KR850005016A - 알루미늄 전해 캐패시터용 고전압 박막의 에칭공정 - Google Patents
알루미늄 전해 캐패시터용 고전압 박막의 에칭공정 Download PDFInfo
- Publication number
- KR850005016A KR850005016A KR1019840008066A KR840008066A KR850005016A KR 850005016 A KR850005016 A KR 850005016A KR 1019840008066 A KR1019840008066 A KR 1019840008066A KR 840008066 A KR840008066 A KR 840008066A KR 850005016 A KR850005016 A KR 850005016A
- Authority
- KR
- South Korea
- Prior art keywords
- thin film
- high voltage
- etching process
- aluminum
- aluminum electrolytic
- Prior art date
Links
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title claims description 13
- 229910052782 aluminium Inorganic materials 0.000 title claims description 13
- 239000010409 thin film Substances 0.000 title claims description 13
- 239000003990 capacitor Substances 0.000 title claims description 10
- 238000005530 etching Methods 0.000 title claims 9
- 238000000034 method Methods 0.000 title claims 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims 2
- 238000007796 conventional method Methods 0.000 description 1
- 238000001878 scanning electron micrograph Methods 0.000 description 1
- 238000004626 scanning electron microscopy Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/004—Details
- H01G9/04—Electrodes or formation of dielectric layers thereon
- H01G9/048—Electrodes or formation of dielectric layers thereon characterised by their structure
- H01G9/055—Etched foil electrodes
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25F—PROCESSES FOR THE ELECTROLYTIC REMOVAL OF MATERIALS FROM OBJECTS; APPARATUS THEREFOR
- C25F3/00—Electrolytic etching or polishing
- C25F3/02—Etching
- C25F3/04—Etching of light metals
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Power Engineering (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Electrochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microelectronics & Electronic Packaging (AREA)
- ing And Chemical Polishing (AREA)
- Fixed Capacitors And Capacitor Manufacturing Machines (AREA)
- Manufacturing Of Printed Circuit Boards (AREA)
- Electrolytic Production Of Metals (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도 및 제3도는 터넘 구조를 보이는, 종래의 방법으로 에칭된 알루미늄 커패시터 박막의 일부분의 회단면에 대한 SEM(주사전자 현미경) 사진.
제2도 및 제3도는 비교적 곧은 연장터널 구조체를 보이는, 본 발명에 따라 에칭된 알루미늄 커패시터 박막의 일부분의 횡단면에 대한 SEM 사진.
Claims (7)
- 직류의 영향하에서 알루미늄 전해 캐패시터 고전압 박막을 전해조에 통과시킴으로써 상기 박막을 에칭하는 공정으로서, 하이큐빅 구조를 갖는 박막은 70C/㎠ 내지 110C/㎠의 전하를 통과시키는 동안 70℃와 85℃ 사이의 온도에서 1.5 %내지 7%의 염산과 염화물로서 최고 2%의 알루미늄을 포함하는 전해조를 통과하는 것을 특징으로 하는 알루미늄 전해 커패시터용 고전압 박막의 에칭공정.
- 제1항에 있어서, 상기 알루미늄 박막의 두께는 100㎛이고 입방도가 70%나 그 이상인 것을 특징으로 하는 알루미늄 전해 커패시터용 고전압 박막의 에칭공정.
- 제1항에 있어서, 전해조에서의 염산의 농도는 3%인 것을 특징으로 하는 알루미늄 전해 커패시터용 고전압 박막의 에칭공정.
- 제1항에 있어서, 상기 전해조에서의 염화물로서의 알루미늄의 농도는 1%인 것을 특징으로 하는 알루미늄 전해 커패시터용 고전압 박막의 에칭공정.
- 제1항에 있어서, 상기 전해조의 온도는 75℃인 것을 특징으로 하는 알루미늄 전해 커패시터용 고전압 박막의 에칭공정.
- 제1항에 있어서, 전류밀도는 0.13A/㎠ 내지 0.85A/㎠의 범위에 있는 것을 특징으로 하는 알루미늄 전해 커패시터용 고전압 박막의 에칭공정.
