MX2012007298A - Sistemas y metodos para recuperar alcohol y concentrar subproductos de los residuos de destilacion. - Google Patents

Sistemas y metodos para recuperar alcohol y concentrar subproductos de los residuos de destilacion.

Info

Publication number
MX2012007298A
MX2012007298A MX2012007298A MX2012007298A MX2012007298A MX 2012007298 A MX2012007298 A MX 2012007298A MX 2012007298 A MX2012007298 A MX 2012007298A MX 2012007298 A MX2012007298 A MX 2012007298A MX 2012007298 A MX2012007298 A MX 2012007298A
Authority
MX
Mexico
Prior art keywords
concentration
systems
methods
stillage
products
Prior art date
Application number
MX2012007298A
Other languages
English (en)
Inventor
Yihui Tom Xu
Original Assignee
Butamax Tm Advanced Biofuels
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Butamax Tm Advanced Biofuels filed Critical Butamax Tm Advanced Biofuels
Publication of MX2012007298A publication Critical patent/MX2012007298A/es

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/143Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/146Multiple effect distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/26Multiple-effect evaporating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/001Processes specially adapted for distillation or rectification of fermented solutions
    • B01D3/002Processes specially adapted for distillation or rectification of fermented solutions by continuous methods
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/001Processes specially adapted for distillation or rectification of fermented solutions
    • B01D3/003Rectification of spirit
    • B01D3/004Rectification of spirit by continuous methods
    • B01D3/005Combined distillation and rectification
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40Extractive distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00Purification; Separation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12FRECOVERY OF BY-PRODUCTS OF FERMENTED SOLUTIONS; DENATURED ALCOHOL; PREPARATION THEREOF
    • C12F3/00Recovery of by-products
    • C12F3/06Recovery of by-products from beer and wine
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36Azeotropic distillation
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12CBEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C11/00Fermentation processes for beer
    • C12C11/11Post fermentation treatments, e.g. carbonation, or concentration
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • Y02P20/129Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Genetics & Genomics (AREA)
  • General Health & Medical Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Apparatus Associated With Microorganisms And Enzymes (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

La presente invención describe sistemas y métodos para separar un alcohol y, particularmente, butanol, de un suministro fermentado y concentrar los residuos de destilación finos en jarabe, en donde los sistemas y métodos incluyen la operación de una o más columnas de destilación de recuperación de alcohol por medio del uso de calor suministrado por vapor generado a partir de la concentración de los residuos de destilación finos en un sistema de evaporación multiefecto de trenes múltiples.
MX2012007298A 2009-12-21 2010-12-21 Sistemas y metodos para recuperar alcohol y concentrar subproductos de los residuos de destilacion. MX2012007298A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US28843909P 2009-12-21 2009-12-21
PCT/US2010/061512 WO2011084784A1 (en) 2009-12-21 2010-12-21 Systems and methods for alcohol recovery and concentration of stillage by-products

Publications (1)

Publication Number Publication Date
MX2012007298A true MX2012007298A (es) 2012-07-30

Family

ID=44069910

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2012007298A MX2012007298A (es) 2009-12-21 2010-12-21 Sistemas y metodos para recuperar alcohol y concentrar subproductos de los residuos de destilacion.

Country Status (13)

Country Link
US (2) US8906204B2 (es)
EP (1) EP2516030A1 (es)
JP (1) JP2013514815A (es)
KR (1) KR20120108009A (es)
CN (1) CN102665843B (es)
AU (1) AU2010339716A1 (es)
BR (1) BR112012015263A2 (es)
CA (1) CA2782579A1 (es)
MX (1) MX2012007298A (es)
NZ (1) NZ600219A (es)
RU (1) RU2548085C2 (es)
WO (1) WO2011084784A1 (es)
ZA (1) ZA201203854B (es)

