KR20170007032A - A cosmetic composition containing flower extract of Heptacodium miconioides and extraction method of flower extract of Heptacodium miconioides - Google Patents

A cosmetic composition containing flower extract of Heptacodium miconioides and extraction method of flower extract of Heptacodium miconioides Download PDF

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Publication number
KR20170007032A
KR20170007032A KR1020150098630A KR20150098630A KR20170007032A KR 20170007032 A KR20170007032 A KR 20170007032A KR 1020150098630 A KR1020150098630 A KR 1020150098630A KR 20150098630 A KR20150098630 A KR 20150098630A KR 20170007032 A KR20170007032 A KR 20170007032A
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extract
water
present
flower
extracting
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KR1020150098630A
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Korean (ko)
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이희준
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이희준
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to a cosmetic composition containing an extract of Liliaceae and a method of extracting Liliaceae.
The present invention relates to a cosmetic composition containing a lavender oil extract,
A step of applying a C1 to C4 alcohol, preferably anhydrous methanol or ethanol and water, to the volumetric flower; And extracting the dried flower with the solvent by heating at a predetermined temperature for a predetermined time in an extractor equipped with a reflux condenser.

Description

[0001] The present invention relates to a cosmetic composition containing an extract of Lilium japonica and a method of extracting it from a flower extract of Heptacum miconioides,

The present invention relates to a cosmetic composition comprising an extract of Liliaceae and a method for extracting Liliaceae. More particularly, the present invention relates to a functional cosmetic composition comprising an extract extracted from a flower of a flower belonging to the genus Phalaenopsis, and a method for extracting the extract from the flower.

As a functional cosmetic composition, a composition is extracted from various flowers and used.

Korean Patent No. 10-0901638 (Jun. 01, 2009) discloses a composition for inhibiting SNARE complex formation containing a flower extract.

The patented invention is characterized in that the patented invention relates to a method for producing a flower of the present invention, which comprises at least one member selected from the group consisting of flower buds such as tiger, willow, Discloses a composition containing an extract obtained from Seed Tree, Raji Yang, Negesvari, Raj briksha, Dhayaro, laurel and mashing.

However, the patented invention has a problem in that it is not effective as a composition of a functional cosmetic composition because the elastase inhibitory and antioxidative effects to be contained in the cosmetic composition are insufficient.

Therefore, there is a need for an invention that has improved inhibition of elastase and antioxidant efficacy.

Korean Patent No. 10-0901638 (Date of Registration June 01, 2009)

It is an object of the present invention to solve the problems of the prior art, and an object of the present invention is to provide a cosmetic composition containing an extract of Liliaceae. It is another object of the present invention to provide a method for extracting flower seeds.

As a technical solution for achieving the object of the present invention, as a first aspect of the present invention, there is provided a cosmetic composition containing an extract of Liliaceae.

According to a second aspect of the present invention, there is provided a cosmetic composition comprising a lavender flower extract obtained by extracting a lavender flower powder with at least one solvent selected from the group consisting of water, an alcohol having 1 to 4 carbon atoms and a mixed solvent thereof do.

In a third aspect of the present invention, 1000 ml of a C1 to C4 alcohol, preferably anhydrous methanol or ethanol and water, is added to 100 g of the present invention, and the mixture is heated at 60 to 90 DEG C for 1 to 30 minutes, A method of extracting a seven-milliliter flower extract extracted with warming for 2 hours and 30 minutes is presented.

According to a fourth aspect of the present invention, there is also provided a method for producing a quinone flower, comprising the steps of: extracting quartz flower powder with at least one solvent selected from the group consisting of water, an alcohol having 1 to 4 carbon atoms and a mixed solvent thereof; Suspending the extracted extract in water, and then sequentially fractionating the extract with hexane, dichloromethane, ethyl acetate and butanol.

According to a fifth aspect of the present invention, there is also provided a method for producing a liquefied petroleum distillate; A pressurizing step of putting a solvent containing a sample in a chamber of an ultra high pressure machine and extracting it by applying an ultrahigh pressure of 100 MPa or more; A separation / purification step of separating the extract from the sample; And a step of lyophilizing or concentrating the purified extract.

According to the present invention, an antioxidant component and an anti-inflammatory component of the extract extracted from the luciferase can provide an elastase inhibitor, an antioxidant and a anti-inflammatory functional cosmetic composition.

1 is an indication of the efficacy as an elastase inhibitor of the present invention.
FIG. 2 is a free radical scavenging test analysis chart for examining the antioxidant efficacy of the present invention.
FIG. 3 is a flow chart for explaining an embodiment of the method of extracting the flower of the present invention.
FIG. 4 is a flowchart for explaining another embodiment of the method for extracting Lycoris chejuensis from the present invention.
FIG. 5 is a flow chart for explaining another embodiment of the method for extracting the flower of the present invention.

