KR20210103360A - Natural cleaning material manufacturing method - Google Patents
Natural cleaning material manufacturing method Download PDFInfo
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- KR20210103360A KR20210103360A KR1020200043538A KR20200043538A KR20210103360A KR 20210103360 A KR20210103360 A KR 20210103360A KR 1020200043538 A KR1020200043538 A KR 1020200043538A KR 20200043538 A KR20200043538 A KR 20200043538A KR 20210103360 A KR20210103360 A KR 20210103360A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0047—Detergents in the form of bars or tablets
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/10—Salts
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/20—Water-insoluble oxides
Abstract
Description
본 발명은 천연 세탁 조성물 제조방법에 관한 것으로, 보다 상세하게 세정 및 살균, 섬유유연성이 우수한 건조염을 담체로 하고, 수질 개선과 항균 효과를 갖춘 천연 활성 산화칼슘을 패각류부터 추출하며, 코코넛 열매 및 팜열매, 소프넛 열매로부터 추출한 알콜 및 지방산과 당을 이용한 천연계 계면활성제를 이용하여 세균 및 미생물의 번식을 전면 차단하고, 우수한 살균과 수질 개선의 기능을 갖도록 한 천연 세탁 조성물 제조방법에 관한 것이다.The present invention relates to a method for preparing a natural laundry composition, and more particularly, to a method for washing and sterilizing, using a dry salt excellent in fabric flexibility as a carrier, and extracting natural active calcium oxide having water quality improvement and antibacterial effect from shellfish, and coconut fruit And it relates to a method of manufacturing a natural laundry composition that completely blocks the growth of bacteria and microorganisms by using a natural surfactant using alcohol, fatty acid, and sugar extracted from palm fruit and soapnut fruit, and has excellent sterilization and water quality improvement functions. .
주지된 바와 같이, 종래의 세탁 세제는 그 유효성분으로 알킬벤젠술폰산나트륨, 알킬술폰산나트륨, 알파올레핀술폰나트륨 등의 음이온 계면활성제와 폴리 옥시에틸렌 알킬페놀에테르, 폴리 옥시에틸렌 알킬에테르, 폴리 옥시에틸렌 알킬에스테르 등을 포함하는 비이온 계면활성제가 주로 사용되고 있으며, 그 유효 성분에 관한 설명 및 예는 미국특허 제3,929,678호 및 유럽특허 제0,241,984호에 잘 나타나 있다.As is well known, conventional laundry detergents include anionic surfactants such as sodium alkylbenzenesulfonate, sodium alkylsulfonate, sodium alpha olefinsulfonate, and polyoxyethylene alkylphenol ether, polyoxyethylene alkyl ether, and polyoxyethylene alkyl as active ingredients. Nonionic surfactants including esters are mainly used, and descriptions and examples of their active ingredients are well shown in US Patent No. 3,929,678 and European Patent No. 0,241,984.
그리고, 분말 세제 제조시 사용되는 주 계면활성제로서 알칸술폰산염이 쓰이고, 거기에다 알파 올레핀 술폰산나트륨과 인산염을 함께 첨가하여 사용하는 내용이 독일 특허 제2,355,788호에 기술되어 있다.In addition, as the main surfactant used in manufacturing powder detergent, an alkanesulfonate is used, and the content of using it by adding sodium alpha olefin sulfonate and phosphate together is described in German Patent No. 2,355,788.
그러나, 이와 같이 조성된 세탁용 분말 세제는 수질오염 문제로 인해 우리나라를 비롯한 각국에서 사용이 부적합 것으로, 그 이유는 이와 같은 술폰산염 형태의 음이온 계면활성제를 주성분으로 하고 있는 분말 세제의 경우, 부영양화 등의 환경오염을 유발시키며, 세탁 후 세탁물에 잔류물이 남아 피부에 자극을 주기 때문이다.However, the powder detergent for laundry formulated in this way is not suitable for use in countries including Korea due to water pollution problems. This is because, after washing, residues remain in the laundry and irritate the skin.