Families Citing this family (55)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8778433B2 (en) 2009-05-26 2014-07-15 Fluid Quip, Inc. Methods for producing a high protein corn meal from a whole stillage byproduct
US20110312053A1 (en) 2010-06-18 2011-12-22 Butamax(Tm) Advanced Biofuels Llc Supplementation of fatty acids for improving alcohol productivity
JP2014516581A (ja) 2011-06-17 2014-07-17 ビュータマックス・アドバンスド・バイオフューエルズ・エルエルシー バイオ燃料製造工程からの共産物及びその製造方法
US9254449B2 (en) * 2011-07-28 2016-02-09 Greenfield Specialty Alcohols Inc. Solid and liquid separation process
JP2015501643A (ja) 2011-12-09 2015-01-19 ビュータマックス・アドバンスド・バイオフューエルズ・エルエルシー 発酵ブロスから生成物アルコールを取り出す方法
WO2013102084A2 (en) 2011-12-30 2013-07-04 Butamax (Tm) Advanced Biofuels Llc Fermentative production of alcohols
WO2013166458A1 (en) 2012-05-04 2013-11-07 Butamax (Tm) Advanced Biofuels Llc Processes and systems for alcohol production and recovery
US9605281B2 (en) 2012-09-12 2017-03-28 Butamax Advanced Biofuels Llc Processes and systems for the fermentative production of alcohols
US20140024064A1 (en) 2012-07-23 2014-01-23 Butamax(Tm) Advanced Biofuels Llc Processes and systems for the production of fermentative alcohols
WO2014018837A1 (en) 2012-07-26 2014-01-30 Cheng Cecilia Butanol purification
US9109196B2 (en) 2012-09-12 2015-08-18 Butamax Advanced Biofuels Llc Processes and systems for the production of fermentation products
CN104919050A (zh) 2012-09-12 2015-09-16 布特马斯先进生物燃料有限责任公司 用于生产发酵产物的工艺和系统
US9249076B2 (en) 2012-09-21 2016-02-02 Butamax Advanced Biofuels Llc Recyclable extractant compositions
CA2884876A1 (en) 2012-09-28 2014-04-03 Butamax Advanced Biofuels Llc Production of fermentation products
AU2013329024A1 (en) 2012-10-11 2015-03-12 Butamax Advanced Biofuels Llc Processes and systems for the production of fermentation products
WO2014105840A1 (en) 2012-12-31 2014-07-03 Butamax Advanced Biofuels Llc Fermentative production of alcohols
US9523104B2 (en) 2013-03-12 2016-12-20 Butamax Advanced Biofuels Llc Processes and systems for the production of alcohols
BR112015020685A2 (pt) 2013-03-15 2017-07-18 Butamax Advanced Biofuels Llc método para a recuperação do butanol, composição, métodos para a extração de álcool e de secagem
US9517985B2 (en) 2013-03-15 2016-12-13 Butamax Advanced Biofuels Llc Method for producing butanol using extractive fermentation
US20150087040A1 (en) * 2013-09-26 2015-03-26 E I Du Pont De Nemours And Company Production of ethanol and recycle water in a cellulosic fermentation process
US9120834B2 (en) * 2013-10-31 2015-09-01 Cms Technologies Holdings, Inc. Membrane separation of ionic liquid solutions
US8722924B1 (en) 2013-11-01 2014-05-13 WB Technologies LLC Integrated ethanol and biodiesel facility
US10221387B2 (en) 2013-11-01 2019-03-05 Rayeman Elements, Inc. Integrated ethanol and biodiesel facility
US10494597B2 (en) 2014-04-11 2019-12-03 Butamax Advanced Biofuels Llc Contamination mitigation
CN104001338B (zh) * 2014-05-13 2018-02-02 上海金力泰化工股份有限公司 一种脱溶剂系统及其操作工艺
US11427839B2 (en) 2014-08-29 2022-08-30 Lee Tech Llc Yeast stage tank incorporated fermentation system and method
US11680278B2 (en) 2014-08-29 2023-06-20 Lee Tech Llc Yeast stage tank incorporated fermentation system and method
US20160244788A1 (en) 2015-02-19 2016-08-25 Api Intellectual Property Holdings, Llc Hydrothermal-mechanical conversion of lignocellulosic biomass to ethanol or other fermentation products
EP3115353A1 (en) * 2015-07-10 2017-01-11 GFBiochemicals Ltd. Process for the isolation of levulinic acid
JP2018532416A (ja) * 2015-07-20 2018-11-08 バックマン ラボラトリーズ インターナショナル,インコーポレイティド 測定、制御、及び自動化を乾燥トウモロコシ粉砕エタノール製造プロセスに適用してエタノール及び副生成物の回収率を最大化する方法
US10486079B1 (en) 2016-01-08 2019-11-26 Whitefox Technologies Limited Process and system for dehydrating a byproduct stream in ethanol production
EP3445864A4 (en) * 2016-04-20 2019-12-25 BioProcess Algae LLC METHOD AND SYSTEM FOR SLURGE FERMENTATION
GB2552297B (en) * 2016-06-15 2020-01-08 Russell Distillers Ltd Liquid treatment apparatus, distillation apparatus, and method of distillation
US11166478B2 (en) 2016-06-20 2021-11-09 Lee Tech Llc Method of making animal feeds from whole stillage
US10267511B2 (en) 2016-07-15 2019-04-23 Bioleap, Inc. Advanced flash exhaust heat recovery
US10618871B2 (en) * 2016-08-17 2020-04-14 Covestro Deutschland Ag Process for producing isocyanate and at least one further chemical product in an integrated production
US10729987B1 (en) 2016-12-09 2020-08-04 Whitefox Technologies Limited Process and system for heat integration in ethanol production
SG11201905673RA (en) 2017-03-20 2019-10-30 Lanzatech Inc A process and system for product recovery and cell recycle
US11117071B2 (en) * 2017-03-29 2021-09-14 LucasE3, L.C. Expanded distillation for ethanol production
US10118107B1 (en) 2017-11-07 2018-11-06 Fluid Quip Process Technologies, Llc Method and system for distilling alcohol in an alcohol production process
US10926267B2 (en) 2017-11-27 2021-02-23 Fluid Quip Technologies, Llc Method and system for reducing the unfermentable solids content in a protein portion at the back end of a corn dry milling process
US11376521B2 (en) 2018-01-29 2022-07-05 LucasE3, L.C. Efficient distillation of ethanol
US11339107B2 (en) 2018-01-29 2022-05-24 LucasE3, L.C. Efficient distillation of ethanol
US10865370B1 (en) * 2018-03-28 2020-12-15 Bioleap, Inc. Cook water preheat using evaporator vapor heat recovery
WO2019215506A1 (en) * 2018-05-07 2019-11-14 Whitefox Technologies Limited Process and system for dehydrating a product stream in ethanol production with molecular sieve and membranes
US10875889B2 (en) 2018-12-28 2020-12-29 Fluid Quip Technologies, Llc Method and system for producing a zein protein product from a whole stillage byproduct produced in a corn dry-milling process
US10392590B1 (en) 2019-01-07 2019-08-27 Fluid Quip Process Technologies, Llc Method and system for distilling alcohol in an alcohol production process
CA3129223C (en) 2019-02-08 2023-07-11 Lanzatech, Inc. Process for recovering close boiling products
US11541326B2 (en) 2019-04-05 2023-01-03 LucasE3, L.C. Regenerative vapor energy recovery system and method
US11186851B2 (en) 2019-04-05 2021-11-30 LucasE3, L.C. Continuous ethanol recovery from fermentation with high solids corn slurry production
US11628378B2 (en) 2020-05-12 2023-04-18 Icm, Inc. Distillation vacuum technology
BR102020011147A2 (pt) * 2020-06-03 2021-12-14 Planetcare Soluções Ambientais Ltda - Me Processo e equipamento concentrador de vinhaça e vinho
BR112023014736A2 (pt) 2021-01-22 2023-12-12 Lee Tech Llc Sistema e método para aperfeiçoamento do processo de moagem úmida e moagem a seco do milho
US12005381B2 (en) 2021-10-15 2024-06-11 Whitefox Technologies Limited Heat integrated process and system for ethanol production using vapor recompression
KR20230157645A (ko) * 2022-05-10 2023-11-17 한화솔루션 주식회사 1,4-사이클로헥산디메탄올 조성물의 정제 방법