Hereinafter, embodiments of the present invention will be described in detail with reference to the accompanying drawings.

The quartz crystal which is a subject of the present invention has the following characteristics.

[bottom]

Scientific name: Heptacodium miconioides (七 子 花))

Family name:

Name: Seven-Son Flower

It has a height of 4-6 m and is bloomed from August to November. It is first known as a garden where the white creamy flowers of jasmine fragrance are bloomed and then red rose flowers bloom. The country of origin is also known as China, and is called the seven flower because it has seven flowers in the stem.

 In the present invention, the flower part of the lacquer is used.

 The composition containing the Lilium chrysanthemum extract of the present invention includes components commonly used in cosmetics in addition to the extract described in this specification as an active ingredient. Such ingredients include, but are not limited to, conventional adjuvants and carriers such as, for example, elastase inhibitors, antioxidants, anti-inflammatory agents and fragrances.

The cosmetic composition containing the Lilium chrysanthemum extract of the present invention is selected from cosmetic composition or ointment of formulation of lotion, gel, water-soluble liquid, cream, essence, oil-in-water (O / W) type and water-in-oil .

The composition of the present invention containing the Lilium chrysanthemum extract of the present invention can be prepared into any of the formulations conventionally produced in the art, and examples thereof include solutions, suspensions, emulsions, pastes, gels, creams, lotions, powders, Containing cleansing, oils, powder foundations, emulsion foundations, wax foundations and sprays, and the like.

When the formulations of the present invention are pastes, creams and gels, animal oils, vegetable oils, waxes, paraffins, starches, tracants, cellulose derivatives, polyethylene glycols, silicones, bentonites, silicas, talc and zinc oxide are used as carrier components But are not limited thereto.

When the formulation of the present invention is a powder and a spray, lactose, talc, silica, aluminum hydroxide, calcium silicate and polyamide powder can be used as a carrier component. In particular, in the case of spray, a mixture of chlorofluorohydrocarbons, propane / Propane, < / RTI > butane, and dimethyl ether.

When the formulation of the present invention is a solution or emulsion, a solvent, a solubilizing agent and an emulsifying agent are used as a carrier component, and examples thereof include water, ethanol, isopropanol, ethyl carbonate, ethyl acetate, benzyl alcohol, benzyl benzoate, , 3-butyl glycol oil, glycerol aliphatic esters, polyethylene glycols and fatty acid esters of sorbitan.

When the formulation of the present invention is a suspension, the carrier component may include water, a liquid diluent such as ethanol and propylene glycol, a suspension such as ethoxylated isostearyl alcohol, polyoxyethylene sorbitol ester and polyoxyethylene sorbitan ester, Castor cellulose, aluminum metahydroxide, bentonite, agar and tracant, but are not limited thereto.

When the formulation of the present invention is an interfacial active agent-containing cleansing, the carrier component may include aliphatic alcohol sulfate, aliphatic alcohol ether sulfate, sulfosuccinic acid monoester, isethionate, imidazolinium derivative, methyltaurate, sarcosinate, fatty acid amide Ether sulfates, alkylamidobentanes, aliphatic alcohols, fatty acid glycerides, fatty acid diethanolamides, vegetable oils, lanolin derivatives, and ethoxylated glycerol fatty acid esters.

As a specific phenomenon of skin aging, reduction of collagen and elastin in skin dermis, reduction of mucopolysaccharide including hyaluronic acid, damage of cells due to ultraviolet rays, and the like are known. Among them, elastin contributes to the elasticity of the tissue by making crosslinks with each other. However, when the elastin degrading enzyme, elastase, is over-expressed by ultraviolet light exposure or the like, for example, the elastin is denatured or destroyed, I think. Therefore, it is important to prevent degeneration and destruction of elastin, which inhibits the action of elastase and imparts elasticity and tautness to the skin, to prevent aging of the skin.

The present inventors investigated the inhibition of elastase activity on various plant extracts, and found that the solvent extract of lucidum flowers has an inhibitory activity of elastase activity.

Fig. 1 is a graph showing the inhibition of the elastase activity of the Lilium japonica flower extract of the present invention.

The active oxygen species are energetic and highly reactive, which accelerate skin aging by disrupting the enzymatic and non-enzymatic antioxidant defense system of the skin, thus controlling enzymatic and non-enzymatic oxidation by active oxygen. very important. Many antioxidants have been developed to inhibit reactive oxygen species associated with such skin aging.

The inventor of the present invention found that the extract of Liliaceae has high antioxidant activity.

