KR20180094364A - Perfume composition representing the fragrance of juice contains wheatgrass extracts - Google Patents

Abstract

The present invention relates to a perfume composition for reproducing the fragrance of wheat (Triticum aestivum) sprout juice having young sprouts, called wheat sprouts, before node portions of wheat are created as a main ingredient. More specifically, the perfume composition for reproducing a fragrance of wheat sprout juice comprises a fragrance component of wheat sprout juice, and one or more components selected from a group consisting of Hedione, iso E Super, Verdox, and Isobornyl acetate. The composition has a high similarity to the unique fragrance of wheat sprout juice and excellent scent satisfaction as results in sensory evaluation and thus can be used as a perfume composition, and a home care product and a personal care product including the same.

Description

(Perfume composition representing the fragrance of juice containing wheatgrass extracts)

The present invention relates to a perfume composition recreating the fragrance of ginseng juice, and more particularly, to a fragrance composition containing fragrance components of ginseng juice; And at least one ingredient selected from the group consisting of Hedione, Iso E super, verdox and isobornyl acetate as active ingredients. And a perfume composition. The present invention also relates to a home care product and a personal care product comprising the perfume composition.

Wheat is wheat ( Triticum aestivum ) is a young sprout before the nodal area of the wheat is formed during germination. Wheat (Triticum aestivum) is a perennial herb with a blossom plant of the monocotyledonous plant. It is also called as wheat. It is originated from Afghanistan or Caucasus, and is cultivated mainly in the fields of temperate regions. Wheat is one of the oldest crops grown between 10,000 and 15,000 BC. It has been widely grown in Europe and China in the Stone Age, and the history of wheat cultivation in Korea is very long.

Chlorophyll of wheat helps blood circulation in vivo. In addition, it is excellent in nutrition because it contains protein, iron, potassium, vitamin B1, vitamin B3, vitamin A, vitamin C, vitamin E, tocopherol, betaglucan and arabinozaylan, And it has high value as a health food. In addition, wheat germ is rich in dietary fiber and is effective in constipation, and the calories are only 17kcal per 100g, so it is popular as a diet material.

Moss has become the main material of juice clens emerging as a trend in recent years. Juice cleanse is a detox therapy that releases accumulated toxins in the body by drinking juice made by juicing only fruit and vegetables without water, syrup or other additives such as sugar. You should only take juice juice periodically at a fixed time interval for a certain period of time, and other foods will be fasted. This juice is also known as 'cleans juice' or 'blue-blood juice'.

The principle of juice clarity is to relax the digestive system during the period when no other food is consumed, and to regulate the biorhythm so that only the discharge activity is achieved. At this time, it consumes the juice containing a large amount of nutrients that can remove the toxins in the body, thereby promoting the action of discharging waste products out of the body.

Following the wellbeing and diet craze, the cleansing method of releasing body waste has been emerged. As juice has become a new trend in the food and beverage market replacing coffee, juice materials such as fruits and vegetables have become a health food and cosmetic material The application is continuing.

Although the fragrance of the wheat has a distinctive scent different from that of natural grass, it is inevitable that the conventional solvent extraction method or steam distillation method will lose the fragrance due to heat and there will be many differences from the original fragrance, There is a problem. Therefore, it was attempted to develop a perfume composition having differentiated and novel characteristics by artificially reproducing the fragrance of ginseng juice having superior preference in terms of taste and aroma in addition to adding ginseng as a main ingredient but adding fruits and vegetables additionally.

Under these circumstances, the present inventors analyzed flavor components and content of ginseng juice in order to reproduce differentiated fragrance inherent in ginseng juice, and found that when the components analyzed by artificial mixing are mixed with the analyzed contents, And it was found that by adding a new fragrance ingredient which does not exist in the fresh juice, the original fragrance of the fresh juice can be reproduced almost similarly, thereby completing the present invention.

It is an object of the present invention to provide a flavor component of gourmet juice; And at least one ingredient selected from the group consisting of Hedione, Iso E super, verdox and isobornyl acetate as active ingredients. And to provide a reproduced perfume composition.

Another object of the present invention is to provide a home care product comprising the perfume composition.

It is still another object of the present invention to provide a personal care product comprising the perfume composition.

In order to solve the above problems and to achieve the object of the present invention, the present invention provides a flavor ingredient of a gourmet juice, And at least one ingredient selected from the group consisting of Hedione, Iso E super, verdox and isobornyl acetate as active ingredients. Thereby providing a reproduced perfume composition.

In the present invention, "wheat" is a young sprout before the nodule area of Triticum aestivum , which is a plant belonging to the monocotyledonous plant, is a grain which maintains the first production amount in the world, Is known to be distributed in temperate regions such as Afghanistan and Caucasia.

In the present invention, "gourmy juice" is a finely grated juice which is cut into a certain size and mixed through a mixer or the like, and fruits such as wheat bran or kiwi can be added. It is also called 'gentle cleansing' or 'gentle blue blood juice'.

