KR890006553A - 비스페놀a 의 제조방법 - Google Patents

비스페놀a 의 제조방법

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Publication number
KR890006553A
KR890006553A KR1019880013167A KR880013167A KR890006553A KR 890006553 A KR890006553 A KR 890006553A KR 1019880013167 A KR1019880013167 A KR 1019880013167A KR 880013167 A KR880013167 A KR 880013167A KR 890006553 A KR890006553 A KR 890006553A
Authority
KR
South Korea
Prior art keywords
weight
bisphenol
reaction
phenol
mixture
Prior art date
Application number
KR1019880013167A
Other languages
English (en)
Other versions
KR910008367B1 (ko
Inventor
그라지와 에드워드
키에딕 마시에즈
콜트 조제프
마주르 아담
마르스직키 저지
자야크 유제니우즈
로데즈코 안나
크지즈 저지
테레락 카시미어즈
스위더스키 즈비그니우
배크 테오드르
Original Assignee
마리안 타니에우스키
인스티튜트 시에즈 키이즈 신테지 오르가니즈 네즈 "블라쵸우니아"
마주르 아담
자클라디 케미즌"블라쵸우니아"
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 마리안 타니에우스키, 인스티튜트 시에즈 키이즈 신테지 오르가니즈 네즈 "블라쵸우니아", 마주르 아담, 자클라디 케미즌"블라쵸우니아" filed Critical 마리안 타니에우스키
Publication of KR890006553A publication Critical patent/KR890006553A/ko
Application granted granted Critical
Publication of KR910008367B1 publication Critical patent/KR910008367B1/ko

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/12—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring polycyclic with no unsaturation outside the aromatic rings
    • C07C39/15—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring polycyclic with no unsaturation outside the aromatic rings with all hydroxy groups on non-condensed rings, e.g. phenylphenol
    • C07C39/16—Bis-(hydroxyphenyl) alkanes; Tris-(hydroxyphenyl)alkanes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/11—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms
    • C07C37/20—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms using aldehydes or ketones

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

내용 없음

Description

비스페놀 A의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (4)

  1. 페놀에 녹아있는 비스페놀 A와 반응부산물의 용액인 건조된 후 결정화 리커로, 양이온 고환 촉매의 존재하에 페놀과 아세톤을 반응시켜 비스페놀 A를 제조하는 방법에 있어서, 페놀과 아세톤의 반응은 반응혼합물에 기초하여 12 내지 20중량%의, 바람직하게는 15 내지 18중량%의 비스페놀 A 초기농도에서 21 내지 35중량%, 바람직하게는 22 내지 28중량%의 비스페놀 A최종농도까지 수행되며, 그리고 반응 혼합물내의 반응 부산물의 함량은 12 내지 24중량%, 바람직하게는 16 내지 20중량%이며, 단 5-30 : 1의 페놀대 아세톤의 몰비로 60 내지 95℃의 온도에서 공정이 수행되는 것을 특징으로 하는 비스페놀 A의 제조방법.
  2. 제1항에 있어서, 반응을 위한 장입 혼합물은 반응 시스템으로부터의 일부의 반응혼합물과 귀환된 페놀리커의 혼합에 의해서 얻어진 것임을 특징으로 하는 방법.
  3. 제1항에 있어서, 촉매는 0.05-0.5 : 1의 중량비로 마이크로다공질 구조 양이온 교환자와 마크로다공질구조 양이온 교환자의 혼합물인 것을 특징으로 하는 방법.
  4. 제1항에 있어서, 비스페놀A 이성체의 함량은 장입 혼합물에 함유된 부산물의 함량의 ½이내인 것을 특징으로 하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019880013167A 1987-10-07 1988-10-07 비스페놀 a의 제조방법 KR910008367B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PL1987268149A PL153396B1 (en) 1987-10-07 1987-10-07 Method of obtaining bisphenol a
PLP268149 1987-10-07

Publications (2)

Publication Number Publication Date
KR890006553A true KR890006553A (ko) 1989-06-13
KR910008367B1 KR910008367B1 (ko) 1991-10-12

Family

ID=20038430

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019880013167A KR910008367B1 (ko) 1987-10-07 1988-10-07 비스페놀 a의 제조방법

Country Status (8)

Country Link
US (1) US4906789A (ko)
KR (1) KR910008367B1 (ko)
CN (1) CN1013363B (ko)
DE (1) DE3833900A1 (ko)
IN (1) IN171653B (ko)
PL (1) PL153396B1 (ko)
RU (1) RU1799376C (ko)
UA (1) UA13478A1 (ko)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5059721A (en) * 1990-07-31 1991-10-22 Shell Oil Company Process for preparing a bisphenol
PL164289B1 (pl) * 1990-11-24 1994-07-29 Inst Ciezkiej Syntezy Orga Sposób otrzymywani blsfenolu A PL PL
DE4312039A1 (de) * 1993-04-13 1994-10-20 Bayer Ag Optimierte Ionenaustauscherschüttungen für die Bis-phenol-A Synthese
US5783733A (en) * 1996-06-13 1998-07-21 General Electric Company Process for manufacture of bisphenol
DE19720540A1 (de) 1997-05-16 1998-11-19 Bayer Ag Verfahren zur Aufarbeitung von Mutterlaugen aus der Bisphenolsynthese
DE19720541A1 (de) 1997-05-16 1998-11-19 Bayer Ag Verfahren zur kontinuierlichen Herstellung von Dihydroxydiphenylalkanen
DE19720539A1 (de) 1997-05-16 1998-11-19 Bayer Ag Verfahren zur kontinuierlichen Herstellung von Dihydroxydiarylalkanen
US20050075520A1 (en) * 2002-03-13 2005-04-07 O'young Drow Lionel System and method of producing bisphenol-A (BPA) using two stage crystallization
US6960697B2 (en) * 2002-03-13 2005-11-01 Mitsubishi Chemical Corporation System and method of producing bisphenol-A (BPA)
US20100121111A1 (en) * 2006-05-31 2010-05-13 Baker Hughes Incorporated Alkoxylations of High Melting Point Substrates in Ketone Solvents

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3049569A (en) * 1958-10-20 1962-08-14 Union Carbide Corp Production of 2, 2-bis(4-hydroxyphenyl) propane
US3221061A (en) * 1961-08-01 1965-11-30 Union Carbide Corp Process for the production of 2,2-bis-(4-hydroxyphenyl) propane
DE2537027C2 (de) * 1975-08-20 1982-06-03 Bayer Ag, 5090 Leverkusen Verfahren zur Herstellung von 4,4'-Dihydroxy-3,3',5,5'-tetraalkyl- diphenylalkanen
US4308405A (en) * 1978-07-05 1981-12-29 Shell Oil Company Preparation of bisphenols
PL124542B1 (en) * 1978-12-30 1983-01-31 Instytut Ciezkiej Syntezy Organicznej "Blachownia" Method of manufacture of bisphenol a
US4391997A (en) * 1981-10-23 1983-07-05 General Electric Company Ion exchange catalyzed bisphenol process

Also Published As

Publication number Publication date
KR910008367B1 (ko) 1991-10-12
RU1799376C (ru) 1993-02-28
IN171653B (ko) 1992-12-05
PL268149A1 (en) 1989-04-17
DE3833900A1 (de) 1989-04-27
CN1013363B (zh) 1991-07-31
CN1034197A (zh) 1989-07-26
PL153396B1 (en) 1991-04-30
US4906789A (en) 1990-03-06
UA13478A1 (uk) 1997-04-25
DE3833900C2 (ko) 1991-08-14

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