KR950003774A - 저순도 산소 제조용 저온 정류 시스템 - Google Patents

저순도 산소 제조용 저온 정류 시스템 Download PDF

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KR950003774A
KR950003774A KR1019940017618A KR19940017618A KR950003774A KR 950003774 A KR950003774 A KR 950003774A KR 1019940017618 A KR1019940017618 A KR 1019940017618A KR 19940017618 A KR19940017618 A KR 19940017618A KR 950003774 A KR950003774 A KR 950003774A
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column
passing
low temperature
purity oxygen
air stream
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KR100225681B1 (ko
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마크 프로쎄어 네일
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조안 엠. 젤사
프랙스에어 테크놀로지, 인코포레이티드
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187—Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/04193—Division of the main heat exchange line in consecutive sections having different functions
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
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    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/0409—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of oxygen
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    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/04103—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression using solely hydrostatic liquid head
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    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04163—Hot end purification of the feed air
    • F25J3/04169—Hot end purification of the feed air by adsorption of the impurities
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    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187—Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/04193—Division of the main heat exchange line in consecutive sections having different functions
    • F25J3/04206—Division of the main heat exchange line in consecutive sections having different functions including a so-called "auxiliary vaporiser" for vaporising and producing a gaseous product
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    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/0429—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of feed air, e.g. used as waste or product air or expanded into an auxiliary column
    • F25J3/04303—Lachmann expansion, i.e. expanded into oxygen producing or low pressure column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
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    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04406—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
    • F25J3/04424—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system without thermally coupled high and low pressure columns, i.e. a so-called split columns
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
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    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/90—Details relating to column internals, e.g. structured packing, gas or liquid distribution
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/02—Processes or apparatus using other separation and/or other processing means using simple phase separation in a vessel or drum
    • F25J2205/04—Processes or apparatus using other separation and/or other processing means using simple phase separation in a vessel or drum in the feed line, i.e. upstream of the fractionation step
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/60—Processes or apparatus using other separation and/or other processing means using adsorption on solid adsorbents, e.g. by temperature-swing adsorption [TSA] at the hot or cold end
    • F25J2205/62—Purifying more than one feed stream in multiple adsorption vessels, e.g. for two feed streams at different pressures
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
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    • F25J2215/00—Processes characterised by the type or other details of the product stream
    • F25J2215/50—Oxygen or special cases, e.g. isotope-mixtures or low purity O2
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    • F25J2250/00—Details related to the use of reboiler-condensers
    • F25J2250/30—External or auxiliary boiler-condenser in general, e.g. without a specified fluid or one fluid is not a primary air component or an intermediate fluid
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    • F25J2250/00—Details related to the use of reboiler-condensers
    • F25J2250/30—External or auxiliary boiler-condenser in general, e.g. without a specified fluid or one fluid is not a primary air component or an intermediate fluid
    • F25J2250/50—One fluid being oxygen

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Abstract

고압 공급공기 스트림이 저압 컬럼의 하단을 리보일하는데 사용되고, 저압공급 공기 스트림이 고압 컬럼으로 직접 공급되는 것을 특징으로 하는 저온 정류시스템이 기재되어 있다.

Description

저순도 산소 제조용 저온 정류 시스템
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제 1 도는 저순도 산소 액체가 고압으로 펌프되고 주열교환기내에서 증발되는 본 발명의 바람직한 일 실시예를 나타내는 개략적인 도면, 제 2 도는 저순도 산소액체가 고압으로 펌프되고 생성물 보일러내에서 증발되는 본 발명의 다른 바람직한 실시예를 나타내는 개략적인 도면, 제 3 도는 저순도 산소 증기가 저압 컬럼으로부터 배출되고 회수되는 본 발명의 또 다른 바람직한 실시예를 나타내는 개략적인 도면, 제 4 도는 공급 스트림이 냉각을 위한 터보팽창에 앞서 더 앞축되는 본 발명의 또 다른 바람직한 실시예를 나타내는 개략적인 도면이다.

Claims (10)