즉 환경 보호 및 연약 피부나 유아용 세탁 세제로의 사용의 부적합하다는 문제가 있었다.That is, there was a problem in that it is not suitable for environmental protection and use as a laundry detergent for delicate skin or infants.
따라서, 최근에 와서는 친환경적인 세탁물질이라는 세제가 제조 판매되고 있지만 화학성분이 들어가지 않은 세제는 존재하지 않는다.Therefore, recently, detergents called eco-friendly laundry materials have been manufactured and sold, but detergents without chemical components do not exist.
사용자들도 값이 싸고 편리한 사용방법 때문에 화학세제를 사용하는 것이 일반적이다.It is common for users to use chemical detergents because of its low cost and convenient use.
그러나, 종래의 화학 세탁세제는 세탁 후에도 화학성분이 섬유 속에 남아서 인체의 피부에 피해를 주고 각종 피부질환, 가려움증, 아토피 피부염 등을 일으키는 단점이 있다.However, conventional chemical laundry detergents have disadvantages in that chemical components remain in the fibers even after washing, causing damage to the skin of the human body and causing various skin diseases, itchiness, atopic dermatitis, and the like.
또한, 세탁한 폐수는 하천과 강과 바다를 오염시켜 환경을 파괴하는 단점이 있으며, 폐수를 처리하는 데에는 막대한 비용이 들어가는 문제점이 있다.In addition, the washed wastewater pollutes rivers, rivers, and the sea, thereby destroying the environment, and there is a problem in that a huge cost is incurred in treating the wastewater.
또, 종래의 화학세제는 하천오염으로 인한 2차 피해 인체에 악영향을 미쳐 그 피해를 처리하는데 막대한 사회적 비용이 투입되야 한다는 문제가 있었다.In addition, there was a problem that conventional chemical detergents have a negative effect on the human body due to secondary damage caused by river pollution, so that enormous social costs must be invested in dealing with the damage.
본 발명은 상기한 종래 기술의 사정을 감안하여 이루어진 것으로, 세정 및 살균, 섬유유연성이 우수한 건조염을 담체로 하고, 수질 개선과 항균 효과를 갖춘 천연 활성 산화칼슘을 패각류부터 추출하며, 코코넛 열매 및 팜열매, 소프넛 열매로부터 추출한 알콜 및 지방산과 당을 이용한 천연계 계면활성제를 이용하여 세균 및 미생물의 번식을 전면 차단하고, 우수한 살균과 수질 개선의 기능을 갖도록 한 천연 세탁 조성물 제조방법을 제공함에 그 목적이 있다. The present invention has been made in view of the circumstances of the prior art, and is obtained by extracting natural active calcium oxide from shellfish with a dry salt excellent in cleaning and sterilization and fiber flexibility as a carrier, improving water quality and having an antibacterial effect, and extracting coconut fruit. And by using a natural surfactant using alcohol, fatty acid and sugar extracted from palm fruit and soapnut fruit to completely block the growth of bacteria and microorganisms, and to provide a method for producing a natural laundry composition that has excellent sterilization and water quality improvement functions. There is a purpose.
상기한 목적을 달성하기 위해, 본 발명의 바람직한 실시예에 따르면 a) 어패류의 패각류 껍질을 1000 내지 1500℃의 열처리과정으로 가열하여 천연 활성 산화칼슘을 얻는 단계와; b) 1000℃로 가열하여 조해성물질이 제거된 건조염을 얻는 단계와; c) 상기 건조염 100 중량％에 대해, 상기 천연 활성 산화칼슘 2 내지 5 중량％를 혼합하는 단계와; d) 상기 건조염 100 중량％에 대해, 코코넛 열매분말 5～10중량％를 혼합하고, 소프넛 열매분말과, 팜 열매분말, 베이킹소다, 레몬으로 이루어진 추가 혼합물을 5 중량％ 내지 20중량％를 혼합하는 단계를 포함하여 이루어진 천연 세탁 조성물 제조방법이 제공된다.In order to achieve the above object, according to a preferred embodiment of the present invention, a) heating the shellfish shells of fish and shellfish to a heat treatment process of 1000 to 1500 ℃ to obtain a natural active calcium oxide; b) heating to 1000° C. to obtain a dried salt from which deliquescent substances are removed; c) mixing 2 to 5% by weight of the natural active calcium oxide with respect to 100% by weight of the dry salt; d) With respect to 100% by weight of the dry salt, 5 to 10% by weight of coconut fruit powder is mixed, and 5 to 20% by weight of an additional mixture consisting of soapnut fruit powder, palm fruit powder, baking soda and lemon A method for preparing a natural laundry composition comprising the step of mixing is provided.
