KR910018434A - 에폭시 수지의 제조방법 - Google Patents

에폭시 수지의 제조방법 Download PDF

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Publication number
KR910018434A
KR910018434A KR1019910004546A KR910004546A KR910018434A KR 910018434 A KR910018434 A KR 910018434A KR 1019910004546 A KR1019910004546 A KR 1019910004546A KR 910004546 A KR910004546 A KR 910004546A KR 910018434 A KR910018434 A KR 910018434A
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KR
South Korea
Prior art keywords
reaction
catalyst
glycidol
carried out
compound
Prior art date
Application number
KR1019910004546A
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English (en)
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KR0168057B1 (ko
Inventor
샤프너 베르너
하디스타모프 디미터
Original Assignee
베르너 발데크
시바-가이기 아게
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Application filed by 베르너 발데크, 시바-가이기 아게 filed Critical 베르너 발데크
Publication of KR910018434A publication Critical patent/KR910018434A/ko
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Publication of KR0168057B1 publication Critical patent/KR0168057B1/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/02—Polycondensates containing more than one epoxy group per molecule
    • C08G59/04—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof
    • C08G59/06—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols
    • C08G59/063—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols with epihalohydrins
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/02—Polycondensates containing more than one epoxy group per molecule
    • C08G59/12—Polycondensates containing more than one epoxy group per molecule of polycarboxylic acids with epihalohydrins or precursors thereof

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Epoxy Resins (AREA)

Abstract

내용 없음

Description

에폭시 수지의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (12)

  1. 2내지 4개의 페놀성 히드록시기를 함유하는 페놀성 화합물 A를 치환되지 않거나 또는 2- 또는 3-위치에서 C1-C4알킬에 의해 치환된 에피할로이히드린과 반응시키는 동안 상기 페놀성 화합물 A의 히드록시-당량당 0.0085몰의 글리시돌을 첨가하는 것을 포함하는, 한정된 α-글리콜기 함량을 갖는 에폭시 수지의 제조방법.
  2. 제1항에 있어서, 페놀 화합물 A의 히드록시-당량당 0.017몰 이상의 3-클로로-1,2-프로판디올을 사용하여, 3-클로로-1,2-프로판디올의 형태로 글리시돌을 첨가하는 방법.
  3. 제1항에 있어서, 촉매의 존재하에 반응시키는 방법.
  4. 제1항에 있어서, 20내지 200℃에서 반응시키는 방법.
  5. 제1항에 있어서, 40내지 120℃에서 반응시키는 방법.
  6. 제1항에 있어서, 용매를 첨가하여 반응시키는 방법.
  7. 제3항에 있어서, 친액성 촉매의 존재하에서 반응시키는 방법.
  8. 제7항에 있어서, 수산화나트륨, 나트륨 메틸레이트, 4차 포스포늄염 및 암모늄염으로 구성된 군으로부터 촉매를 선정하는 방법.
  9. 제7항에 있어서, 촉매가 2-페닐이미다졸인 방법.
  10. 제1항에, 화합물 A가 2가 페놀일 방법.
  11. 제10항에 있어서. 에피클로로히드린 및 글리시돌과 비스페놀 A를 반응시키는 것을 포함하는 방법.
  12. 제10항에 있어서, 3-클로로-1,2-프로판디올 형태의 글리시돌 및 에피클로로히드핀과 비스페놀 A를 반응시키는 것을 포함하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019910004546A 1990-04-12 1991-03-22 에폭시 수지의 제조방법 KR0168057B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH128290 1990-04-12
CH1282/90-4 1990-04-12

Publications (2)

Publication Number Publication Date
KR910018434A true KR910018434A (ko) 1991-11-30
KR0168057B1 KR0168057B1 (ko) 1999-03-20

Family

ID=4206778

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019910004546A KR0168057B1 (ko) 1990-04-12 1991-03-22 에폭시 수지의 제조방법

Country Status (5)