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR768994A (fr) 1934-02-23 1934-08-17 Francois Duriez & Compagine Installation d'appareils pour la concentration des vinasses de distillerie de betteraves combinés pour l'utilisation des vapeurs à la distillerie
US2126974A (en) * 1936-11-03 1938-08-16 Gustave T Reich Recovery of products of fermentation
SE365008B (es) 1971-11-19 1974-03-11 Mo Och Domsjoe Ab
SU721483A1 (ru) * 1978-09-13 1980-03-15 Всесоюзный Научно-Исследовательский Институт Продуктов Брожения Способ производства спирта из крахмалсодержащего сырь
US4309254A (en) 1980-04-17 1982-01-05 Stone And Webster Eng. Corp. Alcohol recovery process
SU996437A1 (ru) * 1981-08-04 1983-02-15 Всесоюзный Научно-Исследовательский Институт Продуктов Брожения Способ производства спирта
US4865973A (en) * 1985-09-13 1989-09-12 Queen's University At Kingston Process for extractive fermentation
US7297236B1 (en) 2001-06-30 2007-11-20 Icm, Inc. Ethanol distillation process
US7867365B2 (en) 2003-03-28 2011-01-11 Thermal Kinetics Systems, Llc Ethanol distillation with distillers soluble solids recovery apparatus
EP1869197A2 (en) 2005-04-12 2007-12-26 E.I. Dupont De Nemours And Company Treatment of biomass to obtain ethanol
BRPI0600553A (pt) * 2006-02-24 2007-11-20 Siemens Ltda processo e sistema para a produção de álcool por destilação de múltiplo efeito
US8425734B2 (en) * 2007-07-02 2013-04-23 I3 Nanotec Llc Membrane-based hybrid process for separation of mixtures of organics, solids, and water
CA2706767A1 (en) 2007-12-14 2009-06-25 William D. Parten Method for controlling butanol concentration in fermentation broth
BRPI0821519A2 (pt) * 2007-12-27 2015-06-16 Gevo Inc Recuperação de alcoois superiores a partir de soluções aquosas diluída
WO2009149270A2 (en) 2008-06-04 2009-12-10 E. I. Du Pont De Nemours And Company A method for producing butanol using two-phase extractive fermentation
CN102439162A (zh) 2009-04-13 2012-05-02 布特马斯先进生物燃料有限责任公司 利用萃取发酵生产丁醇的方法
US8968523B2 (en) 2009-07-15 2015-03-03 Butamax Advanced Biofuels Llc Recovery of butanol isomers from a mixture of butanol isomers, water, and an organic extractant