바람직하게, 상기 d) 과정의 다음으로, 일정 량의 단위로 압착 성형하여 세탁 고형물을 형성하는 단계가 더 포함된 것을 특징으로 하는 천연 세탁 조성물 제조방법이 제공된다.Preferably, after step d), there is provided a method for producing a natural laundry composition, characterized in that the step of forming a laundry solid by compression molding in a unit of a predetermined amount is further included.
바람직하게, 상기 a) 과정을 통해 제조된 활성 산화칼슘 분말 입자는 500 메쉬 이상인 것을 특징으로 하는 천연 세탁 조성물 제조방법이 제공된다.Preferably, there is provided a method for producing a natural laundry composition, characterized in that the active calcium oxide powder particles prepared through the process a) is 500 mesh or more.
바람직하게, 상기 b) 과정을 통해 제조된 건조염 분말 입자는 35 메쉬 이상인 것을 특징으로 하는 천연 세탁 조성물 제조방법이 제공된다.Preferably, there is provided a method for producing a natural laundry composition, characterized in that the dry salt powder particles prepared through the process b) are 35 mesh or more.
바람직하게, 상기 d) 과정에서, 상기 추가 혼합물은 소프넛 열매분말 2～8중량％, 팜 열매분말 1～5중량％, 베이킹소다 1～4중량％, 레몬 1～3중량％로 이루어진 것을 특징으로 하는 천연 세탁 조성물 제조방법이 제공된다. Preferably, in step d), the additional mixture is composed of 2 to 8% by weight of softwood fruit powder, 1 to 5% by weight of palm fruit powder, 1 to 4% by weight of baking soda, and 1 to 3% by weight of lemon. A method for preparing a natural laundry composition is provided.
본 발명에 따른 천연 세탁 조성물 제조방법은 인체에 해가 없으며, 2차로 물을 오염시키지 않고 특히 어린이들의 피부에 안전하며 세탁이나 입욕에 사용하여도 안전한 세탁세제 및 입욕제를 제공할 수 있다는 장점이 있다.The natural laundry composition manufacturing method according to the present invention has the advantage of being able to provide a laundry detergent and bathing agent that is harmless to the human body, does not contaminate water secondary, is safe especially for children's skin, and is safe even for washing or bathing. .
도 1은 본 발명의 일실시예에 따른 천연 세탁 조성물 제조공정을 도시한 공정도,
도 2는 본 발명의 일실시예에 따른 천연 세탁 조성물의 형광증백제 검출시험표,
도 3은 본 발명의 일실시예에 따른 천연 세탁 조성물의 세척효과에 대한 시험표이다. 1 is a process diagram illustrating a process for manufacturing a natural laundry composition according to an embodiment of the present invention;
2 is a fluorescent whitening agent detection test table of a natural laundry composition according to an embodiment of the present invention;
3 is a test table for the washing effect of a natural laundry composition according to an embodiment of the present invention.
이하, 본 발명에 대해 도면을 참조하여 상세하게 설명한다.Hereinafter, the present invention will be described in detail with reference to the drawings.
본 발명의 일실시예에 따른 천연 세탁 조성물은 활성 산화칼슘과, 정제된 건조염, 베이킹 소다와 천연 계면 활성제의 혼합과 분말화 단계를 거쳐 생성되는 천연 세탁 조성물이다.A natural laundry composition according to an embodiment of the present invention is a natural laundry composition produced by mixing and pulverizing active calcium oxide, purified dry salt, baking soda, and a natural surfactant.
