KR890008066A - 아디프산의 제조방법 - Google Patents

아디프산의 제조방법 Download PDF

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Publication number
KR890008066A
KR890008066A KR870012932A KR870012932A KR890008066A KR 890008066 A KR890008066 A KR 890008066A KR 870012932 A KR870012932 A KR 870012932A KR 870012932 A KR870012932 A KR 870012932A KR 890008066 A KR890008066 A KR 890008066A
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KR
South Korea
Prior art keywords
parts
adipic acid
reacted
producing adipic
salt
Prior art date
Application number
KR870012932A
Other languages
English (en)
Other versions
KR910002280B1 (ko
Inventor
조영상
오재춘
Original Assignee
이정오
한국과학 기술원
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 이정오, 한국과학 기술원 filed Critical 이정오
Priority to KR1019870012932A priority Critical patent/KR910002280B1/ko
Priority to JP63136635A priority patent/JP2581759B2/ja
Publication of KR890008066A publication Critical patent/KR890008066A/ko
Application granted granted Critical
Publication of KR910002280B1 publication Critical patent/KR910002280B1/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/50—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C55/00—Saturated compounds having more than one carboxyl group bound to acyclic carbon atoms
    • C07C55/02—Dicarboxylic acids
    • C07C55/14—Adipic acid

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

내용 없음

Description

아디프산의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (5)

  1. 시클로핵사논 또는 시클로핵산올 단독 또는 시클로핵사논과 시클로핵산올 혼합물에 아세트산 용매와 촉매 존재하에 질산 산화시키는 것을 특징으로하는 아디프산의 제조방법.
  2. 제 1 항에 있어서, 아세트산을 원료 1부에 대하여 0.1부 내지 100부를 첨가하여 반응시키는 것을 특지으로 하는 아디프산의 제조방법.
  3. 제 1 항에 있어서, 촉매로서 바나듐염의 경우 원료 1부에 대하여 0.005부 내지 0.05부를, 코발트 염 또는 망간 염은 0.001부 내지 0.005부를, 그리고 구리염은 0.002부 내지 0.1부를 첨가하여 반응시키는 것을 특징으로하는 아디프산의 제조방법.
  4. 제 1 항에 있어서, 반응온도를 45℃-90℃에서 반응시키는 것을 특징으로하는 아디프산의 제조방법.
  5. 제 1 항에 있어서, 반응압력을 1기압 내지 5기압에서 반응시키는 것을 특징으로 하는 아디프산의 제조방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019870012932A 1987-11-17 1987-11-17 아디프산의 제조방법 KR910002280B1 (ko)

Priority Applications (2)

Application Number Priority Date Filing Date Title
KR1019870012932A KR910002280B1 (ko) 1987-11-17 1987-11-17 아디프산의 제조방법
JP63136635A JP2581759B2 (ja) 1987-11-17 1988-06-02 アジピン酸の製造方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1019870012932A KR910002280B1 (ko) 1987-11-17 1987-11-17 아디프산의 제조방법

Publications (2)

Publication Number Publication Date
KR890008066A true KR890008066A (ko) 1989-07-08
KR910002280B1 KR910002280B1 (ko) 1991-04-11

Family

ID=19266076

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019870012932A KR910002280B1 (ko) 1987-11-17 1987-11-17 아디프산의 제조방법

Country Status (2)

Country Link
JP (1) JP2581759B2 (ko)
KR (1) KR910002280B1 (ko)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE60207677D1 (de) * 2002-01-04 2006-01-05 Council Scient Ind Res Ein verbessertes Verfahren zur Herstellung von Adipinsäure
FR2939131B1 (fr) * 2008-12-01 2010-12-17 Rhodia Operations Procede de fabrication d'acide adipique
CN108084012B (zh) * 2016-11-22 2019-12-31 中国科学院大连化学物理研究所 一种氧化环己酮制备己二酸的方法

Also Published As

Publication number Publication date
JPH01135741A (ja) 1989-05-29
KR910002280B1 (ko) 1991-04-11
JP2581759B2 (ja) 1997-02-12

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