In the present invention, "fragrance" refers to an odor that enters the nose as a fragrant but slightly pungent odor. The fragrance of the present invention means fragrant juice, meaning sweet and sweet fragrance.

In the present invention, the term "fragrance" is an organic substance having a strong aroma added to add flavor to cosmetics, food products, and the like, and has excellent volatility at room temperature. Spices can be roughly classified into natural fragrance obtained from roses, lemons, etc., isolated fragrance separated and purified from raw materials such as low-priced natural fragrance and coal tar, and synthetic fragrance synthesized through chemical reaction. It is also called artificial fragrance by combining isolated flavor and synthetic flavor. By application, cosmetics can be divided into fragrances and food fragrances. Cosmetics fragrance is aimed only at fragrance, but food fragrance is mainly flavor with flavor.

The perfume composition of the present invention is a perfume composition that reproduces the fragrance of the ginseng juice. The fragrance composition of the present invention is characterized in that fragrance components of the ginseng juice are selected from the group consisting of Hedione, Iso E super verdox and / or isobornyl acetate isobornyl acetate (Table 7). It was confirmed that the fragrance of the juice was similar to that of the fragrance.

In the present invention, the fragrance ingredient of the ginseng juice is collectively referred to as a component obtained by extracting the fragrance of the ginseng juice. Generally, fragrance is extracted by extraction with a solvent, distillation using water vapor, etc. However, the above methods are not suitable for extracting fragrance components by heating, , And the like, and there are many differences from the perfume characteristics of the original material. Headspace and SPME (solid-phase microextraction) methods have been developed to overcome these disadvantages. These two methods do not require any pretreatment of the sample without solvent and do not require a large amount of sample, and can analyze the fragrance component with the sample itself so that it can reproduce the original fragrance of the sample Method.

The fragrance composition of the present invention may be selected from the group consisting of Limonene, Terpineol, trans-2-hexenal, , Hexanal (Hexanal), and hexyl alcohol; a flavor component of the spirulina juice; And at least one component selected from the group consisting of hedione, Iso E super, verdox and isobornyl acetate as active ingredients. May be a reproduced perfume composition.

In addition, the perfume composition of the present invention may further contain at least one selected from the group consisting of gamma-terpinene, damascenone, beta-pinene, para-cymene, A flavor component of ginseng juice further comprising at least one ingredient selected from the group consisting of neryl acetate, geranyl acetate and beta-ionone; And at least one component selected from the group consisting of hedione, Iso E super, verdox and isobornyl acetate as active ingredients. May be a reproduced perfume composition.

The limonene is one kind of hydrocarbons belonging to terpenes, which is also called 1,8-p-mentadiene, and has a similar aroma to oranges and is used as a raw material for perfumes. D-limonene, which is one of the optical isomers, is contained in about 90% of the main component of orange oil, and is also contained in plant essential oils such as lemon oil, lime oil, and bergamot oil, and is widely distributed in plants. L-limonene, another optical isomer, is contained in oil of peppermint plants such as spearmint oil, turpentine oil, and peppermint oil. Terpineol is a lilac-like liquid, which is a generic term for alcohol in which one molecule of water is released from 1,8-terpine. Alpha, beta, and gamma-terpineol are known, and their main ingredient is alpha-terpineol. The optical isomers of alpha-terpineol are widely distributed as essential oil components in plants. The trans-2-hexenal is a colorless liquid, also called leaf alcohol, which has a fruit and vegetable flavor, and is particularly used as a food flavoring for flavor and aroma of cucumber. The hexanal is widely used in the food industry for the purpose of fruiting fruit with six carbon substituent-free chain-like aldehydes. The hexyl alcohol is a colorless liquid having a fruit flavor and is used as a food flavor for coconut and berry flavor, and is also used for perfuming wine in perfume.

In one embodiment of the present invention, the fragrance components of the ginseng juice were analyzed using a headspace method. As a result, limonene, terpineol, trans-2 Trans-2-hexenal, hexanal and hexyl alcohols were identified and gamma-terpinene, damascenone, beta- Beta-pinene, para-cymene, neryl acetate, geranyl acetate and beta-ionone were identified (Table 1).

In one embodiment of the present invention, the compositions and flavor components of the same ginseng juice were the same, but the similarity and satisfaction of the composition with different contents were evaluated. As a result, the similarity with the ginseng flavor was low, . That is, even if it contains the same ingredient as the fragrance ingredient of the ginseng juice, it is difficult to reproduce the fragrance of the ginseng juice as it is.

Under this background, the inventors of the present invention have found that by additionally adding Hedione, Iso E super, verdox and / or isobornyl acetate to the fragrance ingredient of the gourmet juice, The fragrance of the juice could be reproduced. In particular, the perfume composition of the present invention may contain a herbicide and an iso-super in the fragrance component of the germicidal juice. More specifically, It must contain an iso super, and may additionally contain one or more components in the group consisting of verdose and isobornyl acetate.

