KR20170130209A - The manufacturing method having liquid with Dendropanax morbifera - Google Patents

Abstract

The present invention relates to a liquid concentrate of Dendropanax morbifera. Specifically, the present invention relates to a liquid concentrate of Dendropanax morbifera produced by the steps of: introducing Dendropanax morbifera material into an extractor; extracting a first concentrate of Dendropanax morbifera from the extractor; extracting the first concentrate at 75-95C for 16-28 hours to produce a second concentrate of Dendropanax morbifera; filtering the second concentrate of Dendropanax morbifera through 80-100 mesh, and purifying the same to form a third concentrate of Dendropanax morbifera; and sterilizing the third concentrate of Dendropanax morbifera at 80-90C for 30-60 minutes. Accordingly, an effect of Dendropanax morbifera can be maximized. According to the present invention, a Dendropanax morbifera material is introduced into an extractor; a first concentrate of Dendropanax morbifera is extracted from the extractor; a second concentrate of Dendropanax morbifera is produced by extracting the first concentrate of Dendropanax morbifera at 75-95C for 16-28 hours; the second concentrate of Dendropanax morbifera is filtered through 80-100 mesh and purified to form a third concentrate of Dendropanax morbifera; and the third concentrate of Dendropanax morbifera is sterilized at 80-90C for 30-60 minutes.

Description

[0001] The present invention relates to a method for producing Dendropanax morbifera,

More particularly, the present invention relates to a method for extracting a first bullion concentrate from an extractor, extracting the first bullion concentrate from the extractor, At a temperature of 80 ° C to 90 ° C for 30 minutes to 60 minutes. The second yellowing concentrate obtained by filtering the second yellowing concentrate by filtration at 80 mesh to 100 mesh is sterilized at 80 ° C to 90 ° C for 30 minutes to 60 minutes.

As is well known, Dendropanax morbifera is an evergreen tree belonging to Araliaceae and can be seen in some parts of the southern coast of Korea. When yellow barks are injured, yellow liquor is secreted by Huanghil.

These yellowgrass are glowing with golden light, have a sense of humor, defeating bad aura, and calm all scams comfortably.

The leaf is valuable as a representative economic species of southern temperate zone which has been attracted attention as a mysterious tree with excellent pharmacological effects since it is used as a physiologically active substance containing an anticancer agent and an immunity enhancer.

There have been disclosed a number of techniques for drinking Huangchil because of its beneficial effect on the human body of Huangchil. The patent registration No. 10-441645 is a health drink, and the patent registration No. 10-1196166 is a Huangchil tea.

Specifically, the wood is called "Dendropanax morbifera", which means the panacea for international studies, and it is also called a golden tree. It is a Korean native species native to the southern coast of Korea and Jeju Island. Its height is about 15m. The flowers bloom at the end of June branch, and the fruit is elliptical nucleus with a length of 7 ~ 19㎜. It ripens in color. The constituents and effects of this woody wood are mainly sesquiterpene, which contains water, gum, alcohol, ester and the like. Hwangchil, which is a sap extracted from Hwangchilgi bark, is said to have been used only by the royal family because it has a remarkable pharmacological effect and a delicate environment.

It has been widely accepted that nutritional value, pharmacological value, and therapeutic value have been studied in modern scientific studies and it has been studied in various directions and forms in order to utilize useful materials of Huangchil. Korean Patent Laid-Open Publication No. 2004-0107852 discloses a method for preparing a Huangchil extract having a skin whitening effect and a Huangchil extract according to the method, Korean Patent Registration No. 10-0318019 discloses a Huangchil extract having anticancer activity, 0663284 discloses a seedling extract of Hwangchil, which is excellent in physiological activity. Korean Patent Registration No. 10-0988072 discloses a fermented product of Hwangchulnam and a pharmaceutical composition containing the same, Korean Patent Publication No. 2003-0005098 discloses a fermented product And Korean Unexamined Patent Application Publication No. 2005-0036093 discloses a technique of an ultraviolet cut cosmetic composition containing an extract of Hwangjak tree as an active ingredient.

