KR20150098410A

KR20150098410A - Hair treatment composition containing oriental plant extracts

Info

Publication number: KR20150098410A
Application number: KR1020140019672A
Authority: KR
Inventors: 김혜균; 성은동; 유성일
Original assignee: 우송대학교 산학협력단; 주식회사 이숨
Priority date: 2014-02-20
Filing date: 2014-02-20
Publication date: 2015-08-28

Abstract

According to one aspect of the present invention, there is provided a composition for hair treatment comprising, as an active ingredient, a Sucrose extract, a Rhizome extract, a Yulmu extract, and a Burdock extract.
According to another aspect of the present invention, there is provided a method for preparing a composition comprising the steps of: preparing Sasa extract, Rhizobium extract, Rhizome extract and Burdock extract; Mixing 2.0 to 5.0 parts by weight of the above-prepared sucralose extract, 0.5 to 2.0 parts by weight of a zoosulfur extract, 0.5 to 2.0 parts by weight of a yulmu extract, and 0.5 to 2.0 parts by weight of a burdock extract; And mixing said mixed extract with at least one member selected from the group consisting of an amino acid complex, a hydrolyzed silk, a flavoring agent, a ceramide, an excipient, and purified water, There is provided a method for preparing a composition for treating hair, wherein at least one selected from the group consisting of the above-mentioned Sucrose extract, Ziwu extract, Yulmu extract and burdock extract is extracted with alkaline ionized water.

Description

TECHNICAL FIELD [0001] The present invention relates to hair treatment compositions containing oriental herbal extracts,

The present invention relates to a composition for treating hair containing a herbal extract, and more particularly to a hair treatment composition containing a herbal extract, To a composition for treating hair.

Hair is composed of cuticle, cortex, and medulla, and is known to be damaged by various factors such as heat, light, and chemicals.

The cuticle affects hair protection, luster, softness, etc., and is composed of 5 to 10 fold scaly shapes, accounting for about 10 to 15% of the entire hair, and has the properties of water repellency, lipophilicity and chemical resistance have. The cortex occupies about 85 to 90% of the entire hair, and the cortical cells, the insect material (50%), and each fibrous fiber take a helix structure.

The medulla is a central part of the hair that contains minute air and is known to affect the elasticity, strength, and shine of the hair. The outermost tissue of the above hair structure is a cuticle.

The cuticle protects the tissues in the hair from damage and is located at the outermost position to determine the actual hair filling. However, the cuticle may lose its function due to various physical and chemical stimuli such as external temperature, humidity change, pollutants, stress, and lack of influence, and furthermore, the protective function is lost, The recovery of the damaged hair becomes impossible.

In this regard, various attempts have been made to prevent or ameliorate the hair damage. As one of such attempts, silicone oils such as dimethylpolysiloxane and high molecular weight methylphenylpolysiloxane, ester oils, An oil component such as hydrocarbon oil is utilized.

Particularly, the silicone oil has a low surface tension and is excellent in familiarity with the hair and is widely used because of its good gloss. However, the limit of the blending property unique to the oil component is confirmed, and excessive use of oil for a long time .

Therefore, there is an increasing demand for a product for protection of cuticle, and it is an object of the present invention to provide a composition for treating hair using natural ingredients capable of minimizing irritation to human body while improving the condition of damaged hair, Development is required.

In order to solve the above-mentioned problem, in order to develop a novel substance having high biostability and excellent scalp and hair improving effect, the extracts of Hashuo, hwanghwang, yulmu and burdock are less stimulated to the human body, And completed the present invention.

In addition, we tried to maximize the effect of the mixed extract by differentiating the extraction method.

According to one aspect of the present invention, there is provided a composition for hair treatment comprising, as an active ingredient, a Sucrose extract, a Rhizome extract, a Yulmu extract, and a Burdock extract.

According to one embodiment, the effective ingredient may include 2.0 to 5.0 parts by weight of the extract of Soso, 0.5 to 2.0 parts by weight of a zoosulfur extract, 0.5 to 2.0 parts by weight of an extract of yomu, and 0.5 to 2.0 parts by weight of a burdock extract.

According to one embodiment, the total weight of the Sucrose extract, Zyprexa extract, Yulmu extract and burdock extract may be 50.0 to 95.0 parts by weight based on 100 parts by weight of the hair treatment composition.

According to one embodiment, the composition for hair treatment comprises at least one selected from the group consisting of an amino acid complex, a hydrolyzed silk, a flavoring agent, a ceramide, an excipient, As shown in FIG.

According to one embodiment, at least one selected from the group consisting of the extract of Soso, the extract of Rhizobia, the extract of Yumulmu, and the Burdock Extract may be extracted as alkaline ionized water.

The composition may be a formulation selected from the group consisting of shampoo, rinse, pomade, paste, cream, treatment, serum, hair lotion or essence.

According to another aspect of the present invention, there is provided a method for preparing a composition comprising the steps of: preparing Sasa extract, Rhizobium extract, Rhizome extract and Burdock extract; Mixing 2.0 to 5.0 parts by weight of the above-prepared sucralose extract, 0.5 to 2.0 parts by weight of a zoosulfur extract, 0.5 to 2.0 parts by weight of a yulmu extract, and 0.5 to 2.0 parts by weight of a burdock extract; And mixing said mixed extract with at least one member selected from the group consisting of an amino acid complex, a hydrolyzed silk, a flavoring agent, a ceramide, an excipient, and purified water, There is provided a method for preparing a composition for treating hair, wherein at least one selected from the group consisting of the above-mentioned Sucrose extract, Ziwu extract, Yulmu extract and burdock extract is extracted with alkaline ionized water.

