KR880007546A - 아민알란의 제조방법 - Google Patents

아민알란의 제조방법 Download PDF

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Publication number
KR880007546A
KR880007546A KR870014704A KR870014704A KR880007546A KR 880007546 A KR880007546 A KR 880007546A KR 870014704 A KR870014704 A KR 870014704A KR 870014704 A KR870014704 A KR 870014704A KR 880007546 A KR880007546 A KR 880007546A
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KR
South Korea
Prior art keywords
tetrahydrate
reaction medium
tertiary amine
carried out
alan
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KR870014704A
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English (en)
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KR900005183B1 (ko
Inventor
마이클 마릿 에버릿
Original Assignee
원본미기재
에씰 코오포레이션
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Application filed by 원본미기재, 에씰 코오포레이션 filed Critical 원본미기재
Publication of KR880007546A publication Critical patent/KR880007546A/ko
Application granted granted Critical
Publication of KR900005183B1 publication Critical patent/KR900005183B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic System
    • C07F5/06—Aluminium compounds
    • C07F5/069—Aluminium compounds without C-aluminium linkages

Abstract

내용 없음.

Description

아민알란의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (6)

  1. 하기(a), (b) 및 (c)를 반응시키는 것을 특징으로하는 3차 아민 알란의 제조방법 : (a) 일반식이 MAlH4이고 이때 M은 리튬, 나트륨 및 칼륨으로 이루어진 군으로부터 선택되는 알칼리 금속인 알칼리금속 알루미늄 사수소화물, (b) 할로겐화 수소 및, (c) 착화 3차 아민.
  2. 제1항에 있어서, 대략 등몰량의 (a), (b) 및 (c)를 반응시키는 것을 특징으로 하는 방법.
  3. 제1항 또는 제2항에 있어서, 탄화수소 반응매질의 존재하에 실시되는 방법.
  4. 제1항, 제2항 또는 제3항에 있어서, 상기 사수소화물이 사수소화알루미늄나트륨인 방법.
  5. 제1항, 제2항 또는 제3항 또는 제3항에 있어서, (a)가 NaAlH4이고, (b)가 HCl이며, (c)가 (C2H5)3N인 방법.
  6. 제5항에 있어서, 액체 반응매질로서 톨루엔의 존재하에, 그리고 5℃-50℃의 온도하에 실시됨을 특징으로 하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019870014704A 1986-12-22 1987-12-21 아민알란의 제조방법 KR900005183B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US06/945,286 US4748260A (en) 1986-12-22 1986-12-22 Preparation of amine alanes
US945286 1986-12-22

Publications (2)

Publication Number Publication Date
KR880007546A true KR880007546A (ko) 1988-08-27
KR900005183B1 KR900005183B1 (ko) 1990-07-20

Family

ID=25482916

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019870014704A KR900005183B1 (ko) 1986-12-22 1987-12-21 아민알란의 제조방법

Country Status (7)

Country Link
US (1) US4748260A (ko)
EP (1) EP0273229B1 (ko)
JP (1) JPS63190890A (ko)
KR (1) KR900005183B1 (ko)
CA (1) CA1276941C (ko)
DE (2) DE3780933T2 (ko)
ES (1) ES2003072A4 (ko)