먼저, 상기 활성 산화칼슘은 연안에 있는 패각류(굴껍질, 조개껍질전체, 소라껍질, 전복껍질 등)를 수거하고, 그 패각류 표면에 붙어있는 이물질을 제거하기 위하여 고압호스를 이용하여 세척한다.First, the activated calcium oxide collects shellfish (oyster shells, whole shells, conch shells, abalone shells, etc.) on the coast, and washes them using a high-pressure hose to remove foreign substances attached to the surface of the shellfish. .
그리고, 세척된 패각류를 마이크로 웨이브파 또는 가스, 전기, 석유 등을 원료로 하는 가열로에 투입하고, 내부의 온도를 최고온도 1000℃ 내지 1,500℃ 범위에서 6시간 가량 가열한다.(소성가공공정)Then, the washed shellfish are put into a heating furnace using microwave waves or gas, electricity, petroleum, etc. as raw materials, and the internal temperature is heated at a maximum temperature of 1000°C to 1,500°C for about 6 hours. (Plastic processing process )
상기 소성 가공 후 가열로에서 나온 패각류를 냉각시킨 후, 500 메쉬 이상의 입자로 분쇄하여 분말화한다.After cooling the shellfish from the heating furnace after the plastic processing, it is pulverized into particles of 500 mesh or more.
이렇게 제조된 활성 산화칼슘은 각종 세균과 곰팡이균을 억제시키는 항균 및 살균 작용을 한다.Activated calcium oxide prepared in this way has antibacterial and bactericidal action that inhibits various bacteria and fungi.
상기 건조염은 이온교환막을 통하여 염화나트륨만 추출한 순도가 99% 이상의 소금이고, 천일염에 열을 가하여 조해성 물질을 제거한 소금이다.The dried salt is a salt having a purity of 99% or more obtained by extracting only sodium chloride through an ion exchange membrane, and is a salt obtained by removing deliquescent substances by applying heat to sea salt.
상기 건조염은 천일염을 1000℃에서 4시간가량 가열하여 유기물과 비소, 산화물, 카드뮴, 납, 내화성 유기물을 제거함으로써 제조되고, 입자는 35메쉬가 되게 한다.The dried salt is prepared by heating sea salt at 1000° C. for about 4 hours to remove organic matter, arsenic, oxide, cadmium, lead, and refractory organic matter, and the particle size is 35 mesh.
이러한 건조염은 세정 및 살균 기능이 있으며, 섬유 유연성을 제공하는 기능을 구비하고 있다.These dried salts have cleaning and sterilization functions, and have a function of providing fiber flexibility.
한편, 본 발명의 일실시예에 따른 천연 세탁 조성물은 천연 계면활성제가 구성요소로 포함되는 바, 본 발명에서의 천연 계면활성제는 코코넛 열매 및 팜열매, 소프넛 열매로부터 추출한 알콜 및 지방산과 당을 이용한 천연계 계면활성제이다.On the other hand, the natural laundry composition according to an embodiment of the present invention contains a natural surfactant as a component, and the natural surfactant in the present invention contains alcohol, fatty acids and sugar extracted from coconut fruit, palm fruit, and soapnut fruit. It is a natural surfactant used.
코코넛 열매는 코코야자에서 채취하는 오일로 섭씨 25℃ 이상에서는 액체 상태로 유지되지만, 그 이하의 온도에서는 백색의 고체 상태이고, 거품이 풍부하게 나도록 하며 피부에 수분을 공급하여 안정화시키는 작용과 함께 비누를 단단하게 만드는 역할을 한다.Coconut fruit is an oil harvested from the coco palm, which is maintained in a liquid state at 25°C or higher, but is in a white solid state at a temperature below that, and creates abundant foam and provides moisture to the skin and stabilizes the soap. plays a role in making the
팜열매는 지방산 유지로서 비누가 단단해지도록 해주며, 조밀한 거품이 일어나게 하고, 올레산이 포함되어있어 보습에도 도움을 준다.The palm fruit is a fatty acid oil that makes the soap firm, creates a dense foam, and contains oleic acid to help moisturize.