The hedione is a kind of ester, which is a diffusible perfume, and is also called methyl dihydrojasmonate. In addition, a jasmine-like flavor is produced, and a racemic mixture has a floral-like aroma and a citrus-like aroma. The above-mentioned Aiso Super is a synthesized ketone, which has a similar flavor to sandalwood and cedarwood, and has a very wide range of use such as soap, shampoo, perfume, detergent and fabric softener. The verdose is also called 2-tert-butylcyclohexyl acetate and is characterized by strong apple fruit. The isobornyl acetate is a colorless liquid having a pine tree leaf odor and is frequently used in soaps, bath salts, fragrances and the like.

In one embodiment of the present invention, it was confirmed that the fragrance added with herbicide or isoist super added to the fragrance ingredient of the germicidal juice was very excellent in similarity and satisfaction with fragrance juice (Table 7). In addition, it was confirmed that the fragrance added with herbicide and isozy super and / or verdox or isobornyl to the fragrance component of the germicidal juice was superior in similarity and satisfaction with the fragrance juice flavor, In the case of the fragrance added with all of the four kinds of herodon, isoise super, verdose and isobornyl to the fragrance component, it was confirmed that the degree of similarity and satisfaction with the fragrance juice fragrance was the highest (Table 7).

Accordingly, the perfume composition of the present invention is a specific perfume composition comprising: a fragrance ingredient of ginseng juice; Hedione; And an isoe super ingredient as an active ingredient, a fragrance composition recreating the fragrance of ginseng juice, a fragrance ingredient of ginseng juice; Hedione; Iso super; And a perfume composition recreating the fragrance of ginseng juice comprising a verdose component as an active ingredient, a fragrance component of ginseng juice; Hedione; Iso super; And an isobornyl acetate component as an active ingredient, and a fragrance composition of ginseng juice; Hedione; Iso super; But is not limited to, a fragrance composition that reproduces the fragrance of ginseng juice containing verdose and isobornyl acetate as an active ingredient.

Specifically, the present invention provides a fragrance composition recreating the fragrance of ginseng juice containing the following ingredients.

Specifically, the perfume composition comprises 1 to 70 parts by weight of limonene, 1 to 50 parts by weight of terpenol, 1 to 30 parts by weight of trans-2-hexenyl, 1 to 30 parts by weight of hexanal And 1 to 20 parts by weight of hexyl alcohol. More specifically, the total content of the five components may be 30 to 90 parts by weight per 100 parts by weight of the total composition, and more specifically, May be 50 to 80 parts by weight based on 100 parts by weight of the total composition.

The fragrance composition may further comprise 0.1 to 10 parts by weight of gamma-terpinene, 0.1 to 10 parts by weight of damascenone, 0.1 to 10 parts by weight of beta-pinene, 0.1 to 10 parts by weight of para- 0.1 to 10 parts by weight of neryl acetate, 0.1 to 10 parts by weight of geranyl acetate and 0.1 to 10 parts by weight of beta-ionone.

Also, the perfume composition may contain 0.1 to 20 parts by weight of hedonic acid, 0.1 to 20 parts by weight of iso super, 0.1 to 10 parts by weight of verdose and 0.1 to 10 parts by weight of isobornyl acetate based on 100 parts by weight of the total composition can do.

In another aspect of the present invention, there is provided a home care product comprising the perfume composition.

In the present invention, the term "home care product" refers to products used for household cleaning (e.g., hard surface cleaners, manual and automatic dish care, toilet cleaners and disinfectants, (For example, detergents, fabric softeners, pretreatment stain removers), directional compounds to remove odors or, in some cases, be used as a perfume substitute. , And the like, but the present invention is not limited thereto, and can be applied to all the home care compositions into which the perfume is injected. Specifically, the home care products include laundry detergents, laundry detergent additives, laundry bars, fabric softeners, kitchen detergents, wood and furniture polishes, floor polishes, bath and tile cleaners, toilet cleaners, hard surface cleaners, window cleaners, anti- But are not limited to, cleaners, auto-dishwashing agents and sheeting agents, carpet cleaners, prewash spotters, rust stain cleaners, descalers, deodorants and perfumes.

Products for use in the home care products of the present invention, such as laundry products, may be, but are not limited to, a textile care product comprising the perfume composition and a cationic polymer, an amphoteric surfactant, or a mixture thereof. The cationic polymer used in the textile care product may be selected from the group consisting of cationic guar, cationic cellulose, dimethyldiallylammonium chloride polymer, acrylamide-dimethyldiallylammonium chloride copolymer, PVP-dimethylaminoethyl methacrylate copolymer, Dimethyl diallylammonium chloride copolymer, acrylamide-dimethylaminoethyl methacrylate methyl chloride copolymer, trimethylaminoethyl methacrylate polymer, and the like, but is not limited thereto. The amphoteric surfactant used in the textile care product is selected from the group consisting of alkylamidopropyl betaine, alkyldimethylbetaine, alkylmonoamphoacetate, cocoamphocarboxy glycinate, sarcosinate and alkylamphodiacetate, and the like. Any one or more may be used, but are not limited to.