Therefore, it has been an important issue to produce the above-mentioned cornflower oil, and a new manufacturing method that can be used as a health food by selling it directly was also needed.

Korea Patent Publication No. 2014-0031662 Korean Patent No. 1475180 Korean Patent No. 1565742

Disclosure of Invention Technical Problem [8] Accordingly, the present invention has been made to solve the above problems, and it is an object of the present invention to provide a nutritional supplement rich in nutrients It is aimed to produce Bulgogi tree concentrate which can be used.

In order to solve the above-described problems, the present invention provides a method for producing a fermented soybean milk, which comprises the steps of feeding a fermented raw material to an extractor, extracting a first fermented concentrate from the fermentor and extracting the first fermented concentrate from a second fermented concentrate extracted at 75 to 95 ° C for 16 to 28 hours Is filtered through 80 mesh to 100 mesh to sterilize the third crude sulfuric acid concentrate at 80 ° C to 90 ° C for 30 minutes to 60 minutes.

The volume ratio of the raw material to the raw material and the volume of water is 1: 6 to 10 times as much as the input amount of the raw material for yellowing.

The concentrate is firstly concentrated to a solid content of 50% or more and secondarily concentrated to a solid content of 65% or more in order to efficiently concentrate the concentrate without damaging intrinsic color, flavor and taste inherent to the concentrate.

The primary concentration of the second sulfuric acid concentrate is 0.7 kG decompression and concentration at 50 캜 to 60 캜, but the temperature can be controlled according to the concentration time.

The second sulfur concentrate is concentrated at a reduced pressure of 0.1 to 0.2 kG and at a temperature of 50 to 60 DEG C for 120 to 180 hours.

According to the present invention, Compared with the conventional method in which the effective ingredient of Hwangchujang is extracted with a concentrated solution and the conventional Hwangchujang is simply heated, the concentrate can be easily manufactured while maximizing the efficacy of Hwangchujang.

In addition, the present invention has been optimized through various experiments that can efficiently concentrate without damaging the color, aroma, taste, etc. of hatchery original.

BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 is a diagram showing the overall sequence for a woodchuck concentrate according to the present invention.

For a better understanding of the present invention, a preferred embodiment of the present invention will be described with reference to the accompanying drawings. The embodiments of the present invention may be modified into various forms, and the scope of the present invention should not be construed as being limited to the embodiments described in detail below. The present embodiments are provided to enable those skilled in the art to more fully understand the present invention. Therefore, the shapes and the like of the elements in the drawings can be exaggeratedly expressed to emphasize a clearer description. It should be noted that in the drawings, the same members are denoted by the same reference numerals. Further, detailed descriptions of well-known functions and configurations that may be unnecessarily obscured by the gist of the present invention are omitted.

First, as shown in FIG. 1, the sulfuric acid raw material is introduced into the extractor through steps S101 to S105, the first sulfuric acid concentrated liquid is extracted from the extractor, and the first sulfuric acid concentrated liquid is heated at 75 to 95.degree. The second yellowish concentrate, which has been extracted for 28 hours, is filtered through 80 mesh to 100 mesh and the third yellowish concentrate is sterilized at 80 ° C to 90 ° C for 30 minutes to 60 minutes.

Specifically, in one embodiment of the present invention, the sulfuric acid concentrate is extracted from the extractor at 75 DEG C to 95 DEG C for 16 to 28 hours.

At this time, the extraction temperature and time vary depending on the harvested season.

Depending on the moisture content of the dry ingredients, the extraction temperature and time vary.

The volume ratio of raw material to water is 1: 6 to 10 times the raw material input.

It is heated at room temperature by putting the raw material of yellowing.