소프넛 열매는 우수한 세정력과 유연 효과를 동시에 나타내며, 중성에 가까운 pH를 나타내어 옷감 손상이나 피부 자극이 적어 친환경 섬유 유연 기능성 물질이다.Soapnut fruit exhibits excellent cleaning power and softening effect at the same time, and has a pH close to neutral, so it is an eco-friendly fabric softening functional material with less damage to the fabric and less irritation to the skin.
베이킹소다는 널리 알려진 바와같이, 세척, 중화, 표백, 연수, 연마, 탈취기능을 보유하고 있다.Baking soda has cleaning, neutralization, bleaching, softening, polishing, and deodorizing functions, as is widely known.
<실시예><Example>
먼저, 어패류와, 천일염 및 소프넛 열매와 팜열매, 코코넛 열매, 베이킹 소다와 같은 재료를 준비하는 과정을 수행하였다.First, a process of preparing ingredients such as seafood, sea salt, soapnut fruit, palm fruit, coconut fruit, and baking soda was performed.
어패류의 경우, 연안에 있는 패각류(굴껍질, 조개껍질전체, 소라껍질, 전복껍질 등)를 수거하고, 그 패각류 표면에 붙어있는 이물질을 제거하기 위하여 고압호스를 이용하여 세척한다.In the case of seafood, shellfish (oyster shells, whole shellfish shells, conch shells, abalone shells, etc.) from the coast are collected and washed using a high-pressure hose to remove foreign substances attached to the surface of the shellfish.
그리고, 세척된 패각류를 마이크로 웨이브파 또는 가스, 전기, 석유 등을 원료로 하는 가열로에 투입하고, 내부의 온도를 최고온도 1000℃ 내지 1,500℃ 범위에서 6시간 가량 가열한다.(소성가공공정)Then, the washed shellfish are put into a heating furnace using microwave waves or gas, electricity, petroleum, etc. as raw materials, and the internal temperature is heated at a maximum temperature of 1000°C to 1,500°C for about 6 hours. (Plastic processing process )
상기 소성 가공 후 가열로에서 나온 패각류를 냉각시킨 후, 500 메쉬 이상의 입자로 분쇄하여 분말화하였으며, 그렇게 얻은 천연 활성 산화칼슘은 5ｇ이 되게 하였다.After cooling the shellfish from the heating furnace after the plastic processing, it was pulverized into particles of 500 mesh or more and powdered, and the thus obtained natural active calcium oxide was 5 g.
이어서, 준비된 천일염을 이온교환막을 통하여 염화나트륨만 추출한 순도 99% 이상의 염화나트륨으로 이루어지게 한 다음, 1000℃에서 4시간가량 가열하여 유기물과 비소, 산화물, 카드뮴, 납, 내화성 유기물 등의 조해성 물질을 제거한다.Next, the prepared sea salt is made of sodium chloride with a purity of 99% or more extracted only with sodium chloride through an ion exchange membrane, and then heated at 1000° C. for about 4 hours to remove organic substances, arsenic, oxide, cadmium, lead, and deliquescent substances such as refractory organic substances. .
이때는 용융염 상태이지만, 냉각시키고, 입자는 35메쉬가 되게 분쇄하여 분말처리하고, 그렇게 얻은 건조염은 80ｇ이 되게 하고, 상기 천연 활성 산화칼슘 5ｇ을 혼합한다.At this time, it is in a molten salt state, but it is cooled, the particles are pulverized to 35 mesh, and the dried salt thus obtained is 80 g, and 5 g of the natural active calcium oxide is mixed.
그리고, 천연 계면활성제의 구성이 되는 혼합물을 15ｇ혼합한다.Then, 15 g of the mixture constituting the natural surfactant is mixed.
상기 혼합물은 코코넛 열매 7ｇ과, 추가 혼합물로 이루어진다.The mixture consists of 7 g of coconut fruit and a further mixture.