While the home care products of the present invention, such as those for use in such laundry products, require several cleaning additives, certain simple formulations, such as bleach additives, may require only oxygen bleaching agents and surfactants. The cleaning adjunct may include builders, enzymes, bleaches, bleach activators, catalytic materials, and the like. Specifically, the cleaning adjunct may be selected from the group consisting of a foam promoter, a foam inhibitor (defoamer), a dispersant polymer, a color speckle, a silver care agent, an antioxidant and / or an anticorrosive, a dye, a filler, a bactericide, May contain various active or specialized substances such as stabilizers, stabilizers, enzyme stabilizers, pro-peptides, antioxidants, solubilizers, carriers, processing aids and pigments and in the case of liquid formulations, solvents, chelating agents, Antioxidants, perfumes, processing aids, and other fabric care agents, surfaces, and skin care agents, which may be included in the compositions of the present invention.

The home care product of the present invention, such as a perfume, may be a volatile perfume composition comprising the gel or solidified inventive perfume composition of the present invention and may be a liquid perfume composition comprising the perfume composition of the present invention prepared in liquid form have. In addition, the perfume composition may contain 0.001 to 30% by weight, specifically 1 to 30% by weight, more specifically 1 to 10% by weight, of the perfume composition of the present invention in the weight of the total product. When the perfume composition is added in an amount of less than 0.001% by weight, the fragrance is difficult to be appreciated because the fragrance is very low. When the perfume composition is added in an amount of more than 30% by weight, the fragrance becomes too strong for use as a fragrance. When the perfume composition of the present invention is used as a fragrance additive, the composition can be added as it is or mixed with optional ingredients useful in a flavoring or fragrance. In particular, they may be mixed with one or more of the natural extracts used in the field of a wide variety of natural, synthetic, synthetic chemicals, natural fragrances, flavors, flavors or fragrances. Additionally, the perfume may include one or more ingredients or excipients commonly used with flavors and fragrances, such as carrier materials, thickeners, flavor enhancers and other adjuvants commonly known and used in the art have.

In another aspect of the present invention, there is provided a personal care product comprising the perfume composition. The present invention also provides a cosmetic composition comprising the perfume composition.

In the present invention, "personal care product" is intended to encompass all types of cosmetic products, including cosmetics, hair care products, toiletries, cosmeceuticals, beauty aids, , Personal hygiene and cleansing products, but are not limited thereto, and can be applied to personal care compositions into which perfumes are injected. Specifically, the present invention relates to a cosmetic composition comprising a composition selected from the group consisting of deodorant, antiperspirant, spray, stick and roll-on product, shaving preparation, skin lotion, Nail polish remover, nail cream and lotion, exfoliant, sunscreen, insect repellent, anti-aging agent, lipstick, foundation, face powder, eyeliner , Eye shadow, blushes, makeup, mascara, moisturizing preparation, body and hand preparation, skin care preparation, face and neck preparation, tonic, dressing, hair grooming aid, aerosol fixative, fragrance preparation, aftershave, - up formulation, soft focus preparations, night and day skin care preparations, non-pigmented hair preparations, tanning preparations, synthetic and non-synthetic soap bars, Makeup remover, facial cleanser, cold cream, sunscreen, mousse, spritz, shampoo, shampoo, baby shampoo, baby shampoo, shaving cream, squeegee, nose strip, personal care nonwovens, baby shampoo, baby conditioner, Face masks and muds, face masks, colognes and lotions, hair cuticle coats, shower gels, face and bodywashes, personal care rinse-offs, gels, foam baths, scrubbing cleansers, astringents, nail conditioners, eye shadow sticks, Hair brush, lip balm, lip gloss, hair care pump spray and other non-aerosol sprays, hair-freeze-control gel, hair rib-in conditioner, hair pomade, hair detergent, hair fixative, hair bleach, skin Lotions, pre-shave and pre-electric shave, anhydrous creams and lotions, oil / water, water / type, multiple macros Microemulsions, water-resistant creams and lotions, acne skin preparations, mouthwashes, massage oils, toothpastes, clear gels and sticks, ointment bases, local wound healing agents, aerosol talc, barrier sprays, vitamins and antioxidants, herbal extracts, Hair styling aids, hair-, eye-, nail- and skin-soft products, emit control personal care products, hair conditioning mists, skin care moisturizing mist, skin wipes, pores But are not limited to, skin wipes, pore cleansers, Blemish Reductors, skin exfoliators, skin removers, skin towelette and cloth, depilatories, personal care lubricants and nail coloring aids.

The personal care products of the present invention, such as cosmetics, can be used as a solution, an external ointment, a cream, a foam, a nutritional lotion, a softening longevity pack, a pack, a flexible water, a milky lotion, a makeup base, an essence, But may be formulated as a suspension, emulsion, paste, gel, lotion, powder, soap, surfactant-containing cleansing, oil, powder foundation, emulsion foundation, wax foundation, patch, But is not limited thereto.

