KR910001067A - 크실로오스의 새로운 제조방법 - Google Patents

크실로오스의 새로운 제조방법 Download PDF

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Publication number
KR910001067A
KR910001067A KR1019900008846A KR900008846A KR910001067A KR 910001067 A KR910001067 A KR 910001067A KR 1019900008846 A KR1019900008846 A KR 1019900008846A KR 900008846 A KR900008846 A KR 900008846A KR 910001067 A KR910001067 A KR 910001067A
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South Korea
Prior art keywords
xylose
fraction
syrup
rich
glucose
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KR1019900008846A
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English (en)
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KR0157304B1 (ko
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르뢰 쟝-베르나르
뒤플로 피에릭
까보슈 쟝-자끄
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호케트 프레르
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    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00—Preparation of compounds containing saccharide radicals
    • C12P19/04—Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00—Preparation of compounds containing saccharide radicals
    • C12P19/24—Preparation of compounds containing saccharide radicals produced by the action of an isomerase, e.g. fructose
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00—Preparation of compounds containing saccharide radicals
    • C12P19/02—Monosaccharides
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K13/00—Sugars not otherwise provided for in this class
    • C13K13/002—Xylose
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00—Chemistry: molecular biology and microbiology
    • Y10S435/803—Physical recovery methods, e.g. chromatography, grinding
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00—Chemistry: molecular biology and microbiology
    • Y10S435/8215—Microorganisms
    • Y10S435/911—Microorganisms using fungi
    • Y10S435/938—Pichia

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Biochemistry (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biotechnology (AREA)
  • Health & Medical Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Saccharide Compounds (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

내용 없음.

Description

크실로오스의 새로운 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 본 발명에 따른 방법의 경로를 다이아그램으로 나타낸 도면임.
제2도 내지 4도는 상기 방법을 실시하는데 적합한 설비의 일부를 다이아그램으로 나타낸 도면임.

Claims (8)

  1. -제1단계에서, D-크실롤로오스 시럽을 효소적으로 이성화시켜 D-크실로오스와 D-크실롤로오스의 혼합물을 얻고, -제2단계에서, 상기 혼합물을 크로마토그래피 처리하여 적어도 2분획, 즉, D-크실로오스가 매우 풍부한 것과(분획 X1) D-크실롤로오스가 매우 풍부한 것(분획 X2)의 2분획을 얻으며, - 제3단계에서, 분획 X2를 이성화 단계로 재순환시키고, D-크실롤로오스를 분획 X1으로부터 회수하는 것으로 됨을 특징으로 하는 (후자는 직접 수소첨가 반응시켜도 됨) D-크실롤로오스의 제조방법.
  2. 제1항에 있어서, 출발 D-크실롤로오스를 다음의 연속 단계 , 즉 ;
    -D-글루코오스를 D-아라비톨로 전환시키는, 피차아속의 호삼투성 미생물에 의해 D-글루코오스 시럽을 호기적으로 발효시키고, -D-아라비톨을 D-크실롤로오스로 전환시키는데 적합한, 데히드로게나제 알콜 생산 미생물인 아세토박터, 글루코노박터 또는 클렙시엘라속의 미생물을 이용하여 D-아라비톨을 호기적으로 발효시킨다음 -글루코오스 이소머라제 또는 크실로오스 이소머라제의 작용하에서 D-크실롤로오스 시럽을 D-크실로오스가 풍부한 시럽으로 이성화시키는 단계에 의해 제조함을 특징으로 하는 제조방법.
  3. 제1항 및 제2항중 어느 한항에 있어서, 사용되는 효소가 글루코오스-이소머라제인 것이 특징인 제조방법.
  4. 제1항 내지 3항중 어느 한항에 있어서, 크로마토그래피 분획화 단계를 양이온수지 또는 제올라이트의 도움을 받아 수행하는 것이 특징인 제조방법.
  5. 제4항에 있어서, 크로마토그래피 분획과 단계를 불연속적으로 또는 연속적으로 (시뮬레이트 이동 베드), 바람직하게는 알칼리 또는 알칼리토이온으로 하전된 강산 양이온수지 타잎의 흡착제 또는 NH+ 4, Na+,K+및 Ca2-, Ba2-이온으로 하전된 양이온 제올라이트 타잎의 흡착제상에서 수행하는 것이 특징인 제조방법.
  6. 제1항 내지 5항중 어느 한항에 있어서, 효소적 이성화 단계의 변수를 시럽중에 D-크실로오스가 53%를 초과 하는 함량으로 생성하도록 선택하는 것이 특징인 제조방법.
  7. 제1항 내지 6항중 어느 한항에 있어서, 크로마토그래피 분획화 단계의 변수를 크실로오스 함량(건조물질에 대한 중량으로 표시)이 다음과 같고 D-크실롤로오스 함량은 25%미만인, 크실로오스가 풍부한 분획이 얻어지도록 선택하는 것이 특징인 제조방법 : -60~95%, -바람직하게는 75~90%, 더욱 바람직하게는 80~85%.
  8. 제1항 내지 7항중 어느 한항에 있어서, 크실로오스의 결정화부터의 모액을 크로마토그래피 분획화 단계로 재순환시키는 것이 특징인 제조방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019900008846A 1989-06-16 1990-06-15 크실로오스의 새로운 제조방법 KR0157304B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR8908046A FR2648474B1 (fr) 1989-06-16 1989-06-16 Nouveau procede de fabrication du xylose
FR8908046 1989-06-16

Publications (2)

Publication Number Publication Date
KR910001067A true KR910001067A (ko) 1991-01-30
KR0157304B1 KR0157304B1 (ko) 1998-10-15