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US7833250B2 (en) 2004-11-10 2010-11-16 Jackson Roger P Polyaxial bone screw with helically wound capture connection
US8353932B2 (en) 2005-09-30 2013-01-15 Jackson Roger P Polyaxial bone anchor assembly with one-piece closure, pressure insert and plastic elongate member
US8292926B2 (en) 2005-09-30 2012-10-23 Jackson Roger P Dynamic stabilization connecting member with elastic core and outer sleeve
US7862587B2 (en) 2004-02-27 2011-01-04 Jackson Roger P Dynamic stabilization assemblies, tool set and method
US10729469B2 (en) 2006-01-09 2020-08-04 Roger P. Jackson Flexible spinal stabilization assembly with spacer having off-axis core member
US10258382B2 (en) 2007-01-18 2019-04-16 Roger P. Jackson Rod-cord dynamic connection assemblies with slidable bone anchor attachment members along the cord
US8876868B2 (en) 2002-09-06 2014-11-04 Roger P. Jackson Helical guide and advancement flange with radially loaded lip
US7621918B2 (en) 2004-11-23 2009-11-24 Jackson Roger P Spinal fixation tool set and method
US8540753B2 (en) 2003-04-09 2013-09-24 Roger P. Jackson Polyaxial bone screw with uploaded threaded shank and method of assembly and use
US7377923B2 (en) 2003-05-22 2008-05-27 Alphatec Spine, Inc. Variable angle spinal screw assembly
US7776067B2 (en) 2005-05-27 2010-08-17 Jackson Roger P Polyaxial bone screw with shank articulation pressure insert and method
US7967850B2 (en) 2003-06-18 2011-06-28 Jackson Roger P Polyaxial bone anchor with helical capture connection, insert and dual locking assembly
US8366753B2 (en) 2003-06-18 2013-02-05 Jackson Roger P Polyaxial bone screw assembly with fixed retaining structure
US8936623B2 (en) 2003-06-18 2015-01-20 Roger P. Jackson Polyaxial bone screw assembly
US8092500B2 (en) 2007-05-01 2012-01-10 Jackson Roger P Dynamic stabilization connecting member with floating core, compression spacer and over-mold
US7766915B2 (en) 2004-02-27 2010-08-03 Jackson Roger P Dynamic fixation assemblies with inner core and outer coil-like member
US20050203513A1 (en) 2003-09-24 2005-09-15 Tae-Ahn Jahng Spinal stabilization device
US8979900B2 (en) 2003-09-24 2015-03-17 DePuy Synthes Products, LLC Spinal stabilization device
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US11419642B2 (en) 2003-12-16 2022-08-23 Medos International Sarl Percutaneous access devices and bone anchor assemblies
US7179261B2 (en) 2003-12-16 2007-02-20 Depuy Spine, Inc. Percutaneous access devices and bone anchor assemblies
US7527638B2 (en) 2003-12-16 2009-05-05 Depuy Spine, Inc. Methods and devices for minimally invasive spinal fixation element placement
US8152810B2 (en) 2004-11-23 2012-04-10 Jackson Roger P Spinal fixation tool set and method
US7160300B2 (en) 2004-02-27 2007-01-09 Jackson Roger P Orthopedic implant rod reduction tool set and method
WO2005092218A1 (en) 2004-02-27 2005-10-06 Jackson Roger P Orthopedic implant rod reduction tool set and method
US7651502B2 (en) 2004-09-24 2010-01-26 Jackson Roger P Spinal fixation tool set and method for rod reduction and fastener insertion
US8926672B2 (en) 2004-11-10 2015-01-06 Roger P. Jackson Splay control closure for open bone anchor
JP2008519656A (ja) 2004-11-10 2008-06-12 ロジャー・ピー・ジャクソン 破断伸張部付の螺旋状案内及び前進フランジ
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US9216041B2 (en) 2009-06-15 2015-12-22 Roger P. Jackson Spinal connecting members with tensioned cords and rigid sleeves for engaging compression inserts
US9168069B2 (en) 2009-06-15 2015-10-27 Roger P. Jackson Polyaxial bone anchor with pop-on shank and winged insert with lower skirt for engaging a friction fit retainer
US8556938B2 (en) 2009-06-15 2013-10-15 Roger P. Jackson Polyaxial bone anchor with non-pivotable retainer and pop-on shank, some with friction fit
US8444681B2 (en) 2009-06-15 2013-05-21 Roger P. Jackson Polyaxial bone anchor with pop-on shank, friction fit retainer and winged insert