The cosmetics of the present invention may further comprise at least one cosmetically acceptable carrier to be incorporated in cosmetics for general skin, and examples thereof include oil, water, a surfactant, a humectant, a lower alcohol, a thickener, a chelate Coloring matters, preservatives, fragrances, and the like may be appropriately compounded, but the present invention is not limited thereto. The cosmetically acceptable carrier included in the cosmetic of the present invention varies depending on the formulation.

When the formulation of the present invention is an ointment, a paste, a cream or a gel, the carrier component may be an animal oil, a vegetable oil, a wax, a paraffin, a starch, a tracer, a cellulose derivative, polyethylene glycol, silicone, bentonite, silica, talc, zinc oxide Mixtures of these may be used.

When the formulation of the present invention is a powder or a spray, lactose, talc, silica, aluminum hydroxide, calcium silicate, polyamide powder or a mixture thereof may be used as the carrier component, Propellants such as fluorohydrocarbons, propane / butane or dimethyl ether.

When the formulation of the present invention is a solution or emulsion, a solvent, a dissolving agent or an emulsifying agent is used as a carrier component, and examples thereof include water, ethanol, isopropanol, ethyl carbonate, ethyl acetate, benzyl alcohol, benzyl benzoate, 1,3-butyl glycol oil may be used, in particular fatty acid esters of cottonseed oil, peanut oil, corn oil, olive oil, castor oil and sesame oil, glycerol aliphatic esters, polyethylene glycols or sorbitan may be used have.

When the formulation of the present invention is a suspension, a carrier such as water, a liquid diluent such as ethanol or propylene glycol, a suspension such as ethoxylated isostearyl alcohol, polyoxyethylene sorbitol ester and polyoxyethylene sorbitan ester, Crystalline cellulose, aluminum metahydroxide, bentonite, agar or tracant, etc. may be used.

When the formulation of the present invention is a soap, an alkali metal salt of a fatty acid, a fatty acid hemiester salt, a fatty acid protein hydrolizate, isethionate, a lanolin derivative, an aliphatic alcohol, a vegetable oil, glycerol, .

In the cosmetic of the present invention, the content of the perfume composition may vary depending on the formulation. For example, wash-off type cosmetics, such as make-up removers, detergents, and the like, where the active ingredient remains on the skin in a short period of time, may be relatively high concentrations. On the other hand, in the case of leave-on type cosmetics such as lotion, cream, essence and the like in which the active ingredient remains on the skin for a long period of time, the concentration may be lower than that of the wash-off type cosmetics.

The personal care products of the present invention, for example, hair care products, can be used as a shampoo (including complex shampoos such as two-in-one conditioning shampoos), hair conditioners, rinses after shampooing, hair dyeing, But are not limited to, styling agents (including setting aids such as gels and sprays, and grooming adjuvants such as pomades, conditioners, permanent liquids, and relaxants), and hair smoothing products. The hair care product may include, but is not limited to, the perfume composition of the present invention and any one or more selected from the group consisting of a cationic surfactant, an amphoteric surfactant, a nonionic surfactant, and a cationic polymer. The cationic surfactant used in the hair care product may be at least one selected from the group consisting of cetrimonium chloride, stearamidopropyldimethylamine, dicetyldimethylammonium chloride and ester quatro. It does not. The amphoteric surfactant used in the hair care product may be at least one selected from the group consisting of cocamidopropyl betaine, cocoamphocarboxy glycinate and coco amphocarboxy propionate, but is not limited thereto. The nonionic surfactant used in the hair care product may be at least one selected from the group consisting of lauryl acid diethanolamide, coconut fatty acid diethanolamide, coconut fatty acid monoethanolamide, lauryldimethylamine oxide and palm oil alkyldimethylamine oxide May be used, but is not limited thereto. The cationic polymer used in hair care products is a natural cationic polymer group consisting of guar hydroxypropyl trimonium chloride, hydroxypropyl guar hydroxypropyl trimonium chloride and quaternary hydroxyethyl cellulose; And a synthetic cationic polymer group consisting of dimethyldiallylammonium chloride polymer, acrylamide dimethyl allylammonium chloride copolymer and polyvinyl pyrrolidone dimethyl amino ethyl methacrylate copolymer, may be used. It is not limited. The hair dye may be a hair dye containing the perfume composition of the present invention, a precursor and a coupler, but is not limited thereto.

The personal care products of the present invention, such as body care products, may be used as a single component or as a single component for bath and shower additives, fragrance and flavor containing preparations, hair care products, deodorants and depot preparations, decorative preparations, Can be used in combination with a stabilizer. The body care product may be a body oil, a body lotion, a body gel, a treatment cream, a skin protective ointment, a shaving preparation such as a shaving foam or gel, a skin powder such as a baby powder, a moisturizing gel, a moisturizing spray, Sprays, cellulite gels, and peeling agents. Suitable bath and shower additives include shower gel, bath-salt, bubble bath and soap. Formulations containing fragrant and flavor substances include perfumes, lotions and shaving lotions (aftershave formulations). The body care product may be in the form of a cream, ointment, paste, foam, gel, lotion, powder, makeup, spray, stick or aerosol, but is not limited thereto. The body care product may also include, but is not limited to, a stabilizing mixture, and optionally additional UV absorbers, sterically hindered amines, complexing agents, and phenolic or non-phenolic antioxidants.