Primary enrichment Second enrichment Decompression 0.7 kG 0.1 to 0.2 kG Temperature 50 ° C to 60 ° C
Temperature adjustable 50 ° C to 60 ° C time Time control according to temperature
possible 120 to 180 hours

As shown in Table 1, the concentrate is firstly concentrated to a solid content of 50% or more and secondarily concentrated to a solid content of 65% or more in order to efficiently concentrate the concentrate without damaging the color, flavor,

The primary concentration is 0.7 kG decompression and concentration at 50 ° C to 60 ° C, but the temperature can be controlled according to the concentration time and the like.

The secondary concentration is reduced by 0.1 to 0.2 kG and concentrated at 50 to 60 ° C for 120 to 180 hours to prepare a secondary concentrate in the primary concentrate.

Thereafter, filtration is performed by 80 mesh to 100 mesh to purify.

And labeling according to the Food Sanitation Law, inspection of packaging materials, filling of quantities (240g) and sterilization at 80 ℃ ~ 90 ℃ for 30 ~ 60 minutes.

At this time, it is sterilized in a high-temperature transient heat exchanger (HTST, UHT) or tubular.

After this, the product which has been packed through the property, foreign body, content, and sensory test is inspected and shipped.

According to one embodiment of the present invention, the raw material of Horticultural wood can be extracted into the extractor at a temperature of 70 to 90 ° C for 10 to 18 hours.

In an embodiment of the present invention, saponin is decomposed in the heat at a high temperature of 90 ° C or higher for a long time, so that the saponin content is reduced and the pH is lowered.

The content of saponin in the extracts of yellowtail larvae differed according to the extraction method. The extraction of yellowtail increased sharply from 9 hours at 75 ℃ and increased rapidly from 76 ℃ to 84 ℃ for more than 12 hours. ℃, the content of saponin and so on increases rapidly from 6 hours.

75 ℃ 76 ° C to 84 ° C 85 ° C to 95 ° C Appropriate time 9 12 6 Sensibility (Preference, Preference, 100 out of 100) 90 75 85

As a result of sensory evaluation including taste and preference of 20 persons of the sensory research institute as shown in Table 2, the sensory evaluation was performed at 90 points at 75 ° C, 75 points at 76 ° C to 84 ° C, and 85 points at 75 ° C 85 ° C and 95 ° C, respectively, and the saponin content and the degree of preference did not increase when extracted at a high temperature for a long time.

In general, the extraction rate of solute is proportional to the difference in concentration between the extraction material and the solvent. Therefore, the extraction is firstly carried out for the production of an efficient yellowing extract and the water gradient is added to the remaining yellowing oil to increase the concentration gradient of the solute. Mixing with the extracted yellow juice can increase the saponin content.

The total saponin content of the Huangchil extract increased with increasing extraction time and showed the highest content when extracted for 18 hours. In addition, the content of saponin in the orange juice extracted at 85 ℃ for 12 hours showed the highest content and decreased in the 18 hour extract. The total saponin content of the yellowish liquor extracted at 75 ℃ and 85 ℃ for 6 ~ 12 hours eluted more than 90% of the orange juice extracted for 18 hours.

The content of total saponin in the fermented liquorice extracted twice with the difference of the extraction temperature was higher than the one extracted at 75 ℃ or 85 ℃.

The content of saponin increased with increasing extraction time up to 18 hours at 75 ℃.

When the extraction temperature is lower than 75 캜, extraction of saponin and the like is not perfect and extraction time is long. When the temperature is above 95 캜, weak saponin is broken and loss occurs.

At this time, the extraction temperature and time vary depending on the harvested season, or the extraction temperature and time vary depending on the moisture content of the dry raw material.

After the filtered extract is transferred to the mixing tank, other raw materials and additives are added and mixed. In this case, the compounding temperature is preferably 45 to 65 ° C. When the temperature is lower than 45 ° C, the mixing ratio of the raw material and the additive is considerably lowered. When the temperature is higher than 65 ° C, the mixing ratio is increased and the temperature is increased in advance.