  1. (A) 상단에 켄덴서가 있는 제 1 컬럼과 하단에 리보일러가 있는 제 2 컬럼을 포함하며, 제 1 컬럼의 압력이 제 2 컬럼의 압력을 초과하는 압력에서 조작되는 저온 정류 플랜트를 제공하는 단계 : (B)39 내지 100psia의 압력범위에서 제 1공급공기 스트림을 제공하고,공급 공기 스트림을 바닥 리보일러로 통과시키는 단계, (C)공급공기를 바닥 리보일러에서 제 1 및 제 2 컬럼중 적어도 하나로 통과시키는 단계 : (D)제 1 공급 공기 스트림의 압력보다 더 낮은 압력으로 제 2 공급 공기 스트림을 제공하고, 제 2 공급 공기스트림을 제 1 컬럼으로 통과시키는 단계 : (E) 제 2컬럼으로부터 저순도의 산소를 배출하고 배출된 저순도 산소를 제 1 공급공기 스트림 및 제 2 공급 공기스트림과 간접 열교환시켜 가온시키는 단계 : (F)생성물로서 생성되는 가온 저순도 산소를 회수하는 단계를 포함하는 저순도 산소 제조를 위한 저온 정류방법.
  2. 제 1 항에 있어서, 저순도 산소가 액체로서 제 2 컬럼으로부터 배출되고, 압력이 증가하며, 회수전에 증발되는 것을 특징으로 하는 저온 정류방법.
  3. 제 1 항에 있어서, 저순도 산소가 증기로서 제 2 컬럼으로부터 배출되고 액체로서 제 2 컬럼으로부터 부가적인 저순도 산소를 배출하는 단계와 부가적인 저순도 산소 생성물로서 상기 배출된 액체를 회수하는 단계를 더 포함하는 것을 특징으로하는 저온 정류방법.
  4. 제 1 항에 있어서, 제 1 컬럼에서 질소가 풍부한 증기 및 산소가 풍부한 액체를 생성하는 단계, 상단 컨덴서에서 산소가 풍부한 액체와 간접 열교환에 의해 질소가 풍부한 증기를 응축하는 단계, 및 제 1 및 제 2 컬럼 중 적어도 하나에서 환류로서 응축된 질소가 풍부한 유체를 적용하는 단계를 더 포함하는 것을 특징으로 하는 저온 정류 방법.
  5. 제 1 항에 있어서, 제 1 공급 공기스트럼을 초과하는 압력을 가지고, 제 2 컬럼으로부터 배출된 액체 저순도 산소와 간접 열교환되면서 부가적인 공급 공기스트림을 통과시키는 단계를 더 포함하는 것을 특징으로하는 저온 정류방법.
  6. 제 1 항에 있어서, 95몰%를 초과하는 질소농도를 가지는 저온 정류 플랜트로부터 질소함유 유체를 회수하는 단계를 더 포함하는 것을 특징으로 하는 저온 정류방법.
  7. (A)상단에 컨덴서가 있는 제 1 컬럼 및 하단에 리보일러가 있는 제 2 컬럼; (B)주 열교환기 및 제 1 공급스트림을 주열교환기로 통과시키고 주열교환기에서 하단의 리보일러로 통과시키는 수단 ; (C)하단 리보일러로 부터 제 1 및 제 2 컬럼 중 적어도 하나로 유체를 통과시키는 수단 ; (D)제 1 공급스트림보다 더 낮은 압력에서도 제 2 공급스트림을 주열교환기로 주열교환기에서 제 1 컬럼으로 통과시키는 수단 ; (E)제 2 컬럼에서 주열교환기로 생성유체를 통과시키는 수단 ; (F)주열교환기에서 생성유체를 회수하는 수단을 포함하는 저순도 산소제조를 위한 저온 정류장치.
  8. 제 7 항에 있어서, 제 2 컬럼에서 주열교환기로 생성유체를 통과시키는 수단이 액체펌프를 포함하는 것을 특징으로 하는 저온 정류장치
  9. 제 7 항에 있어서, 제 1 컬럼의 상단에서 상단 응축기로 유체를 통과시키는 수단, 제 1 컬럼의 하부에서 상단 컨덴서로 유체를 통과시키는 수단 및 상단 컨덴서로부터 유체를 제 1 및 제 2 컬럼 중 적어도 하나로 통과시키는 수단을 더 포함하는 것을 특징으로 하는 저온 정류장치.
  10. 제 7 항에 있어서, 주열교환기로 부가적인 공급스트림을 주열교환기로, 주 열교환기에서 제 2 컬럼으로 통과시키는 수단을 더 포함하는 것을 특징으로 하는 저온 정류 장치.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019940017618A 1993-07-22 1994-07-21 저순도 산소 제조용 저온 정류 시스템 KR100225681B1 (ko)

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ES2107720T3 (es) 1997-12-01
KR100225681B1 (ko) 1999-10-15
EP0635690A1 (en) 1995-01-25
CA2128582A1 (en) 1995-01-23
BR9402897A (pt) 1995-04-11
DE69405829T2 (de) 1998-04-09
CA2128582C (en) 1998-08-25
CN1089427C (zh) 2002-08-21
DE69405829D1 (de) 1997-10-30
JPH07305953A (ja) 1995-11-21
CN1102473A (zh) 1995-05-10
EP0635690B1 (en) 1997-09-24

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