The present invention relates to a composition for reproducing the fragrance of ginseng juice. It has been confirmed through sensory evaluation that the degree of similarity with the intrinsic fragrance of the ginseng juice is high and the satisfaction of the fragrance is excellent. The perfume composition and the home care Products and personal care products.

Hereinafter, the present invention will be described in detail with reference to Examples and Experimental Examples. However, the following Examples and Experimental Examples are merely illustrative of the present invention, and the present invention is not limited to the following Examples and Experimental Examples.

Experimental Example  One. Headspace method  Analysis of fragrance components of ginseng juice

The headspace analysis method is a method in which a sample fragrance component can be sampled as it is in a natural state. In the present invention, the headspace analysis method is used, and the components of the juice are analyzed using the method described in the literature under the following analysis conditions .

Milk juice was purchased from Mercy Juice (http://mercyjuice.com), juiced on the day of ordering, and received directly at the store the next day. The shampoo juice was covered with a wrap which was able to be hermetically sealed, and circulated air was passed through the tenax column while the outside air was forcibly circulated by the power device to collect fragrance components.

The tenax column, in which the odor was collected, was connected to a gas chromatographic analyzer to analyze the type and content of the collected fragrance. The results are shown in Table 1 below.

<Analysis condition>

Analytical Instruments: Hewlett Packard 6890

Detector: MSD

Column: HP-20M 0.2 mm ID x 25 m

Injection temperature: 250 ° C

Detector temperature: 250 ° C

Oven temperature: 55 占 폚 (0 minutes) to 215 占 폚 (40 minutes), 4.0 占 폚 / min

Split Ratio: 30: 1

Mobile phase gas: helium 18 cm / sec

Injection amount: 0.3 ml

Analysis of fragrance component of ginseng juice Perfume name weight (%) Limonene 28.4 Terpineol 17.5 Trans-2-hexenal &lt; / RTI &gt; 14.3 Hexanal 8.9 Hexyl alcohol 7.2 Gamma-terpinene &lt; / RTI &gt; 3.6 Damascenone 2.6 Beta-pinene &lt; / RTI &gt; 2.5 Para-cymene 1.6 Neryl acetate 1.3 Geranyl acetate &lt; RTI ID = 0.0 &gt; 0.7 Beta-ionone &lt; / RTI &gt; 0.6 Other 10.8 total 100.0

As a result of analysis, the major fragrance components of the ginseng juice were limonene, terpineol, trans-2-hexenyl, hexanal and hexyl alcohol, which accounted for about 76% of the total fragrance ingredient.

Experimental Example  2. Preparation and comparative analysis of fragrance of fragrance juice

&Lt; 2-1 > Preparation of fragrance to reproduce fragrant juice

Based on the fragrance juice component (Table 1) analyzed in Experimental Example 1, a fragrance component of the fragrance juice fragrance having the composition and contents shown in Table 2 was prepared. Then, comparative analysis was performed on the ginseng fragrance ingredient of Table 1 above and the fragrance juice reproduction fragrance of the following Table 2 as follows.

Fragrance Perfume name Comparative Example 1 Limonene 28.4 Terpineol 17.5 Trans-2-hexenal &lt; / RTI &gt; 14.3 Hexanal 8.9 Hexyl alcohol 7.2 Gamma-terpinene &lt; / RTI &gt; 3.6 Damascenone 2.6 Beta-pinene &lt; / RTI &gt; 2.5 Para-cymene 1.6 Neryl acetate 1.3 Geranyl acetate &lt; RTI ID = 0.0 &gt; 0.7 Beta-ionone &lt; / RTI &gt; 0.6 Other 10.8 total 100.0

<2-2> Sensory Evaluation of Flavor Reproducing Flavor of Waxy Juice

The sensory evaluation of the similarity and satisfaction with the fragrance juice flavor of the fragrance of the fragrance juice produced in the above Experimental Example <2-1> was performed. The sensory evaluation subjects were 20 normal healthy men and women aged 25 to 35 years. The similarity of the perfume juice reproducible perfume of Comparative Example 1 was evaluated by the 5-point rating method according to the following Table 3. The satisfaction was evaluated by the 5-point rating method according to the following Table 4 for each of the perfumes, Are shown in Table 5 below. The evaluation room and the sample preparation room were separated so that the evaluator had no prior knowledge of the sample.