The absorbance of the stable DPPH exhibits the maximum absorbance at 540 nm. As the free radical DPPH is cleared by the quencher flower extract sample, the purple to transparent color, that is, as the free radical scavenging ratio is increased, the absorbance at the wavelength of 540 nm Free radical scavenging test was applied.

FIG. 2 is a free radical scavenging test analysis chart for antioxidant activity test of the present invention.

FIG. 3 is a flow chart for explaining an embodiment of the method of extracting the flower of the present invention. As shown in FIG. 3, the extract method of the present invention comprises a solvent administration step (S100) in which 1000 ml of a C1 to C4 alcohol, preferably anhydrous methanol or ethanol, and water are added to 100 g of a quercus flower; And a step (S110) of extracting the quartz flower composition by warming the quartz flower administered with the solvent at a predetermined temperature for a predetermined time in an extractor equipped with a reflux condenser.

The temperature in the extractor is preferably 60 to 90 占 폚, and the heating time is preferably 1 to 30 minutes to 2 hours and 30 minutes.

In addition, in the above example, 100 g of white lycopene was washed with purified water and dried. Then, 1000 ml of anhydrous methane, ethanol and water were added, and the mixture was warm-extracted at 80 ° C for 2 hours in an extractor equipped with a reflux condenser. The remaining residue is further extracted one or more times by the same method as described above, and the filtered extract is combined, concentrated under reduced pressure, and lyophilized to obtain a dried extract.

FIG. 4 is a flowchart for explaining another embodiment of the method for extracting Lycoris chejuensis from the present invention. As shown in FIG. 4, the extraction method of the present invention comprises extracting the three-dimensional flower powder with at least one solvent selected from the group consisting of water, an alcohol having 1 to 4 carbon atoms, and a mixed solvent thereof S200); Suspending the extracted extract in water, and then sequentially fractionating the extract with hexane, dichloromethane, ethyl acetate and butanol (S210).

FIG. 5 is a flow chart for explaining another embodiment of the method for extracting the flower of the present invention. As shown in FIG. 5, the extract method of the present invention comprises a step (S300) of adding a solvent to a lavender flower sample; A pressurization step (S310) of adding a solvent containing a sample in a chamber of an ultra high-pressure machine and extracting it by applying an ultrahigh pressure of 100 MPa or more; A separation / purification step (S320) of separating the extract from the sample; And lyophilizing or concentrating the purified extract (S330).

The embodiments of the present invention described above are only a few of various embodiments of the present invention. It is a matter of course that various methods of extracting the cosmetic composition containing the Lilac flower extract and the Lilac flower extract are within the scope of the present invention.

Claims (5)

A cosmetic composition containing an extract of Lilac. The method according to claim 1,
Wherein the cosmetic composition is selected from cosmetic compositions or ointments in the form of a lotion, a gel, a water-soluble liquid, a cream, an essence, an oil-in-water (O / W) type and a water-in-oil (W / O) type.
A step of applying a C1 to C4 alcohol, preferably anhydrous methanol or ethanol and water, to the volumetric flower; And extracting the quercus flowers to which the solvent has been administered by heating at a predetermined temperature for a predetermined time in an extractor equipped with a reflux condenser. Extracting the volumetric flour powder with at least one solvent selected from the group consisting of water, an alcohol having 1 to 4 carbon atoms, and a mixed solvent thereof; Suspending the extracted extract in water, and then sequentially fractionating the extract with hexane, dichloromethane, ethyl acetate and butanol. Adding a solvent to the sieved flower sample; A pressurizing step of putting a solvent containing a sample in a chamber of an ultra high pressure machine and extracting it by applying an ultrahigh pressure of 100 MPa or more; A separation / purification step of separating the extract from the sample; And lyophilizing or concentrating the purified extract.
KR1020150098630A 2015-07-10 2015-07-10 A cosmetic composition containing flower extract of Heptacodium miconioides and extraction method of flower extract of Heptacodium miconioides KR20170007032A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112641819A (en) * 2020-12-30 2021-04-13 台州学院 Application of flos heptadendri chinensis extract in preparation of ATP citrate lyase inhibitor

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100901638B1 (en) 2009-03-23 2009-06-09 성균관대학교산학협력단 SNARE complex formation inhibiting composition comprising natural extracts

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100901638B1 (en) 2009-03-23 2009-06-09 성균관대학교산학협력단 SNARE complex formation inhibiting composition comprising natural extracts

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112641819A (en) * 2020-12-30 2021-04-13 台州学院 Application of flos heptadendri chinensis extract in preparation of ATP citrate lyase inhibitor
CN112641819B (en) * 2020-12-30 2022-07-26 台州学院 Application of flos heptadendri chinensis extract in preparation of ATP citrate lyase inhibitor

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