- 제1항에 있어서, 에치쿨통은 80C/㎠과 90C/㎠ 사이의 범위에 있는 것을 특징으로 하는 안루미늄 전해 커패시터용 고전압 박막의 에칭공정.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US563,345 | 1983-12-20 | ||
US06/563,345 US4474657A (en) | 1983-12-20 | 1983-12-20 | Single step electro chemical etch process for high volt aluminum anode foil |
US563345 | 1983-12-20 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR850005016A true KR850005016A (ko) | 1985-08-19 |
KR910009167B1 KR910009167B1 (ko) | 1991-10-31 |
Family
ID=24250139
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019840008066A KR910009167B1 (ko) | 1983-12-20 | 1984-12-18 | 알루미늄 전해 커패시터용 고전압 박지의 에칭 공정 |
Country Status (5)
Country | Link |
---|---|
US (1) | US4474657A (ko) |
EP (1) | EP0147896B1 (ko) |
JP (1) | JPS6123798A (ko) |
KR (1) | KR910009167B1 (ko) |
DE (1) | DE3469572D1 (ko) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4525249A (en) * | 1984-07-16 | 1985-06-25 | North American Philips Corporation | Two step electro chemical and chemical etch process for high volt aluminum anode foil |
US4518471A (en) * | 1984-08-29 | 1985-05-21 | North American Philips Corporation | Two step electrochemical etch process for high volt aluminum anode foil |
JP2787801B2 (ja) * | 1994-03-10 | 1998-08-20 | 日本蓄電器工業株式会社 | 電解コンデンサ用アルミニウム電極箔のエッチング方法 |
FR2755111B1 (fr) * | 1996-10-28 | 1998-12-31 | Ceric | Dispositif pour le transport de produits ceramiques |
US6168706B1 (en) | 1998-12-11 | 2001-01-02 | Pacesetter, Inc. | Process for producing high etch gains for electrolytic capacitor manufacturing |
US6238810B1 (en) | 1999-04-07 | 2001-05-29 | Pacesetter, Inc. | Process for using surface active agents to produce high etch gains for electrolytic capacitor manufacturing |
US6224738B1 (en) | 1999-11-09 | 2001-05-01 | Pacesetter, Inc. | Method for a patterned etch with electrolytically grown mask |
US6325551B1 (en) | 1999-12-08 | 2001-12-04 | New Focus, Inc. | Method and apparatus for optically aligning optical fibers with optical devices |
US6736956B1 (en) | 2001-05-07 | 2004-05-18 | Pacesetter, Inc. | Non-uniform etching of anode foil to produce higher capacitance gain without sacrificing foil strength |
US6858126B1 (en) | 2002-11-06 | 2005-02-22 | Pacesetter, Inc. | High capacitance anode and system and method for making same |
US7452473B1 (en) | 2003-10-06 | 2008-11-18 | Pacesetter, Inc. | Laser marking of raw aluminum anode foil to induce uniform patterning etching |
US7150767B1 (en) | 2003-11-03 | 2006-12-19 | Pacesetter, Inc. | Method for producing an electrode for a capacitor from foil |
US7578924B1 (en) | 2004-07-29 | 2009-08-25 | Pacesetter, Inc. | Process for producing high etch gains for electrolytic capacitor manufacturing |
US7445646B1 (en) | 2004-08-06 | 2008-11-04 | Pacesetter, Inc. | Method of producing an anode for an electrolytic capacitor |
US8535507B1 (en) | 2008-01-11 | 2013-09-17 | Pacesetter, Inc. | Electrochemical drilling system and process for improving electrical porosity of etched anode foil |
US8206600B2 (en) * | 2008-09-15 | 2012-06-26 | Pacesetter, Inc. | Nanoimprinting of an optic to control the etch pattern on electrolytic capacitor foil |
US9090986B1 (en) | 2014-01-30 | 2015-07-28 | Pacesetter, Inc. | Method for making electrode foils having reduced particle detachment and reduced leakage current |
CN104630871B (zh) * | 2015-01-13 | 2017-08-18 | 肇庆华锋电子铝箔股份有限公司 | 一种低压硬质高比容铝电极箔的腐蚀工艺方法 |
US10072349B2 (en) | 2016-01-05 | 2018-09-11 | Pacesetter, Inc. | Etch solutions having bis(perfluoroalkylsulfonyl)imides, and use thereof to form anode foils with increased capacitance |
US9978529B2 (en) | 2016-01-11 | 2018-05-22 | Pacesetter, Inc. | Oxide on edges of metal anode foils |
US10090112B2 (en) | 2016-01-15 | 2018-10-02 | Pacesetter, Inc. | Use of etch resist masked anode frame for facilitation of laser cutting, particle and leakage current reduction |
US9969030B2 (en) | 2016-05-12 | 2018-05-15 | Pacesetter, Inc. | Laser drilling of metal foils for assembly in an electrolytic capacitor |