5-point Rating Method for Similarity score Similarity One Very different 2 a little bit different 3 so so 4 A little similar 5 Very similar

Five-point rating method for satisfaction score satisfaction One Not very good 2 It's not good. 3 so so 4 A little good 5 very good

Evaluation results - similarity and satisfaction rater Similarity satisfaction number age gender Comparative Example 1 Comparative Example 1 One 26 female 3 3 2 31 female 2 4 3 28 female 3 3 4 29 female 2 2 5 31 female 4 3 6 30 female One 2 7 29 female 2 3 8 29 female 3 2 9 32 female One 2 10 34 female 3 3 11 35 south 4 3 12 26 south 2 3 13 28 south 3 4 14 25 south One 3 15 33 south 4 2 16 31 south 2 3 17 32 south 3 3 18 31 south 2 2 19 28 south 3 3 20 29 south 3 2 Average 2.55 2.75

As a result of the analysis, it was found that the fragrance reproducible flavor of the ginseng juice combined with the fragrance juice combined with the flavor fragrance of the ginseng juice of Table 1 was low, Respectively. As a result, it was judged that it was impossible to reproduce the fragrance of juice by the headspace analysis result alone. Therefore, it was confirmed that it is desirable to reproduce the fragrance of the juice by adding a new fragrance ingredient based on the head space result.

Experimental Example  3. Spice flavor improving fragrance with added new fragrance ingredient

<3-1> Preparation of flavor improving fragrance

In order to improve the degree of similarity and satisfaction of the perfume of Comparative Example 1 prepared in Experimental Example 2, an aroma improving fragrance of ginseng juice added with a new fragrance ingredient was prepared.

Specifically, a new combination of improving fragrances was prepared using artificial synthetic substances such as HEDION, ISOTHER SUPER, VARDOX and isobornyl acetate as the constituents of the perfume of Comparative Example 1. [ The content of HEDION, AISO SUPER, VARDOX and isobornyl acetate was determined according to the judgment of the professional group of the fermenter, and the total content of the four kinds of components was added in such a manner that the total content was 10 to 20 parts by weight, The external components were adjusted to meet the total content of 100 parts by weight in accordance with the content change. The composition of the improved fragrances of the new combination is shown in Table 6 below.

Composition table of fresh perfume composition (unit: parts by weight) Perfume name Manufacturing example  One Manufacturing example  2 Manufacturing example  3 Manufacturing example  4 Manufacturing example  5 Limonene 34.5 32.1 28.5 29.5 30 Terpineol 13.5 12.4 13.5 12.5 14.6 Trans-2-hexenal &lt; / RTI &gt; 10.2 9.8 8.4 8.6 9.4 Hexanal 8.4 5.4 6.3 6.5 4.1 Hexyl alcohol 4.8 5.1 6.9 5.6 4.3 Gamma-terpinene &lt; / RTI &gt; 3.2 3.4 3.1 2.9 5.4 Damascenone 2.6 2.8 3.1 5.2 2.4 Beta-pinene &lt; / RTI &gt; 2.5 4.3 1.9 2.4 1.5 Para-cymene 1.5 0.8 1.1 1.2 1.3 Neryl acetate 1.5 4.5 2.5 1.3 2.9 Geranyl acetate &lt; RTI ID = 0.0 &gt; 0.4 0.5 0.8 1.2 1.2 Beta-ionone &lt; / RTI &gt; 0.6 0.7 0.8 0.9 1.4 Hedione - 2.5 2.5 2.6 2.8 Iso E super 1.2 - 2.5 1.8 2.4 Verdox 0.8 1.2 - 1.1 1.3 Isobornyl acetate 0.2 0.2 0.1 - 0.4 Other 14.1 14.3 18 16.7 14.6 total 100.0 100.0 100.0 100.0 100

&Lt; 3-2 > Sensory evaluation of flavor improving fragrance of juice

The sensory evaluation of the similarity and preference with the fragrance juice flavor of the flavor improving fragrance of the ginseng juice prepared in Experimental Example <3-1> was performed. The sensory evaluation subjects were 20 normal healthy men and women aged 25 to 35 years. The similarity of each of the fragrance of fragrance juice of Preparation Examples 1 to 5 to each of the perfume fragrances was evaluated by the 5-point rating method according to Table 3. The satisfaction was evaluated by the 5-point rating method according to Table 4 The evaluation results are shown in Table 7 below. The evaluation room and the sample preparation room were separated so that the evaluator had no prior knowledge of the sample.