Also Published As

Publication number Publication date
AU2010339716A1 (en) 2012-06-14
WO2011084784A1 (en) 2011-07-14
US8906204B2 (en) 2014-12-09
CN102665843A (zh) 2012-09-12
JP2013514815A (ja) 2013-05-02
KR20120108009A (ko) 2012-10-04
EP2516030A1 (en) 2012-10-31
BR112012015263A2 (pt) 2016-03-15
US20150060259A1 (en) 2015-03-05
CN102665843B (zh) 2015-09-23
RU2548085C2 (ru) 2015-04-10
CA2782579A1 (en) 2011-07-14
US20110315541A1 (en) 2011-12-29
RU2012130949A (ru) 2014-01-27
ZA201203854B (en) 2013-08-28
NZ600219A (en) 2014-07-25

Similar Documents

Publication Publication Date Title
MX2012007298A (es) Sistemas y metodos para recuperar alcohol y concentrar subproductos de los residuos de destilacion.
MY173771A (en) A method for producing a target substance by fermentation
GB201213579D0 (en) Desalination system and method for desalination
MY181137A (en) Process and systems for obtaining 1,4-butanediol from fermentation broths
MY152034A (en) Method for purifying an alcohol from a fermentation broth using a falling film, a wiped film, a thin film or a short path evaporator
MX338976B (es) Procesos de separacion por osmosis directa.
WO2012102896A3 (en) Processes and systems for enzymatically isolating lignin and other bioproducts from herbaceous plants
UA95936C2 (ru) Способ выделения бетаина
WO2011059751A3 (en) Forward osmosis separation processes
WO2010009240A3 (en) Cooling and processing materials
MX2008015571A (es) Metodo de destilado de columna de etapa multiple (mscd) para recuperacion de una sustancia disuelta osmotica.
MX365785B (es) Metodo para la purificacion de acidos carboxilicos a partir de los caldos de fermentacion.
BRPI0823256B8 (pt) uso de sacarose como substrato para produção fermentativa de 1,2-propanodiol
WO2010017230A3 (en) Methods, systems and compositions related to microbial bio-production of butanol and/or isobutanol
MY172577A (en) Method for producing alcohol from cellulose-containing biomass
WO2012141546A3 (ko) 미생물 발효를 통해 제조된 생성물을 흡착제를 이용하여 분리 정제하는 장치 및 방법
CO7170120A2 (es) Un sistema y un método para la producción integrada de etanol de primera y segunda generación, y uso de puntos de integración para dicha producción
CL2012003133A1 (es) Proceso para la recuperacion de betaina a partir de una melaza, que comprende someter melaza a la seccion de una enzima formadora de fructano y separar cromatograficante una fraccion que contiene betaina; y producto de melaza de remolacha azucacrera modificada.
WO2012008809A3 (ko) L-오르니틴 생산능이 향상된 미생물 및 이를 이용한 l-오르니틴 생산방법
PH12018500512A1 (en) Process for potash recovery from biomethanated spent wash with concomitant environmental remediation of effluent
MY187692A (en) Distillation system for reducing energy consumption by thermal coupling
TW200745000A (en) Azeotropic distillation method
FR3024044B1 (fr) Procede d'extraction de molecules produites par fermentation anaerobie a partir de biomasse fermentescible
WO2009005010A1 (ja) バイオマスエタノール製造方法
TH133893A (th) ชุดเครื่องและวิธีการสำหรับการแยก และการทำให้บริสุทธิ์แก่ผลิตภัณฑ์ซึ่งถูกผลิตขึ้นโดยการหมักจุลชีพโดยการใช้ตัวดูดซับ

Legal Events

Date Code Title Description
FA Abandonment or withdrawal