추가 혼합물은 소프넛 열매를 6ｇ, 팜 열매분말 3ｇ, 베이킹소다 3ｇ, 레몬 2ｇ을 준비하고, 분쇄기로 분쇄하여 입자는 35메쉬가 되게 분말처리한다.For the additional mixture, prepare 6g of soap nut, 3g of palm fruit powder, 3g of baking soda, and 2g of lemon, and pulverize it with a grinder to make 35 mesh particles.
다음으로, 상기 건조염과 천연 활성 산화칼슘이 혼합된 혼합물에 상기 천연 계면활성제 분말을 투입하여 혼합한다. 혼합은 통상의 믹서기를 통해 혼합하여도 무방하다.Next, the natural surfactant powder is added to a mixture of the dried salt and natural active calcium oxide and mixed. Mixing may be mixed through a conventional mixer.
상기 과정을 통해 제조된 상기 천연 세탁물 조성분말을 약 2ｇ단위로 압착 성형하여 세탁 고형물을 제작한다. 세탁 고형물은 입욕제로도 사용할 수 있으며, 형태는 동전모양, 꽃모양, 원구모양 등 금형의 형태에 따라 다양하게 제품화할 수있다.The natural laundry composition powder prepared through the above process is press-molded into about 2 g to produce a laundry solid. Washing solids can also be used as bathing agents, and the shape can be manufactured in various ways depending on the shape of the mold, such as coin shape, flower shape, or sphere shape.
한편, 이때, 본 발명의 일실시예에 따른 천연 세탁 조성물은 일정 단위의 분말 또는 고형물 또는 액상 형태로 성형하는 단계를 더 거치면서 다양한 형태의 조성물로 제조 가능한 바, 소비자의 사용처나 사용환경에 따라 자유롭게 천연 세탁 조성물의 형태를 선택해서 사용할 수 있다.On the other hand, at this time, the natural laundry composition according to an embodiment of the present invention can be manufactured into a composition of various types while further undergoing the step of molding into a powder or solid or liquid form of a certain unit. You can freely choose the type of natural laundry composition and use it.
또한, 본 발명의 일실시예에 따른 천연 세탁 조성물은 대조균들에 대한 세척 및 살균효과를 갖추고 있으면서 인체에 무해한 조성물이므로 손세정제, 샴푸, 린스, 주방세제, 과일세정제 등으로 광범위하게 사용 가능하다.In addition, the natural laundry composition according to an embodiment of the present invention is a composition that is harmless to the human body while having a cleaning and sterilizing effect on control bacteria, so it can be widely used as hand sanitizer, shampoo, conditioner, dishwashing detergent, fruit cleaner, etc. .
<실험예 1><Experimental Example 1>
살균 효과의 측정Determination of bactericidal effect
본 발명에 따른 천연 세탁 조성물을 한국 의류시험 연구원에 항균효과를 측정하였으며, 시험방법은 용기 내부에 배양한 균을 준비하고, 다른 용기에는 본 발명의 시료를 균과 함께 투입하여 5분 후 대조시료와 시험시료의 균수를 비교하여 균의 감소율을 측정하였다.The antibacterial effect of the natural laundry composition according to the present invention was measured by the Korea Apparel Testing Research Institute, and the test method was to prepare the cultured bacteria in a container, and put the sample of the present invention together with the bacteria in another container, and after 5 minutes, a control sample The reduction rate of bacteria was measured by comparing the number of bacteria with the test sample.