Country Link
EP (1) EP0452265B1 (ko)
JP (1) JP3044493B2 (ko)
KR (1) KR0168057B1 (ko)
DE (1) DE59108415D1 (ko)
ES (1) ES2097801T3 (ko)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0610987B1 (en) * 1993-02-01 1996-04-10 Shell Internationale Researchmaatschappij B.V. Process for the preparation of alpha-glycol-containing glycidyl ether resins
EP0864594A1 (de) * 1997-03-06 1998-09-16 Ciba SC Holding AG Alpha-Glykolgruppen enthaltende Glycidylverbindungen
TW455584B (en) 1998-09-23 2001-09-21 Shell Int Research Process for the preparation of glycidylesters of branched carboxylic acids
ATE279474T1 (de) * 2002-10-19 2004-10-15 Leuna Harze Gmbh Härtbare epoxidharzzusammensetzung
EP1752436A1 (en) 2003-11-20 2007-02-14 SOLVAY (Société Anonyme) Pseudo-azeotropic composition containing dichloropropanol and process for producing such composition
JP5419446B2 (ja) 2005-05-20 2014-02-19 ソルヴェイ（ソシエテ アノニム） 耐腐食性装置内でのクロロヒドリンの調製方法
KR20080037613A (ko) 2005-05-20 2008-04-30 솔베이(소시에떼아노님) 폴리히드록실화 지방족 탄화수소의 클로로히드린으로의전환 방법
US8124814B2 (en) 2006-06-14 2012-02-28 Solvay (Societe Anonyme) Crude glycerol-based product, process for its purification and its use in the manufacture of dichloropropanol
FR2913421B1 (fr) 2007-03-07 2009-05-15 Solvay Procede de fabrication de dichloropropanol.
FR2913684B1 (fr) 2007-03-14 2012-09-14 Solvay Procede de fabrication de dichloropropanol
TW200911740A (en) 2007-06-01 2009-03-16 Solvay Process for manufacturing a chlorohydrin
TWI500609B (zh) 2007-06-12 2015-09-21 Solvay 含有環氧氯丙烷的產品，其製備及其不同應用中的用途
TW200911693A (en) 2007-06-12 2009-03-16 Solvay Aqueous composition containing a salt, manufacturing process and use
US20100261255A1 (en) * 2007-08-23 2010-10-14 Celio Lume Pereira Process, adapted microbes, composition and apparatus for purification of industrial brine
KR20100089835A (ko) 2007-10-02 2010-08-12 솔베이(소시에떼아노님) 용기의 내부식성 향상을 위한 실리콘-함유 조성물의 용도
FR2925045B1 (fr) 2007-12-17 2012-02-24 Solvay Produit a base de glycerol, procede pour son obtention et son utilisation dans la fabrication de dichloropropanol
TWI478875B (zh) 2008-01-31 2015-04-01 Solvay 使水性組成物中之有機物質降解之方法
CN101980995B (zh) 2008-04-03 2014-06-18 索尔维公司 包含甘油的组合物、获得该组合物的方法以及它们在二氯丙醇生产中的用途
FR2935968B1 (fr) 2008-09-12 2010-09-10 Solvay Procede pour la purification de chlorure d'hydrogene
CN102712738A (zh) * 2009-11-04 2012-10-03 索尔维公司 环氧树脂的制造方法
FR2954772B1 (fr) * 2009-12-24 2012-12-28 Solvay Procede de fabrication d'une resine epoxy
JP6049087B2 (ja) 2010-09-30 2016-12-21 ソルヴェイ（ソシエテ アノニム） 天然起源のエピクロロヒドリンの誘導体
KR102409661B1 (ko) * 2017-06-07 2022-06-17 디아이씨 가부시끼가이샤 에폭시 수지, 제조 방법, 에폭시 수지 조성물 및 그 경화물

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS543900A (en) * 1977-06-13 1979-01-12 Mitsubishi Petrochem Co Ltd Novel alpha-glycol resin composition and its preparation
US4465722A (en) * 1982-07-08 1984-08-14 Ciba-Geigy Corporation Process for the preparation of epoxide resins by the advancement method

Also Published As

Publication number Publication date
ES2097801T3 (es) 1997-04-16
EP0452265A2 (de) 1991-10-16
JPH04234867A (ja) 1992-08-24
JP3044493B2 (ja) 2000-05-22
EP0452265B1 (de) 1996-12-18
DE59108415D1 (de) 1997-01-30
KR0168057B1 (ko) 1999-03-20
EP0452265A3 (en) 1992-04-29

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