (HCC-1240zf) en la deshidro-cloración de 1,1,1,3- tetracloropropano (HCC-250fb). En la práctica normal, FeC13 se utiliza como el catalizador para la deshidrocloración de HCC-250fb para producir 1,1,3-tricloro- propeno y/o 3,3,3-tricloropropeno. En la presente invención la mejora comprende, usando como material de partida, una mezcla que comprende HCC-250fb y Heavies generados a partir de la reacción de CCI4 y etileno para producir HCC-250fb, en el que los Heavies comprenden uno o más isómeros tetracloropentano. Estos compuestos reducen o eliminan la formación de compuestos de punto de ebullición altos no deseados (HBC).
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US13/796,328 US8889927B2 (en) | 2013-03-12 | 2013-03-12 | Method to reduce the formation of high boiling compounds during the dehydrochlorination of 1,1,1,3-tetrachloropropane |
PCT/US2014/019794 WO2014164001A1 (en) | 2013-03-12 | 2014-03-03 | Method to reduce the formation of high boiling compounds during the dehydrochlorination of 1,1,1,3- tetrachloropropane |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2015012041A true MX2015012041A (es) | 2015-12-16 |
Family
ID=51530208
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2015012041A MX2015012041A (es) | 2013-03-12 | 2014-03-03 | Metodo para reducir la formacion de compuestos de alto punto de ebullicion durante la deshidrocloracion de 1,1,1,3-tetracloropropa no. |
Country Status (6)
Country | Link |
---|---|
US (1) | US8889927B2 (es) |
EP (1) | EP2970064A4 (es) |
JP (1) | JP2016510814A (es) |
CN (2) | CN105121394B (es) |
MX (1) | MX2015012041A (es) |
WO (1) | WO2014164001A1 (es) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CZ309260B6 (cs) * | 2014-10-16 | 2022-06-29 | Spolek Pro Chemickou A Hutní Výrobu, Akciová Společnost | Způsob přípravy chlorovaného alkenu |
WO2016058569A1 (en) * | 2014-10-16 | 2016-04-21 | Spolek Pro Chemickou A Hutni Vyrobu, Akciova Spolecnost | Process |
CN109311785A (zh) * | 2016-06-23 | 2019-02-05 | 蓝立方知识产权有限责任公司 | 氯代烷烃的脱氯化氢方法 |
CN109809959B (zh) | 2017-11-22 | 2021-10-01 | 江西天宇化工有限公司 | 一种1,1,1,2,3-五氯丙烷的制备方法 |
EP3774701A1 (en) | 2018-04-03 | 2021-02-17 | Blue Cube IP LLC | Method for the production of a halogenated alkene by catalyzed dehydrohalogenation of a halogenated alkane |
WO2020041731A1 (en) | 2018-08-24 | 2020-02-27 | Blue Cube Ip Llc | Gallium catalyzed dehydrochlorination of a chlorinated alkane |
CN111643917B (zh) * | 2020-06-15 | 2021-09-17 | 威海新元化工有限公司 | 一种1,1,3-三氯丙烯的连续生产装置及方法 |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4966613A (es) * | 1972-10-27 | 1974-06-27 | ||
JPS5259103A (en) * | 1975-11-10 | 1977-05-16 | Shin Etsu Chem Co Ltd | Process for preparation of tetrachloroalkane |
US4535194A (en) | 1983-07-06 | 1985-08-13 | Monsanto Co. | Process for producing 1,1,2,3-tetrachloropropene |
US4650914A (en) | 1983-07-06 | 1987-03-17 | Monsanto Company | Process for producing 1,1,2,3-tetrachloropropene |
DE3460965D1 (en) * | 1983-07-06 | 1986-11-20 | Monsanto Co | Process for producing monoadducts of olefins and telogens reactive therewith |
US6534688B2 (en) | 2001-06-11 | 2003-03-18 | Vulcan Chemicals | Dehydrochlorination stabilization of polychlorinated alkanes |
US8258355B2 (en) * | 2007-07-25 | 2012-09-04 | Honeywell International Inc. | Processes for preparing 1,1,2,3-tetrachloropropene |
WO2009085862A1 (en) * | 2007-12-19 | 2009-07-09 | Occidental Chemical Corporation | Methods of making chlorinated hydrocarbons |
JP2010229047A (ja) | 2009-03-26 | 2010-10-14 | Tokuyama Corp | トリクロロプロペンの製造方法 |
US8779222B2 (en) | 2009-08-31 | 2014-07-15 | Sumitomo Chemical Company, Limited | Method for producing 1,1,3-trichloro-1-propene |
JP2011057650A (ja) * | 2009-09-14 | 2011-03-24 | Tokuyama Corp | クロロプロペンの製造方法 |
US8426655B2 (en) * | 2010-03-26 | 2013-04-23 | Honeywell International Inc. | Process for the manufacture of hexafluoro-2-butene |
JP2012097017A (ja) | 2010-11-01 | 2012-05-24 | Tokuyama Corp | クロロプロペンの製造方法 |
US8586804B2 (en) * | 2010-12-01 | 2013-11-19 | E. I. Du Pont De Nemours And Company | Synthesis of 1,1,3-trichloro-1-propene |
CN103119005B (zh) * | 2010-12-16 | 2016-10-26 | 株式会社德山 | 碳数为3的氯化烃的制备方法 |
US9475739B2 (en) | 2011-08-07 | 2016-10-25 | Blue Cube Ip Llc | Process for the production of chlorinated propenes |
-
2013
- 2013-03-12 US US13/796,328 patent/US8889927B2/en active Active
-
2014
- 2014-03-03 MX MX2015012041A patent/MX2015012041A/es unknown
- 2014-03-03 JP JP2016500539A patent/JP2016510814A/ja active Pending
- 2014-03-03 CN CN201480014679.8A patent/CN105121394B/zh active Active
- 2014-03-03 EP EP14778850.9A patent/EP2970064A4/en not_active Withdrawn
- 2014-03-03 WO PCT/US2014/019794 patent/WO2014164001A1/en active Application Filing
- 2014-03-03 CN CN201710356736.6A patent/CN107266286B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN105121394B (zh) | 2017-06-20 |
EP2970064A4 (en) | 2016-09-21 |
CN107266286B (zh) | 2020-09-04 |
CN105121394A (zh) | 2015-12-02 |
US8889927B2 (en) | 2014-11-18 |
WO2014164001A1 (en) | 2014-10-09 |
JP2016510814A (ja) | 2016-04-11 |
US20140275658A1 (en) | 2014-09-18 |
CN107266286A (zh) | 2017-10-20 |
EP2970064A1 (en) | 2016-01-20 |
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