KR930701145A - 박편(薄片) 형상 미분말 및 그 제조방법 및 화장료(化粧料) - Google Patents
박편(薄片) 형상 미분말 및 그 제조방법 및 화장료(化粧料)Info
- Publication number
- KR930701145A KR930701145A KR1019920703247A KR920703247A KR930701145A KR 930701145 A KR930701145 A KR 930701145A KR 1019920703247 A KR1019920703247 A KR 1019920703247A KR 920703247 A KR920703247 A KR 920703247A KR 930701145 A KR930701145 A KR 930701145A
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- KR
- South Korea
- Prior art keywords
- ppm
- flake
- alkoxysilane
- fine powder
- silica
- Prior art date
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/0254—Platelets; Flakes
- A61K8/0258—Layered structure
- A61K8/0262—Characterized by the central layer
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/40—Compounds of aluminium
- C09C1/405—Compounds of aluminium containing combined silica, e.g. mica
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/06—Treatment with inorganic compounds
- C09C3/063—Coating
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/436—Interference pigments, e.g. Iridescent, Pearlescent
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/60—Particulates further characterized by their structure or composition
- A61K2800/61—Surface treated
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/54—Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
- C01P2004/82—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases
- C01P2004/84—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases one phase coated with the other
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/20—Powder free flowing behaviour
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/42—Magnetic properties
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
- C09C2200/10—Interference pigments characterized by the core material
- C09C2200/102—Interference pigments characterized by the core material the core consisting of glass or silicate material like mica or clays, e.g. kaolin
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
- C09C2200/50—Interference pigments comprising a layer or a core consisting of or comprising discrete particles, e.g. nanometric or submicrometer-sized particles
- C09C2200/505—Inorganic particles, e.g. oxides, nitrides or carbides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C2220/00—Methods of preparing the interference pigments
- C09C2220/10—Wet methods, e.g. co-precipitation
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- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
- Silicon Compounds (AREA)
Abstract
가질로서의 박편형상물징의 표면에 구형상의 입자를 피복함으로써, 그 표면의 광의 난반사에 의한 기질의 광택도의 억제, 미끄럼성의 향상 등을 도모함을 목적으로 한다.
박편형상 미분말은, 천연운모 등의 박편형상물질의 표면에 실리카입자가 담지되거나, 또는 그 실리카입자 그 위에 알콕시실란의 가수분해물 또는 실리카겔로 고정화되어 이루어지는 것이다.
박편형상미분말은, 박편형상물질과 실리카입자를 함유하는 분산액중에, 알콕시실란을 첨가하여 가수분해하거나, 또는, 규산액을 첨가하여, 이것을 겔화하여 제조한다. 이 박편형상 미분말을 각종 성분과 함께 배합하여 화장료로서 이용할 수가 있다.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 횡축에 유전률(誘電率)(ε)(-)을 취하고, 종축에 이온농도 (N)(ppm)를 취하며, 박편형상 물질에 실리카입자를 부착할 때의 분산액의 바람직한 영역을 도시한 것이다.
제2도 및 제3도는, 실시예1 및 실시예21에 의하여 각각 얻어진 박편형상 미분말 표면의 입자구조를 나타낸 사진이며,
제4도 및 제5도는 실시예 1과 실시예21의 박편형상 미분말을 고착강도 테스트에 제공한 후의 각각의 표면의 입자구조를 나타낸 사진이다.
Claims (15)
- 박편형상물질과 살리카입자를 함유하는 분산액중에, 알콕시실란 및/또는 규산액을 첨가하여, 이 알콕시실린을 가수분해하고, 및/또는 규산액을 겔화하여 상기 실리카입자를 상기 박편형상물질의 표면에 고정화하는 것을 특징으로 하는 박편형상 미분말의 제조방법.