US9852849B2 (en) | 2016-05-27 | 2017-12-26 | Pacesetter, Inc. | Using etch resist patterns and formation for facilitation of laser cutting, particle and leakage current reduction |
US9976226B2 (en) | 2016-07-28 | 2018-05-22 | Pacesetter, Inc. | Method of stressing oxides |
US10309033B2 (en) | 2016-12-02 | 2019-06-04 | Pacesetter, Inc. | Process additives to reduce etch resist undercutting in the manufacture of anode foils |
US10240249B2 (en) | 2016-12-02 | 2019-03-26 | Pacesetter, Inc. | Use of nonafluorobutanesulfonic acid in a low pH etch solution to increase aluminum foil capacitance |
US10422050B2 (en) | 2016-12-02 | 2019-09-24 | Pacesetter, Inc. | Process for using persulfate in a low pH etch solution to increase aluminum foil capacitance |
US10894157B2 (en) | 2017-04-04 | 2021-01-19 | Pacesetter, Inc. | Laser marking of raw anode foil to induce uniform pattering and etching with oxide passivation mask |
CN110729130B (zh) * | 2019-09-11 | 2021-04-06 | 南通南辉电子材料股份有限公司 | 一种适用于小片宽电极箔生产的化成方法 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2209712A (en) * | 1937-05-06 | 1940-07-30 | Joseph B Brennan | Method of treating aluminum |
GB966627A (en) * | 1962-04-09 | 1964-08-12 | British Dielectric Res Ltd | Improvements in or relating to the electrolytic etching of anodisable metal foil |
CH578781A5 (ko) * | 1973-07-09 | 1976-08-13 | Alusuisse | |
JPS5125439A (ko) * | 1974-08-28 | 1976-03-02 | Fujitsu Ltd | |
JPS5264659A (en) * | 1975-11-21 | 1977-05-28 | Nippon Chikudenki Kougiyou Kk | Method of etching aluminum foil for electrolytic capacitor |
JPS5479462A (en) * | 1977-12-06 | 1979-06-25 | Showa Aluminium Co Ltd | Aluminium alloy foil for electrolyte capacitor anode |
DE2801218C3 (de) * | 1978-01-12 | 1980-11-20 | Siemens Ag, 1000 Berlin Und 8000 Muenchen | Verfahren zum elektrolytischen Ätzen einer rekristallisierten Aluminiumfolie und deren Verwendung |
US4201836A (en) * | 1978-08-28 | 1980-05-06 | Polychrome Corporation | Aluminum substrates grained with a saturated solution of aluminum salts of mineral acids |
US4315806A (en) * | 1980-09-19 | 1982-02-16 | Sprague Electric Company | Intermittent AC etching of aluminum foil |
JPS5766618A (en) * | 1980-10-13 | 1982-04-22 | Showa Aluminium Co Ltd | Aluminum alloy foil for electrolytic condenser electrode |
JPS5766617A (en) * | 1980-10-13 | 1982-04-22 | Showa Aluminium Co Ltd | Aluminum alloy foil for electrolytic condenser electrode |
JPS5766616A (en) * | 1980-10-13 | 1982-04-22 | Showa Aluminium Co Ltd | Method of producing alumihum foil for electrolytic condenser electrode |
US4332652A (en) * | 1980-11-28 | 1982-06-01 | Sprague Electric Company | AC Etching of aluminum capacitor foil |
JPS6059982B2 (ja) * | 1980-12-09 | 1985-12-27 | 昭和アルミニウム株式会社 | 電解コンデンサ電極用アルミニウム箔の製造方法 |
US4332651A (en) * | 1981-05-20 | 1982-06-01 | Sprague Electric Company | AC Etching of aluminum capacitor foil |
US4336113A (en) * | 1981-06-26 | 1982-06-22 | American Hoechst Corporation | Electrolytic graining of aluminum with hydrogen peroxide and nitric or hydrochloric acid |
JPS5757856A (en) * | 1981-07-24 | 1982-04-07 | Showa Alum Corp | Aluminum alloy foil for electrolytic capacitor |
US4376686A (en) * | 1981-11-16 | 1983-03-15 | Sprague Electric Company | AC Etching of aluminum capacitor foil |
-
1983
- 1983-12-20 US US06/563,345 patent/US4474657A/en not_active Expired - Lifetime
-
1984
- 1984-12-17 DE DE8484201882T patent/DE3469572D1/de not_active Expired
- 1984-12-17 EP EP84201882A patent/EP0147896B1/en not_active Expired
- 1984-12-18 KR KR1019840008066A patent/KR910009167B1/ko not_active IP Right Cessation
- 1984-12-18 JP JP26549384A patent/JPS6123798A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
DE3469572D1 (en) | 1988-04-07 |
KR910009167B1 (ko) | 1991-10-31 |
JPH0551680B2 (ko) | 1993-08-03 |
EP0147896B1 (en) | 1988-03-02 |
US4474657A (en) | 1984-10-02 |
JPS6123798A (ja) | 1986-02-01 |
EP0147896A1 (en) | 1985-07-10 |
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