1. 시험조건1. Test conditions
1) 시험균: Escherichia coli ATCC 259221) Test bacteria: Escherichia coli ATCC 25922
2) 배지: Nutrient broth/Tryptic soy agar2) Medium: Nutrient broth/Tryptic soy agar
3) 시험균의 준비: 0.85％ Nacl3) Preparation of test bacteria: 0.85% Nacl
4) 초기균 농도: 1.6× 106 CFU/mL4) Initial bacterial concentration: 1.6×10 6 CFU/mL
5) 대조편: 멸균 증류수5) Control: sterile distilled water
6) 시료의 종류 및 농도: Tablet, 0.26ｇ/L6) Sample type and concentration: Tablet, 0.26 g/L
7) 접촉시간 및 조건: 5min, (25± 1)℃, 200 r/min shaking7) Contact time and conditions: 5min, (25± 1)℃, 200 r/min shaking
8) 중화용액: D/E broth8) Neutralization solution: D/E broth
2. 살균력(％): [(A－B)/A]× 1002. Sterilization power (%): [(A-B)/A] × 100
(A: 초기균수, B: 접촉후 시험편의 균수)(A: Initial number of bacteria, B: Number of bacteria on test piece after contact)
3. 시험결과3. Test results
살균력(％): ASTM E 2315:2016Sterilization (%): ASTM E 2315:2016
8.78.7
이상에서 살펴본 바와 같이, 본 발명에 따른 천연 세탁 조성물은 매우 짧은 시간인 5분동안 시료와 대조군을 측정해본 결과, 8.7％의 매우 높은 살균력을 발휘한다는 것을 알 수 있었으며, 세탁 세제로의 사용 가능성이 매우 높음을 알 수 있었다.As described above, it was found that the natural laundry composition according to the present invention exhibited a very high sterilization power of 8.7% as a result of measuring the sample and the control for a very short time of 5 minutes, and the possibility of use as a laundry detergent was high. was found to be very high.
<실험예 2><Experimental Example 2>
형광 증백제 검출 측정Fluorescent Brightener Detection Measurements
본 발명에 따른 천연 세탁 조성물을 한국 의류시험 연구원에 의뢰하여 형광 증백제 검출을 측정하였다.The natural laundry composition according to the present invention was requested to the Korea Clothing Testing Institute and the detection of the optical brightener was measured.
도 2에 도시된 바와 같은 조건하에서 형광증백제의 유무 검출을 측정해본 결과, 형광 증백제가 검출되지 않았음을 알 수 있었다. As a result of measuring the presence or absence of a fluorescent whitening agent under the conditions as shown in FIG. 2 , it was found that no fluorescent whitening agent was detected.
<실험예 3><Experimental Example 3>
세척 효과의 측정Measurement of cleaning effectiveness
본 발명에 따른 천연 세탁 조성물을 한국 의류시험 연구원에 의뢰하여 세척력에 대한 효과를 측정하였다.The natural laundry composition according to the present invention was requested to the Korea Apparel Testing Research Institute to measure the effect on cleaning power.
그 결과, 도 3에 도시된 바와 같은 조건하에서 시료 1은 29.7％의 세척효과를, 시료 2는 40.2％의 매우 높은 세척력을 발휘한다는 것을 알 수 있었으며, 세탁 세제로의 사용 가능성이 매우 높음을 알 수 있었다.As a result, it was found that sample 1 exhibited a cleaning effect of 29.7% and sample 2 exhibited a very high cleaning power of 40.2% under the conditions shown in FIG. 3, indicating that the possibility of use as a laundry detergent is very high. could
본 발명의 실시예에 따른 천연 세탁 조성물은 세균 및 미생물의 번식을 전면 차단하고, 높은 세척력과 우수한 살균과 수질 개선의 기능을 갖는다는 것을 알 수 있었다.It was found that the natural laundry composition according to the embodiment of the present invention completely blocks the propagation of bacteria and microorganisms, and has high cleaning power, excellent sterilization and water quality improvement.
한편, 본 발명의 실시예에 따른 천연 세탁 조성물은 수산화칼륨, 또는 수산화칼슘, 가성소다, 알긴산 겔, 금화규겔 등을 추가로 더 첨가하여 제조할 수 있는 바, 바람직하게 이러한 추가 첨가물질은 건조염 100 중량％에 대해, 각각 1~8중량％이다.On the other hand, the natural laundry composition according to an embodiment of the present invention can be prepared by further adding potassium hydroxide, calcium hydroxide, caustic soda, alginic acid gel, silica gel, etc. It is 1 to 8 weight% with respect to weight%, respectively.