- 제1항에 있어서, 분산액의 유전률(ε)이, 15≤ε≤80의 범위에 있고, 더구나, 분산액중의 카티온과 아니온의 함께 이온농도(N)가,
- ① ε=15일 때, 200ppm ! N≤5X104ppm
- ② ε=80일 때, 3X104ppm ! N≤2X105ppm
- ③ 15<ε=80일 때, 유전률(ε)(-)을 X축, 이온농도(N)(ppm)를 Y축으로 취하여 나타낸 (X, Y)좌표에 있어서, A(15, 200), B(15, 5X104), C(80, 2X105)에 의해 형성되는 사변형 영역내에 있는 것을 특징으로 하는 박편형상 미분말의 제조방법.
- 유기용매 및/또는 물로 이루어지는 분산매에, 박편형상물질과 구형상의 실리카입자를 분산시켜서, 이 박편형성물질의 표면에 이 실리카입자를 부착시키고, 이어서, 이 분산액 중에 알콕시실란 및/또는 규산액을 첨가하여, 이 알콕시실란을 가수분해하고, 및/또는 규산액을 겔화하여 상기 실리카입자를 상기 박편형상물질의 표면에 고정화하는 것을 특징으로 하는 박편형상 미분말의 제조방법.
- 제3항에 있어서, 분산액의 유전률(ε)이, 15≤ε≤80의 범위에 있고, 분산액증의 카티온과 아니온의 함께 이온농도(N)가,
- ① ε=15일 때, 200ppm ! N≤5X104ppm
- ② ε=80일 때, 3X104ppm ! N≤2X105ppm
- ③ 15<ε=80일 때, 유전률(ε)(-)을 X축, 이온농도(N)(ppm)를 Y축으로 취하여 나타낸 (X, Y)좌표에 있어서, A(15, 200), B(15, 5X104), C(80, 2X105) 및 C(80, 3X104)에 의해 형성되는 사변형 영역내에 있는 것을 특징으로 하는 박편형상 미분말의 제조방법.
- 내용 없음
- 제5항에 있어서, 박편형상물질의 표면에 실리카입자가 알콕시실란의 가수분해물 및/또는 실리카겔로 고정회되어 이루어지는 박편형상 미분말.
- 박편형상물질의 표면에 구형상의 실리카입자가 피복된 박편형상 미분말의 배합되어 이루어진 화장료.
- 제7항에 있어서, 박편형상물질의 표면에 실리카 입자가 알콕시실란의 가수분해물 및/또는 실리카겔로 고정된 박편형사 미분말이 배합되어 이루어진 이루어진 화장료.
- ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP90-216403 | 1990-08-16 | ||
JP21640390 | 1990-08-16 | ||
PCT/JP1991/001087 WO1992003119A1 (en) | 1990-08-16 | 1991-08-15 | Flaky fine powder, production thereof, and cosmetic |
Publications (2)
Publication Number | Publication Date |
---|---|
KR930701145A true KR930701145A (ko) | 1993-06-11 |
KR0145423B1 KR0145423B1 (ko) | 1998-07-15 |
Family
ID=16688019
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019920703247A KR0145423B1 (ko) | 1990-08-16 | 1991-08-15 | 박편형상 미분말 및 그 제조방법 및 화장료 |
Country Status (7)
Country | Link |
---|---|
EP (1) | EP0543999B1 (ko) |
JP (1) | JP2784261B2 (ko) |
KR (1) | KR0145423B1 (ko) |
AT (1) | ATE171974T1 (ko) |
DE (1) | DE69130322D1 (ko) |
SG (1) | SG49806A1 (ko) |
WO (1) | WO1992003119A1 (ko) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE60014273T2 (de) | 1999-07-29 | 2005-10-06 | Merck Patent Gmbh | Feine schuppenförmige Pigmente und deren Herstellungsverfahren |
US6511672B2 (en) * | 2001-01-17 | 2003-01-28 | Color Access, Inc. | Compositions containing optical diffusing pigments |
JP4824183B2 (ja) * | 2001-02-28 | 2011-11-30 | 株式会社コーセー | 固形粉末化粧料 |
AU2003248263A1 (en) * | 2002-07-11 | 2004-02-02 | Catalysts And Chmicals Industries Co., Ltd. | Cosmetic |
JP4095920B2 (ja) * | 2003-03-31 | 2008-06-04 | 株式会社資生堂 | 複合粉末、それを配合した化粧料、及び複合粉末の製造方法 |