Evaluation results - similarity and satisfaction rater Similarity satisfaction number age gender Manufacturing example
One Manufacturing example
2 Manufacturing example
3 Manufacturing example
4 Manufacturing example
5 Manufacturing example
One Manufacturing example
2 Manufacturing example
3 Manufacturing example
4 Manufacturing example
5 One 26 female 3 4 4 3 4 3 3 4 5 5 2 31 female 2 5 5 4 5 4 4 5 4 5 3 28 female 3 4 5 3 5 3 5 2 4 4 4 29 female 3 4 3 3 4 2 5 2 5 5 5 31 female 5 3 4 3 5 3 4 4 4 4 6 30 female 3 5 5 3 5 2 3 3 2 4 7 29 female 4 2 3 4 5 3 2 4 3 4 8 29 female 3 4 4 4 4 3 2 3 4 5 9 32 female 2 5 4 5 4 3 5 3 3 5 10 34 female 3 4 4 5 4 4 4 4 4 5 11 35 south 3 3 5 5 4 3 4 4 4 5 12 26 south 2 3 5 3 4 2 2 4 4 3 13 28 south 4 2 3 4 5 3 2 4 3 3 14 25 south 3 4 3 4 5 4 2 5 3 4 15 33 south 3 5 3 4 5 4 3 5 5 4 16 31 south 2 3 4 4 4 4 3 4 5 4 17 32 south 5 3 3 3 4 3 3 4 5 4 18 31 south 2 5 3 5 3 5 2 4 4 5 19 28 south 3 2 3 5 3 4 5 4 4 5 20 29 south 3 3 4 4 4 3 2 4 4 4 Average 29.1 3.05 3.65 3.85 3.9 4.3 3.25 3.25 3.8 3.95 4.35

The subject to be evaluated proceeded in the same manner as in Experimental Example 2 above.

As a result of the similarity evaluation, the comparative example 1 in which only the major components of the ginseng juice was combined showed a low degree of similarity as shown in Table 5 (Table 5).

As can be seen from Production Examples 1 to 5 of Table 7, it was evaluated that the degree of similarity was increased when hederone, isoise super, verdose and / or isobornyl acetate were added. Especially, the degree of similarity of Production Examples 2, 3, 4 and 5 in which the heddone was additionally mixed was further increased, and it was found that the heddone was the main component of the perfume reproduction of the ginseng juice. Further, the similarity of Production Examples 3, 4, and 5, which were added to Hedione with iso super as compared with Comparative Example 1, was further increased, and in particular, both Hedione, As a result, the degree of similarity of Production Example 5 was found to be the most remarkably increased. As a result, it was confirmed that the combination of the above-mentioned four components was more similar (Table 7).

As a result of the satisfaction evaluation, the comparative example 1 in which only the major components of the ginseng juice was combined showed a low satisfaction as shown in Table 5 (Table 5).

On the other hand, as can be seen from Production Examples 1 to 5 of Table 7, it was evaluated that the satisfaction was increased when hederone, isoise super, verdose and / or isobornyl acetate were added. In particular, the satisfaction level of Production Examples 1 to 5, in which hedione or isoiste supplements were additionally mixed, was further increased, so that it was found that the hendione or isoist super was the main component of the perfume juice reproducibility. Further, it was confirmed that Production Examples 3 to 5 containing both a herdone and an iso-super supernatant were significantly more satisfactory than those containing a herbicide and an iso-super supernatant, The satisfaction of Production Example 5 in which both of isobornyl acetate was further added was the greatest increase, and it was confirmed that the combination of the above-mentioned four ingredients was more satisfactory (Table 7).

Thus, it has been found that in addition to the fragrance juice ingredient, the perfume juice of compositions comprising Hedione and iso super and / or verdose or isobornyl acetate is highly satisfied with perfume similarity and flavor, As a fragrance composition recreating the fragrance of home care products? It can be used as a personal care product.

Claims (8)

Fragrance component of gourd juice; And at least one component selected from the group consisting of hedione, Iso E super, verdox and isobornyl acetate as active ingredients. The perfume composition being reproduced.
3. The flavor enhancer composition of claim 1, wherein the flavor component of the ginseng juice is selected from the group consisting of Limonene, Terpineol, trans-2-hexenal, Hexanal and hexyl alcohol &Lt; RTI ID = 0.0 &gt; 1, &lt; / RTI &gt;
3. The composition of claim 2, wherein the fragrance ingredient of the buds juice comprises gamma-terpinene, damascenone, beta-pinene, para-cymene, wherein the perfume composition further comprises at least one component selected from the group consisting of neryl acetate, geranyl acetate and beta-ionone.
The perfume composition of claim 2, wherein the perfume composition comprises 1 to 70 parts by weight of limonene, 1 to 50 parts by weight of terpineol, 1 to 30 parts by weight of trans-2-hexenyl, 1 to 30 parts by weight of hexa And 1 to 20 parts by weight of hexyl alcohol.
The perfume composition of claim 3, wherein the perfume composition comprises from 0.1 to 10 parts by weight of gamma-terpinene, from 0.1 to 10 parts by weight of damascenone, from 0.1 to 10 parts by weight of beta-pinene, from 0.1 to 10 parts by weight of para 0.1 to 10 parts by weight of neryl acetate, 0.1 to 10 parts by weight of geranyl acetate and 0.1 to 10 parts by weight of beta-ionone.
The perfume composition of claim 1, wherein the perfume composition comprises from 0.1 to 20 parts by weight of a hedonic, from 0.1 to 20 parts by weight of iso super, from 0.1 to 10 parts by weight of verdose and from 0.1 to 10 parts by weight of isobornyl acetate &Lt; / RTI &gt;
7. A home care product comprising a perfume composition according to any one of claims 1 to 6.
9. A personal care product comprising a perfume composition according to any one of the preceding claims.