KR880002790A - 디프로파프길옥시벤젠 화합물 및 그의 제조방법 - Google Patents

디프로파프길옥시벤젠 화합물 및 그의 제조방법 Download PDF

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KR880002790A
KR880002790A KR1019870008799A KR870008799A KR880002790A KR 880002790 A KR880002790 A KR 880002790A KR 1019870008799 A KR1019870008799 A KR 1019870008799A KR 870008799 A KR870008799 A KR 870008799A KR 880002790 A KR880002790 A KR 880002790A
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준야 다까하시
시게오 나까무라
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모리 히데오
스미또모 가가꾸 고오교 가부시끼가이샤
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Abstract

내용 없음

Description

디프로파프길옥시벤젠 화합물 및 그의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (15)

  1. 하기 일반식(I)의 화합물.
    [상기 식중, X는 할로겐원자이고, Y는 C1-C4알킬기, C2-C4알케닐기, C1-C3알콕시기, C3-C4알케닐옥시기, C3-C4알키닐옥시기, 페닐에 의해 치환된 C2-C3알케닐기, 할로겐에 의해 치환된 C3-C4알케닐옥시기, 할로겐, C1-C3알콕시, C1-C3알카노일, 시아노, 히드록시카르보닐, C1-C3알킬아미노카르보닐 및 페닐로 구성된 군으로부터 선택된 하나의 치환체에 의해 치환된 C1-C3알콕시, 또는 일반식 :-CH2O-R1,-CH=CH-R2, -CH=N-R3또는 -CO-R4(식중, R1은 C1-C3알킬기, C3-C4알케닐기 또는 C3-C4알키닐기이고, R2는 시아노기, 메톡시카르보닐기 또는 아세틸기이고, R3은 디멜틸 아미노기 또는 페닐기이고, R4는 C1-C2알킬기이다)의 기이다.]
  2. 제 1항에 있어서, X가 염소원자이고, Y가 C1-C3알킬기,C2-C3알케닐기,C1-C3알콕시기,C3알키닐옥시기, 할로(C2)알콕시기, 할로(C3)알케닐옥시기, 메틸카르보니메톡시기, 2-시아노비닐기, 페닐아미노메틸기,또는 일반식 : -CH2OR1(식중, R1는 메틸기, C3알케닐기, 또는 C3알키닐기이다)의 기임을 특징으로 하는 화합물.
  3. 제 1항에 있어서, X가 염소원자이고, Y가 메틸기, 에틸기, 메톡시기, 에톡시기, 프로필옥시기, 비닐기, 프로파르길옥시기, 2-플루오로에톡시기, 메톡시메톡시기, 3-클로로-2-프로페닐기, 2-클로로-2-프로페닐기, 메틸카르보닐케톡시기, 2-시아노비닐기 또는 페닐이미노멜틸기임을 특징으로 하는 화합물.
  4. 불활성 담체 또는 희석제와 함께 활성 성분으로 살진균학적으로 유용한 양의최소한 하나의 하기 일반식(I)의 화합물을 함유함을 특징으로 하는 살진균 조성물.
    [상기 식중, X는 할로겐원자이고, Y는 C1-C4알킬기, C2-C4알케닐기, C1-C3알콕시기, C3-C4알케닐옥시기, C3-C4알키닐옥시기, 페닐에 의해 치환된 C2-C3알케닐기, 할로겐에 의해 치환된 C3-C4알케닐옥시기, 할로겐, C1-C3알콕시, C1-C3알카노일, 시아노, 히드록시카르보닐, C1-C3알킬아미노카르보닐 및 페닐로 구성된 군으로부터 선택된 하나의 치환체에 의해 치환된 C1~C3알콕시, 또는 일반식 :-CH2O-R1,-CH=CH-R2, -CH=N-R3또는 -CO-R4알키닐기이고, R2는 시아노기, 메톡시카르보닐기 또는 아세틸기이고, R3은 디멜틸 아미노기 또는 페닐기이고, R4는 C1-C2알킬기이다)의 기이다.]
