KR930000617A - 아세탈화된 아조 염료의 제조방법 - Google Patents

아세탈화된 아조 염료의 제조방법 Download PDF

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Publication number
KR930000617A
KR930000617A KR1019920010637A KR920010637A KR930000617A KR 930000617 A KR930000617 A KR 930000617A KR 1019920010637 A KR1019920010637 A KR 1019920010637A KR 920010637 A KR920010637 A KR 920010637A KR 930000617 A KR930000617 A KR 930000617A
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KR
South Korea
Prior art keywords
formula
alkyl
catalyst
dye
preparing
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Application number
KR1019920010637A
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English (en)
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KR100196106B1 (ko
Inventor
한젠 권터
자이틀러 게오르크
Original Assignee
빅케, 바르츠
바스프 악티엔게젤샤프트
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Publication of KR930000617A publication Critical patent/KR930000617A/ko
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Publication of KR100196106B1 publication Critical patent/KR100196106B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B31/00—Disazo and polyazo dyes of the type A->B->C, A->B->C->D, or the like, prepared by diazotising and coupling
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/003—Marking, e.g. coloration by addition of pigments
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00—Monoazo dyes prepared by diazotising and coupling
    • C09B29/06—Monoazo dyes prepared by diazotising and coupling from coupling components containing amino as the only directing group
    • C09B29/08—Amino benzenes
    • C09B29/0805—Amino benzenes free of acid groups
    • C09B29/0807—Amino benzenes free of acid groups characterised by the amino group
    • C09B29/0809—Amino benzenes free of acid groups characterised by the amino group substituted amino group
    • C09B29/0811—Amino benzenes free of acid groups characterised by the amino group substituted amino group further substituted alkylamino, alkenylamino, alkynylamino, cycloalkylamino aralkylamino or arylamino
    • C09B29/0813—Amino benzenes free of acid groups characterised by the amino group substituted amino group further substituted alkylamino, alkenylamino, alkynylamino, cycloalkylamino aralkylamino or arylamino substituted by OH, O-C(=X)-R, O-C(=X)-X-R, O-R (X being O,S,NR; R being hydrocarbonyl)
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B31/00—Disazo and polyazo dyes of the type A->B->C, A->B->C->D, or the like, prepared by diazotising and coupling
    • C09B31/02—Disazo dyes
    • C09B31/04—Disazo dyes from a coupling component "C" containing a directive amino group
    • C09B31/043—Amino-benzenes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B43/00—Preparation of azo dyes from other azo compounds
    • C09B43/28—Preparation of azo dyes from other azo compounds by etherification of hydroxyl groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heat Sensitive Colour Forming Recording (AREA)

Abstract

내용 없음

Description

아세탈화된 아조 염료의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (4)

  1. 물과 방향족 탄화수소의 2-상 반응 혼합물 중에서 커플링 반응을 수행하고, 이어서 수성상을 분리해내고, 유기상으로 존재하는 생성된 일반식(Ⅳ)의 염료를, 중간 분리 업이, 촉매로서 다가 카르복실산의 존재하에 일반식(Ⅴ)의 비닐 에테르와 반응시키는 것으로 이루어지는, 하기 일반식(Ⅱ)의 아민의 디아조늄염을 하기 일반식(Ⅲ)의 커플링 성분과 커플링시키고, 이어서 생성된 하기 일반식(Ⅳ)의 염료를 하기 일반식(Ⅴ)의 비닐 에테르와 반응시키는 것으로 이루어지는, 하기 일반식(Ⅰ)의 염료를 제조하는 방법:
    상기 식에서 n은 0또는 1이고, R1, R2, R3및 R5는 서로 같거나 또는 다르고, 각각 서로 독립적으로 수소, C1-C4-알킬, C1-C4-알콕시, 할로겐 또는 니트로이고, R4및 R5는 서로 같거나 또는 다르고, 각각 서로 독립적으로 수소, C1-C4-알콕시, 니트로 또는 C1-C4-알카노일아미노이고, R6은 C1-C14-알킬이고, R8은 수소 또는 C1-C4-알킬이고, R9는 C1-C18-알킬 또는 시클로헥실이고, L은 C1-C3-알킬렌이다.
  2. 제1항에 있어서, 촉매로서 2가 카르복실산이 사용됨을 특징으로 하는 방법.
  3. 제1항에 있어서, 촉매로서 말레산이 사용됨을 특징으로 하는 방법.
  4. 제1항에 있어서, 일반식(Ⅰ)에서 n이 0임을 특징으로 하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019920010637A 1991-06-20 1992-06-19 아세탈화된 아조 염료의 제조 방법 KR100196106B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE4120363A DE4120363C1 (ko) 1991-06-20 1991-06-20
DEP4120363.1 1991-06-20

Publications (2)

Publication Number Publication Date
KR930000617A true KR930000617A (ko) 1993-01-15
KR100196106B1 KR100196106B1 (ko) 1999-06-15

Family

ID=6434366

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019920010637A KR100196106B1 (ko) 1991-06-20 1992-06-19 아세탈화된 아조 염료의 제조 방법

Country Status (7)

Country Link
US (1) US5247071A (ko)
EP (1) EP0519270B1 (ko)
JP (1) JPH05194866A (ko)
KR (1) KR100196106B1 (ko)
CA (1) CA2071434C (ko)
DE (2) DE4120363C1 (ko)
ES (1) ES2079735T3 (ko)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4343823A1 (de) * 1993-12-22 1995-06-29 Basf Ag Verwendung von Azofarbstoffen zum Markieren von Kohlenwasserstoffen sowie neue Azofarbstoffe
WO2007099059A1 (de) * 2006-03-01 2007-09-07 Basf Se Verwendung von rylenen als markierungsmittel für flüssigkeiten
CN106634016B (zh) * 2016-12-10 2018-10-09 遵义师范学院 一种溶剂黄124的合成方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3244753A (en) * 1966-04-05 Process f-or manufacture cf acetals
US4011209A (en) * 1970-06-17 1977-03-08 Aziende Colori Nazionali Affini Acna S.P.A. Organic solvent-soluble azo dyes
NL7108044A (ko) * 1970-06-17 1971-12-21
DE3627461A1 (de) * 1986-08-13 1988-02-25 Basf Ag Farbstoffmischungen

Also Published As

Publication number Publication date
DE59204554D1 (de) 1996-01-18
EP0519270B1 (de) 1995-12-06
EP0519270A3 (en) 1993-07-21
EP0519270A2 (de) 1992-12-23
CA2071434C (en) 2002-09-03
ES2079735T3 (es) 1996-01-16
US5247071A (en) 1993-09-21
DE4120363C1 (ko) 1992-07-02
KR100196106B1 (ko) 1999-06-15
CA2071434A1 (en) 1992-12-21
JPH05194866A (ja) 1993-08-03

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