한편, 본 발명의 실시예에 따른 천연 세탁 조성물 제조방법은 단지 상기한 실시예에 한정되는 것이 아니라 그 기술적 요지를 이탈하지 않는 범위내에서 다양한 변경이 가능하다.On the other hand, the method for manufacturing a natural laundry composition according to an embodiment of the present invention is not limited to the above-described embodiment, and various modifications are possible without departing from the technical gist thereof.
Claims (6)
b) 1000℃로 가열하여 조해성물질이 제거된 건조염을 얻는 단계와;
c) 상기 건조염 100 중량％에 대해, 상기 천연 활성 산화칼슘 2 내지 5 중량％를 혼합하는 단계와;
d) 상기 건조염 100 중량％에 대해, 코코넛 열매분말 5～10중량％를 혼합하고, 소프넛 열매분말과, 팜 열매분말, 베이킹소다, 레몬으로 이루어진 추가 혼합물을 5 중량％ 내지 20중량％를 혼합하는 단계를 포함하여 이루어진 천연 세탁 조성물 제조방법.a) heating the shellfish shell of fish and shellfish to a heat treatment process of 1000 to 1500° C. to obtain natural active calcium oxide;
b) heating to 1000° C. to obtain a dried salt from which deliquescent substances are removed;
c) mixing 2 to 5% by weight of the natural active calcium oxide with respect to 100% by weight of the dry salt;
d) With respect to 100% by weight of the dry salt, 5 to 10% by weight of coconut fruit powder is mixed, and 5 to 20% by weight of an additional mixture consisting of soapnut fruit powder, palm fruit powder, baking soda and lemon A method for preparing a natural laundry composition comprising the step of mixing.
상기 d) 과정의 다음으로, 일정 단위의 분말 또는 고형물 또는 액상 형태로 성형하는 단계가 더 포함된 것을 특징으로 하는 천연 세탁 조성물 제조방법.The method of claim 1,
After step d), the method for manufacturing a natural laundry composition, characterized in that it further comprises the step of forming a predetermined unit of powder or solid or liquid form.
상기 a) 과정을 통해 제조된 활성 산화칼슘 분말 입자는 500 메쉬 이상인 것을 특징으로 하는 천연 세탁 조성물 제조방법.The method of claim 1,
The method for producing a natural laundry composition, characterized in that the active calcium oxide powder particles prepared through the step a) is 500 mesh or more.
상기 b) 과정을 통해 제조된 건조염 분말 입자는 35 메쉬 이상인 것을 특징으로 하는 천연 세탁 조성물 제조방법.The method of claim 1,
The method for producing a natural laundry composition, characterized in that the dry salt powder particles prepared through step b) are 35 mesh or more.
상기 d) 과정에서, 상기 추가 혼합물은 소프넛 열매분말 2～8중량％, 팜 열매분말 1～5중량％, 베이킹소다 1～4중량％, 레몬 1～3중량％로 이루어진 것을 특징으로 하는 천연 세탁 조성물 제조방법.The method of claim 1,
In the process d), the additional mixture is natural, characterized in that it consists of 2 to 8% by weight of softwood fruit powder, 1 to 5% by weight of palm fruit powder, 1 to 4% by weight of baking soda, and 1 to 3% by weight of lemon. A method for preparing a laundry composition.
상기 d)과정에서, 수산화칼륨, 또는 수산화칼슘, 가성소다, 알긴산 겔, 금화규겔 중 어느 하나 이상의 첨가물이 건조염 100 중량％에 대해, 각각 1~8중량％ 더 첨가되어 제조되는 것을 특징으로 하는 천연 세탁 조성물 제조방법.The method of claim 1,
In the process d), potassium hydroxide, or calcium hydroxide, caustic soda, alginic acid gel, and any one or more additives of silica gel, based on 100% by weight of the dry salt, each 1 to 8% by weight is added to the natural, characterized in that it is prepared A method for preparing a laundry composition.
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|---|---|---|---|---|
| KR102427519B1 (en) * | 2022-05-23 | 2022-07-29 | 이석중 | Laundry detergent for desalting and color transfer prevention containing natural surfactant and manufacturing method thereof |
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| KR102355808B1 (en) | 2022-01-26 |
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