  5. 제 4항에 있어서, 부가적인 활성 성분으로서 최소한 하나의 벤즈이미다졸, 티오파네이트 및 고리형 이미드 살진규제를 더 함유함을 특징으로 하는 살진균 조성물.
  6. 제 5항에 있어서, 벤즈이미다졸, 티오파네이트 또는 고리형 아미드 살진균제가 메틸 1-(부틸카르바모일)벤즈이미다졸--2-일-카르바메이트, 2-(2-푸릴)벤즈아미다졸, 2-(4-티아졸릴)벤즈이미다졸, 메틸벤즈이미다졸-2-일카르바메이트, 1,2-비스(3-메톡시카르보닐-2-티오우레이도)벤젠, 1,2-비스(3-엑톡시카르보닐-2-티오우레이도)벤젠, 2-(O,O-디메티오포르포릴 아미노)-1-(3′-메톡시카르보닐-2′티오우레이도)벤젠이고 고리형 이미드 살진균제가 3-(3′,5′-디클로로페닐)-1,2-디메틸시클로프로판1,2-디카르복사미드, 3-(3′,5′-디클로로페닐)-1-이소프로필카르바모일 이미다졸리딘-2,4-디온, 3-(3′,5′-디클로로페닐)-5-메틸-5-비닐옥사졸린-2, 4-디온, 또는 에틸(RS)-3-(3′,5′-디클로로페닐)-5-메틸-2,4-디옥소옥사졸리딘-5-카르복실레이트임을 특징으로 하는 살진균 조성물.
  7. 제 4항에 있어서, 약제-내성을 갖는 식물병원성 진균에 대하여 효과적임을 특징으로 하는 살진균 조성물.
  8. 살진균학적으로 유효한 양의 최소한 하나의 하기 일반식(I)의 화합물을 식물 병원성 진균에 살포함을 특징으로 하는 식물 병원성 진균의 방제 방법.
    [상기 식중, X는 할로겐원자이고, Y는 C1-C4알킬기, C2-C4알케닐기, C1-C3알콕시기, C3-C4알케닐옥시기, C3-C4알키닐옥시기, 페닐에 의해 치환된 C2-C3알케닐기, 할로겐에 의해 치환된 C3-C4알케닐옥시기, 할로겐, C1-C3알콕시, C1-C3알카노일, 시아노, 히드록시카르보닐, C1-C3알킬아미노카르보닐 및 페닐로 구성된 군으로부터 선택된 하나의 치환체에 의해 치환된 C1-C3알콕시, 또는 일반식 :-CH2O-R1,-CH=CH-R2, -CH=N-R3또는 -CO-R4(식중, R1은 C1-C3알킬기, C3-C4알케닐기 또는 C3-C4알키닐기이고, R2는 시아노기, 메톡시카르보닐기 또는 아세틸기이고, R3은 디멜틸 아미노기 또는 페닐기이고, R4는 C1-C2알킬기이다)의 기이다.]
  9. 제 8항에 있어서, 식물 병원성 진균이 약재-내성 균주임을 특징으로 하는 방제 방법.
  10. 살진균학적으로 유효한 양의 최소한 하나의 하기 일반식(I)의 화합물 및 벤즈이미다졸, 티오페네이트 또는 고리형 이미드 살진균제를 식물 병원성 진균에 살포함을 특징으로 하는 식물 병원성 진균의 방제 방법.
    [상기 식중, X는 할로겐원자이고, Y는 C1-C4알킬기, C2-C4알케닐기, C1-C3알콕시기, C3-C4알케닐옥시기, C3-C4알키닐옥시기, 페닐에 의해 치환된 C2-C3알케닐기, 할로겐에 의해 치환된 C3-C4알케닐옥시기, 할로겐, C1-C3알콕시, C1-C3알카노일, 시아노, 히드록시카르보닐, C1-C3알킬아미노카르보닐 및 페닐로 구성된 군으로부터 선택된 하나의 치환체에 의해 치환된 C1-C3알콕시, 또는 일반식 :-CH2O-R1,-CH=CH-R2, -CH=N-R3또는 -CO-R4(식중, R1은 C1-C3알킬기, C3-C4알케닐기 또는 C3-C4알키닐기이고, R2는 시아노기, 메톡시카르보닐기 또는 아세틸기이고, R3은 디멜틸 아미노기 또는 페닐기이고, R4는 C1-C2알킬기이다)의 기이다.]
  11. 하기 일반식(I)의 화합물의 살진균제로서의 용도.
    [상기 식중, X는 할로겐원자이고, Y는 C1-C4알킬기, C2-C4알케닐기, C1-C3알콕시기, C3-C4알케닐옥시기, C3-C4알키닐옥시기, 페닐에 의해 치환된 C2-C3알케닐기, 할로겐에 의해 치환된 C3-C4알케닐옥시기, 할로겐, C1-C3알콕시, C1-C3알카노일, 시아노, 히드록시카르보닐, C1-C3알킬아미노카르보닐 및 페닐로 구성된 군으로부터 선택된 하나의 치환체에 의해 치환된 C1-C3알콕시, 또는 일반식 :-CH2O-R1,-CH=CH-R2, -CH=N-R3또는 -CO-R4(식중, R1은 C1-C3알킬기, C3-C4알케닐기 또는 C3-C4알키닐기이고, R2는 시아노기, 메톡시카르보닐기 또는 아세틸기이고, R3은 디멜틸 아미노기 또는 페닐기이고, R4는 C1-C2알킬기이다)의 기이다.]