US9980753B2 (en) 2009-06-15 2018-05-29 Roger P Jackson pivotal anchor with snap-in-place insert having rotation blocking extensions
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US7901437B2 (en) 2007-01-26 2011-03-08 Jackson Roger P Dynamic stabilization member with molded connection
US10076361B2 (en) 2005-02-22 2018-09-18 Roger P. Jackson Polyaxial bone screw with spherical capture, compression and alignment and retention structures
US8105368B2 (en) 2005-09-30 2012-01-31 Jackson Roger P Dynamic stabilization connecting member with slitted core and outer sleeve
CA2670988C (en) 2006-12-08 2014-03-25 Roger P. Jackson Tool system for dynamic spinal implants
US8475498B2 (en) 2007-01-18 2013-07-02 Roger P. Jackson Dynamic stabilization connecting member with cord connection
US9451989B2 (en) 2007-01-18 2016-09-27 Roger P Jackson Dynamic stabilization members with elastic and inelastic sections
US8366745B2 (en) 2007-05-01 2013-02-05 Jackson Roger P Dynamic stabilization assembly having pre-compressed spacers with differential displacements
US8012177B2 (en) 2007-02-12 2011-09-06 Jackson Roger P Dynamic stabilization assembly with frusto-conical connection
US8979904B2 (en) 2007-05-01 2015-03-17 Roger P Jackson Connecting member with tensioned cord, low profile rigid sleeve and spacer with torsion control
US10383660B2 (en) 2007-05-01 2019-08-20 Roger P. Jackson Soft stabilization assemblies with pretensioned cords
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US8911477B2 (en) 2007-10-23 2014-12-16 Roger P. Jackson Dynamic stabilization member with end plate support and cable core extension
KR101569224B1 (ko) * 2007-12-26 2015-11-13 제이에스알 가부시끼가이샤 알루미늄막 형성용 조성물 및 알루미늄막의 형성 방법
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JP5191379B2 (ja) * 2008-12-26 2013-05-08 エア・ウォーター株式会社 アミンアランの精製方法
CN103826560A (zh) 2009-06-15 2014-05-28 罗杰.P.杰克逊 具有套接杆和带摩擦配合压缩套爪的带翼插件的多轴骨锚
US11229457B2 (en) 2009-06-15 2022-01-25 Roger P. Jackson Pivotal bone anchor assembly with insert tool deployment
US8998959B2 (en) 2009-06-15 2015-04-07 Roger P Jackson Polyaxial bone anchors with pop-on shank, fully constrained friction fit retainer and lock and release insert
US9668771B2 (en) 2009-06-15 2017-06-06 Roger P Jackson Soft stabilization assemblies with off-set connector
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JP5865479B2 (ja) 2011-03-24 2016-02-17 ロジャー・ピー・ジャクソン 複合関節とポップ装着式シャンクとを有する多軸の骨アンカー
US8911479B2 (en) 2012-01-10 2014-12-16 Roger P. Jackson Multi-start closures for open implants
US8911478B2 (en) 2012-11-21 2014-12-16 Roger P. Jackson Splay control closure for open bone anchor
US10058354B2 (en) 2013-01-28 2018-08-28 Roger P. Jackson Pivotal bone anchor assembly with frictional shank head seating surfaces
US8852239B2 (en) 2013-02-15 2014-10-07 Roger P Jackson Sagittal angle screw with integral shank and receiver
US9566092B2 (en) 2013-10-29 2017-02-14 Roger P. Jackson Cervical bone anchor with collet retainer and outer locking sleeve
US9717533B2 (en) 2013-12-12 2017-08-01 Roger P. Jackson Bone anchor closure pivot-splay control flange form guide and advancement structure
US9451993B2 (en) 2014-01-09 2016-09-27 Roger P. Jackson Bi-radial pop-on cervical bone anchor
US10064658B2 (en) 2014-06-04 2018-09-04 Roger P. Jackson Polyaxial bone anchor with insert guides
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Also Published As

Publication number Publication date
EP0273229A3 (en) 1989-07-19
EP0273229A2 (en) 1988-07-06
DE273229T1 (de) 1988-11-24
DE3780933D1 (de) 1992-09-10
US4748260A (en) 1988-05-31
JPH0224277B2 (ko) 1990-05-29
ES2003072A4 (es) 1988-10-16
DE3780933T2 (de) 1992-12-24
JPS63190890A (ja) 1988-08-08
EP0273229B1 (en) 1992-08-05
CA1276941C (en) 1990-11-27
KR900005183B1 (ko) 1990-07-20

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