JP2009114100A (ja) * | 2007-11-05 | 2009-05-28 | Osaka Prefecture | 微粒子シリカ被覆板状粉体およびそれを含有する化粧料 |
JP5359593B2 (ja) | 2009-06-22 | 2013-12-04 | 信越化学工業株式会社 | 複合粒子及びその製造方法、ならびに化粧料 |
US9205031B2 (en) | 2009-06-24 | 2015-12-08 | Shin-Etsu Chemical Co., Ltd. | Composite particles, method for preparing the same and cosmetic composition |
JP2011105673A (ja) * | 2009-11-19 | 2011-06-02 | Noevir Co Ltd | 粉末状化粧料 |
KR101563967B1 (ko) * | 2012-10-18 | 2015-10-28 | 주식회사 엔엔엠테크놀러지 | 개선된 유변학적 특성 및 촉감을 가지며 친수성이 조절된 전분 입자 |
JP2015113306A (ja) * | 2013-12-12 | 2015-06-22 | 花王株式会社 | 無機複合粉体の製造方法 |
JP7016099B2 (ja) * | 2017-02-14 | 2022-02-21 | トピー工業株式会社 | ケイ酸塩被覆体及びその製造方法 |
JPWO2020040169A1 (ja) * | 2018-08-22 | 2021-09-24 | トピー工業株式会社 | ケイ酸塩被覆体 |
EP3842386A4 (en) * | 2018-08-22 | 2022-09-07 | Topy Kogyo Kabushiki Kaisha | SILICATE COATED BODY |
JP2021169421A (ja) * | 2020-04-15 | 2021-10-28 | 信越化学工業株式会社 | 複合粒子及びその製造方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3151354A1 (de) * | 1981-12-24 | 1983-07-07 | Merck Patent Gmbh, 6100 Darmstadt | Perlglanzpigmente, verfahren zu ihrer herstellung und ihre verwendung |
JPS60228406A (ja) * | 1984-04-27 | 1985-11-13 | Pola Chem Ind Inc | 化粧料 |
DE3616133A1 (de) * | 1985-09-25 | 1987-11-19 | Merck Patent Gmbh | Kugelfoermige sio(pfeil abwaerts)2(pfeil abwaerts)-partikel |
FI100659B (fi) * | 1988-08-05 | 1998-01-30 | Huber Corp J M | Paperipigmenttikomposiittituotteita ja menetelmä niiden valmistamiseks i |
DE3922178A1 (de) * | 1989-07-06 | 1991-01-17 | Merck Patent Gmbh | Plaettchenfoermige substrate |
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1991
- 1991-08-15 KR KR1019920703247A patent/KR0145423B1/ko not_active IP Right Cessation
- 1991-08-15 AT AT91914627T patent/ATE171974T1/de active
- 1991-08-15 SG SG1996006477A patent/SG49806A1/en unknown
- 1991-08-15 WO PCT/JP1991/001087 patent/WO1992003119A1/ja active IP Right Grant
- 1991-08-15 JP JP3513494A patent/JP2784261B2/ja not_active Expired - Lifetime
- 1991-08-15 DE DE69130322T patent/DE69130322D1/de not_active Expired - Lifetime
- 1991-08-15 EP EP91914627A patent/EP0543999B1/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
SG49806A1 (en) | 1998-06-15 |
KR0145423B1 (ko) | 1998-07-15 |
JP2784261B2 (ja) | 1998-08-06 |
EP0543999B1 (en) | 1998-10-07 |
ATE171974T1 (de) | 1998-10-15 |
EP0543999A1 (en) | 1993-06-02 |
EP0543999A4 (en) | 1993-09-15 |
WO1992003119A1 (en) | 1992-03-05 |
DE69130322D1 (de) | 1998-11-12 |
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