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Country Status (14)

Country Link
US (1) US5238826A (ko)
EP (1) EP0403392B1 (ko)
JP (1) JP2981257B2 (ko)
KR (1) KR0157304B1 (ko)
AT (1) ATE109209T1 (ko)
BR (1) BR9002828A (ko)
CA (1) CA2019036C (ko)
DE (1) DE69010999T2 (ko)
DK (1) DK0403392T3 (ko)
ES (1) ES2060976T3 (ko)
FI (1) FI95576C (ko)
FR (1) FR2648474B1 (ko)
IE (1) IE64306B1 (ko)
RU (1) RU1838418C (ko)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2652589B1 (fr) * 1989-10-04 1995-02-17 Roquette Freres Procede de fabrication de xylitol et de produits riches en xylitol.
US5728225A (en) * 1993-07-26 1998-03-17 Roquette Freres Viscous liquid compositions of xylitol and a process for preparing them
GB9514538D0 (en) 1995-07-15 1995-09-13 Cerestar Holding Bv Process for the production of xylitol
FR2749307B1 (fr) * 1996-05-29 1998-09-04 Roquette Freres Procede de preparation de d-arabitol
JPH11266888A (ja) 1997-10-17 1999-10-05 Ajinomoto Co Inc キシリトールの製造法
JP3855486B2 (ja) 1997-10-17 2006-12-13 味の素株式会社 キシリトールの製造法
US6036865A (en) * 1998-06-15 2000-03-14 Union Carbide Chemicals & Plastics Technology Corporation Separation processes
US6045703A (en) * 1998-06-15 2000-04-04 Union Carbide Chemicals & Plastics Technology Corporation Separation processes
FI106853B (fi) 1998-11-18 2001-04-30 Xyrofin Oy Menetelmä polyolien valmistamiseksi arabinoksylaania sisältävästä materiaalista
JP2000210095A (ja) 1999-01-20 2000-08-02 Ajinomoto Co Inc キシリト―ル又はｄ―キシルロ―スの製造法
JP2001008682A (ja) * 1999-06-24 2001-01-16 Ajinomoto Co Inc Ｄ−アラビトール、ｄ−キシルロース及びキシリトールの製造法
WO2001012834A1 (en) * 1999-08-18 2001-02-22 Hydrios Biotechnology Oy Process for the preparation and simultaneous separation of enzyme-catalysed products
US6894199B2 (en) 2001-04-27 2005-05-17 Danisco Sweeteners Oy Process for the production of xylitol
FI20011889A (fi) 2001-09-26 2003-03-27 Xyrofin Oy Menetelmä ksylitolin valmistamiseksi
US6998480B2 (en) * 2002-03-08 2006-02-14 Tate & Lyle Public Limited Company Process for improving sucralose purity and yield
US6943248B2 (en) * 2003-04-30 2005-09-13 Tate & Lyle Public Limited Company Crystalline form of sucralose, and method for producing it
US7812153B2 (en) * 2004-03-11 2010-10-12 Rayonier Products And Financial Services Company Process for manufacturing high purity xylose
CN103201395B (zh) 2010-06-26 2016-03-02 威尔迪亚有限公司 糖混合物及其生产和使用方法
GB2505148B8 (en) 2011-04-07 2016-12-07 Virdia Ltd Lignocellulose conversion processes and products
CN102796797B (zh) * 2012-08-09 2014-07-09 山东天力药业有限公司 微生物转化葡萄糖制备木糖醇及其中间体d-木酮糖的方法及所用的菌种
DK3416740T3 (da) 2016-02-19 2021-02-08 Intercontinental Great Brands Llc Fremgangsmåder til dannelse af multiple værdistrømme ud fra biomassekilder
CN110382684A (zh) 2016-12-21 2019-10-25 创新生物科学公司 产生木糖醇的梅奇酵母种

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1518510A (fr) * 1967-04-12 1968-03-22 Kyowa Hakko Kogyo Kk Procédé de production de d-ribulose et d-xylulose par fermentation
JPS543949B1 (ko) * 1968-05-25 1979-02-28
US3619369A (en) * 1968-10-31 1971-11-09 Noda Inst For Scientific Res Process for producing xylitol by fermentation
US4490468A (en) * 1980-04-23 1984-12-25 Purdue Research Foundation Production of ethanol by yeast using xylulose
US4394178A (en) * 1981-12-10 1983-07-19 Union Carbide Corporation Bulk lactulose/lactose separation by selective adsorption on zeolitic molecular sieves

Also Published As

Publication number Publication date
EP0403392A2 (fr) 1990-12-19
IE64306B1 (en) 1995-07-26
ATE109209T1 (de) 1994-08-15
DK0403392T3 (da) 1994-08-22
CA2019036C (en) 2000-01-11
DE69010999D1 (de) 1994-09-01
FI95576B (fi) 1995-11-15
KR0157304B1 (ko) 1998-10-15
BR9002828A (pt) 1991-08-20
FR2648474A1 (fr) 1990-12-21
JPH0367596A (ja) 1991-03-22
DE69010999T2 (de) 1994-12-15
EP0403392A3 (fr) 1991-05-08
EP0403392B1 (fr) 1994-07-27
FR2648474B1 (fr) 1995-01-06
ES2060976T3 (es) 1994-12-01
CA2019036A1 (en) 1990-12-16
RU1838418C (ru) 1993-08-30
FI95576C (fi) 1996-02-26
IE902172A1 (en) 1991-01-02
US5238826A (en) 1993-08-24
FI903009A0 (fi) 1990-06-15
IE902172L (en) 1990-12-16
JP2981257B2 (ja) 1999-11-22

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