On the other hand, it is sterilized for 30 minutes to 60 minutes at 80 ° C to 90 ° C, and the packaged product is inspected through the property, foreign matter, content, sensory test , The system operator sets each blending ratio of the selected raw materials to the concentrate by a blending ratio program prepared in advance according to the product by the system operator, and in the process of disinfecting the raw materials or packaging them in a small scale, (Amount of loss) can be set in advance and used in consideration of the amount of the liquid.

For this purpose, the equipment identification information of each extractor or identifier can be transmitted to the main server. Here, the identification information of each equipment may include proximity communication identification information (NFC ID) and the like. At this time, the priority information according to the yield can be set in advance according to the importance, and the supply of each of the corresponding raw materials to the equipment identification information can be commanded to the person in charge so that the equipment having a predetermined ranking or more is prepared for the loss in advance according to the ranking ranking.

≪ Example 1-1 >

A liquid tea using the above-mentioned Bulgogi concentrate can be made.

The gruel mass concentrate, the gruel concentrate 0.20 wt%, the fructooligosaccharide 4.00 wt.%, The honey 3.00 wt.%, The honeycomb seed concentrate 90.3 wt.%, The beeswax concentrate 1.00 wt.%, The ginseng fruit concentrate 0.25 wt. , And 0.04% by weight citric acid.

At this time, the yellowtail concentrate is extracted for 12 hours at 85 ° C.

For the production of the Bulgogi tree concentrate, the first extraction is performed, the water is added to the remaining Bulgogi tree to increase the concentration gradient of the solute, and then the second extraction is performed, and then the saponin content is increased by mixing with the first extracted sulfuric acid solution.

≪ Example 1-2 >

A method for preparing a liquid tea using the Bulgogi concentrate is prepared by weighing a Bulgogi concentrate.

The Bulgogi concentrate is placed in an extractor, and the Bulgogi extract is extracted at 85 ° C for 12 hours.

To the extraction tank, 88 wt% to 93 wt% of the above extract was added, and at 45 ° C and 5 ° C, 0.5 wt% to 1.5 wt% of bean curd concentrate, 0.1 wt% to 0.3 wt% of ginseng fruit concentrate, 0.1 to 0.3% by weight of Ganoderma lucidum concentrate, 0.1 to 0.3% by weight of Ganoderma concentrate, 3 to 5% by weight of fructooligosaccharide, 2 to 4% by weight of honey and 0.03 to 0.05% By weight.

Sterilized at a temperature of 90 ° C or higher for 1 hour, filtered through a 1 micron to 25 micron filter, filled in quantitatively, packed and checked after quality inspection.

≪ Example 2 >

First, a certain amount of raw material composed of yellowtail, barley, and sardine is put into the extractor.

The extractor is fed with 0.03-0.05 wt% of the complex mineral relative to the amount of the raw material.

Water heated in the extractor is directly extracted.

After completion of the extraction, the mixture is passed through a heat exchanger and cooled to 20 ° C or lower.

The cooled solution is subjected to primary centrifugation and then filtered with a 1 탆 filter.

The filtered concentrate is transferred to a mixing tank, and then purified water and additives are added thereto. The mixture is mixed at a temperature of 15 to 25 ° C, and the mixture is secondly filtered with a 0.5 μm filter.

The filtered solution is sterilized at 130 ° C to 150 ° C for 30 seconds to 50 seconds in a hot-state heat exchanger (UHT).

The sterilized liquid is cooled to 35 DEG C or lower, and the liquid having been cooled is dosed in a container at room temperature.

Heating the mixture at 88 to 100 ° C for 20 to 30 minutes using the heat exchanger,

The extraction time is varied according to the extraction brix of the concentrate, and the raw materials are added at a ratio of 2.5 to 3 wt% with respect to the amount of heated water.