  12. 하기 일반식(Ⅱ′)의 화합물을 프로파프길 할라이드와 반응시킴을 특징으로 하는 하기 일반식(Ⅰ´)의 화합물의 제조방법.
    [상기 식중, X는 할로겐원자이고, Y′는 C1-C4알킬기, C2-C4알케닐기, C1-C3알콕시기, C3-C4알케닐옥시기, C3-C4알키닐옥시기, 페닐에 의해 치환된 C2-C3알케닐기, 할로겐에 의해 치환된 C3-C4알케닐옥시기, 할로겐, C1-C3알콕시, C1-C3알카노일, 시아노, 히드록시카르보닐, C1-C3알킬아미노카르보닐 및 페닐로 구성된 군으로부터 선택된 하나의 치환체에 의해 치환된 C1-C3알콕시, 또는 일반식 : -CO-R4(식중, R4는 C1-C2알킬기이다)의 기이다.]
  13. 하기 일반식(Ⅲ)의 화합물을 일반식 : R5-Z의 화합물과 반응시킴을 특징으로 하는 하기 일반식(I-2)의 화합물의 제조방법.
    [상기 식중, X는 할로겐원자이고, R5는 C1-C3알킬기, C3-C4알케닐기,C3-C4알키닐기, 할로겐에 의해 치환된 C3-C4알케닐기, 할로겐, C1-C3알콕시, C1-C3알카노일, 시아노, 히드록시카르보닐, C1-C3알킬아미노카르보닐 및 페닐로 구성된 군으로부터 선택된 하나의 치환체에 의해 치환된 C1-C3알킬기이고, Z는 이탈기이다.]
  14. 하기 일반식(Ⅳ)의 화합물을 일반식 :@의 화합물 중 하나와 반응시킴을 특징으로 하는 하기 일반식(I-3)의 제조방법.
    [상기 식중, X는 할로겐원자이고, Y″는 C2-C4알케닐기,페닐에 의해 치환된 C2-C3알케닐기 또는 일반식 : -CH=CH-R2(식중 R2는 시아노기, 메톡시카르보닐기 또는 아세틸기이다)의 기이고, R6은 C1~C3알킬기, 페닐에 의해 치환된 C1~C2알킬기이고, R7은 저급 알킬기이고, Z′는 할로겐원자이다.]
  15. 하기 일반식(Ⅳ)의 화합물을 1,1-디메틸히드라진 또는 아닐린과 반응시킴을 특징으로 하기 일반식(I-4)의 화합물의 제조방법.
    [상기 식중, X는 할로겐원자이고, R3은 디멜틸아미노기 또는 페닐기이다.]
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019870008799A 1986-08-12 1987-08-11 디프로파프길옥시벤젠 화합물 및 그의 제조방법 KR880002790A (ko)

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JP18889286 1986-08-12
JP188892 1986-08-12
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JP21295586 1986-09-09
JP266458 1986-11-07
JP26645886 1986-11-07

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CA2036514A1 (en) * 1990-02-19 1991-08-20 Masahito Nakayama Azoxy compounds
GB9927056D0 (en) 1999-11-17 2000-01-12 Karobio Ab Thyroid receptor antagonists for the treatment of cardiac and metabolic disorders

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AU589241B2 (en) * 1985-12-27 1989-10-05 Sumitomo Chemical Company, Limited Dipropargyloxybenzene compounds and their production
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