In order to limit the maximum output value of the conveying pipe motor of the extractor or the motors of the high temperature instantaneous heat exchanger in multiple stages or to limit the output heat source value of the electric hot line of the extractor, TPR (Thyristor Power Regulator) which controls the input power of the extractor or the like or the motor speed at a constant level can be used for several minutes to several minutes.

In particular, the heat treatment of the high-temperature instantaneous heat exchanger not only inhibits the growth of microorganisms but also affects the quality of the concentrate itself (nutrient destruction, flavor and texture loss, etc.). Therefore, the above-described apparatus or a device described below may be used to sterilize the liquid at a predetermined stage, and nonthermal sterilization may be further performed.

For example, sterilization of packed or unpacked Bulgogi concentrate using a Teflon-coil UVC system such as ultraviolet sterilization, filter sterilization, high hydrostatic pressure technology (HHP) Can be used.

In addition, it is also possible to use a tube made of quartz material because of the characteristic that ultraviolet sterilizing wavelength should be transmitted well. That is, when a small quartz tube of generally small size is replaced with a Teflon tube, it is also preferable to use a quartz tube because the tube may be crushed by the pressure of the fluid.

(PID) operation in accordance with a control deviation from a value obtained by feedback and digitally converting an output signal for driving an inverter motor of the high temperature instantaneous heat exchanger, and outputs a control signal through calculation A PLC control unit for controlling the motor and operating the low load mode in which the motor is intermittently operated for a predetermined period of time when the sterilization is completed and when the concentration is completed, Can be used.

In one embodiment of the present invention, the sulfuric acid concentrate is extracted from the extractor at 75 DEG C to 95 DEG C for 16 to 28 hours.

At this time, the extraction temperature and time vary depending on the harvested season. Depending on the moisture content of the dry ingredients, the extraction temperature and time vary.

In order to avoid a sudden supply of power to the load at the first start after the power-on of the extractor, it is necessary to gradually raise the output to the set value of the control signal, or to perform a zero crossing control or a phase angle control And an angle control unit (not shown).

The first concentration is performed at a reduced pressure of 0.7 kG and the second concentration is performed at a reduced pressure of 0.1 to 0.2 kG and a concentration of 50 to 60 ° C for 120 to 180 hours. The control unit controls the control unit so that the power source is preheated and the power source is preheated in order to gradually increase the concentration of the yellowing liquid in the extractor so that the number of revolutions of the inverter motor for reducing the pressure is gradually reduced around the time when the concentration is completed. The power of the inverter motor of the air diffuser and the blower is slowly turned on by the phase control method and the power is turned off after a certain time that the inverter motor is completely stopped and the power of the inverter is turned off by using the phase control method of the phase controller, According to the phase control method, when the sterilization is completed, the inverter motor is slowly rotated By turning on / off operation, the rotation speed of the inverter motor can be switched accurately and stably according to the temporal change according to the change characteristics of ORP and PH.

Claims (5)

The second crude oil concentrate is extracted from the first crude oil concentrate at 75 ° C to 95 ° C for 16 to 28 hours and filtered through 80 mesh to 100 mesh, Purified yellow pepper concentrate which has been sterilized at 80 ° C to 90 ° C for 30 minutes to 60 minutes. The method according to claim 1,
Wherein the volume ratio of the raw material of yellowing raw material to the volume of water is 1: 6 to 10 times as much as the input amount of the greening raw material. The method according to claim 1,
Characterized in that the concentrate is first concentrated to a solid content of 50% or more and secondarily concentrated to a solid content of 65% or more in order to efficiently concentrate the concentrate without damaging the inherent color, concentrate. The method according to claim 1,
Wherein the primary concentration of the second sulfuric acid concentrate is 0.7 kG decompression and concentration at 50 캜 to 60 캜, but the temperature can be controlled according to the concentration time. The method according to claim 1,
Wherein the second sulfuric acid concentrate is concentrated at a reduced pressure of 0.1 to 0.2 kG and at a temperature of 50 to 60 DEG C for 120 to 180 hours.

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