The above-mentioned mixed extract of Hashuro, hwanghwang, yulmu and burdock provide nutrients to the hair to keep the hair healthy and prevent the damage, minimize the irritation to the human body, prevent and improve the scalp trouble and itch to clean the hair Keep it healthy.

It should be understood, however, that the effects of the present invention are not limited to the above-described effects, but include all effects that can be deduced from the detailed description of the present invention or the configuration of the invention described in the claims.

1 is a flowchart illustrating a method of manufacturing a composition for hair treatment according to an embodiment of the present invention.

As used herein, the terminology used herein is intended to encompass all commonly used generic terms that may be considered while considering the functionality of the present invention, but this may vary depending upon the intent or circumstance of the skilled artisan, the emergence of new technology, and the like. Also, in certain cases, there may be a term selected arbitrarily by the applicant, in which case the meaning thereof will be described in detail in the description of the corresponding invention. Therefore, the term used in the present invention should be defined based on the meaning of the term, not on the name of a simple term, but on the entire contents of the present invention.

Unless defined otherwise, all terms used herein, including technical or scientific terms, have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. Terms such as those defined in commonly used dictionaries are to be interpreted as having a meaning consistent with the contextual meaning of the related art and are to be interpreted as either ideal or overly formal in the sense of the present application Do not.

Hereinafter, embodiments of the present invention will be described in detail, but it should be apparent that the present invention is not limited by the following examples.

Composition for hair treatment

The composition for hair treatment of the present invention may contain, as an active ingredient, a mushroom extract, a ziwu extract, a yulmu extract, and a burdock extract.

Pleuropterus multflorus is a medicinal plant that has been cultivated for a long time because of its origins in China. It has no hair on the whole, and its roots grow into the ground and sometimes form round root roots. do.

The root of the root is used as a medicinal herb in a herbal medicine, and it is known that it has an effect of a tonic, a gangjeong, a blood-sucking, an interpolation, a giant wind, and a scion. It is used as a remedy for symptoms such as weakness of the body, back pain, arteriosclerosis, positive blood pressure, hypertension, chronic hepatitis, tuberculous lymphadenitis, enteritis, swelling and constipation.

The Rehmannia glutinosa ) is a perennial plant of the dicotyledonous plant monocotyledonous ginseng grown as a medicinal plant. The roots are thick and fleshy, with reddish brown and sideways. The stem stands straight, 20-30 cm high and has a glandular hair. Leaves from roots are united, long elliptical shape, dull end, pointed bottom, wavy sawtooth on edge, wrinkled leaf surface, and vein on back. Leaves hang on the stem.

In one room, it is said that the raw thing of the root is the raw persimmon, the dried persimmon, and steamed and dried persimmon. It is used for the weakness, weakness, weakness, weakness of the child, dementia, premature ejaculation, and erectile dysfunction, and it is used for the fragile constitution, hematemesis, nosebleed, uterine bleeding, menstrual impurity and constipation. It is effective in thirst and throat caused by heat inside the organ, and it stops the blood and nosebleeds.

The Coix lachrymajobi there is . mayuen ) is also known as the runner, the inhabitant, the meaning (薏米) of the annual plant of the unicorn plant lepidoptera. The stomach grows hard and straight, and branches are divided. Leaves are sloping and narrow, with a width of about 2.5cm, with the lower part becoming a sheath. The flower blooms in July-September, and the flower ear of about 3cm in length runs on the end of the flower ear which comes out from the leaf axil. There is a female flower eagle wrapped in an oval sheath at the bottom. The bract is rigid and elliptical in shape and is about 1.2cm long and ripened to blackish brown. When the ovary matures, the leaf sheath becomes hard and becomes dark brown.

The yulmu is a naturalized plant derived from China and cultivated as a medicinal crop. Seed is called 薏苡仁 (薏苡仁), eat tea, diuretic, analgesia, gyeonggyeong, tonic action, edema, neuralgia, rheumatism, bladder stones are used as medicines. Leaves are used as tea substitutes, and roots are used for jaundice and neuralgia. The leaves on the stem are also used as feed.

The burdock ( Arctium lappa ) is a biennial plant of the dicotyledonous plant Lachrymaceae. It is about 50 ~ 150cm high. Straight roots grow 30 ~ 60cm and stem comes out from the end. The leaves on the roots come out in rows and the petiole is long. It is staggered and heart-shaped in the trunk. The outer surface is dark green, but the back side has dense white fur, and this shape has sawtooth on the edge.

The burdock is a naturalized plant derived from Europe. It is used as a diuretic and sweating agent in Europe. The seed is used as a diuretic when there is a swelling and is used as an antidote to sore throat and poisonous insect.

According to one embodiment, the effective ingredient may include 2.0 to 5.0 parts by weight of the extract of Soso, 0.5 to 2.0 parts by weight of a zoosulfur extract, 0.5 to 2.0 parts by weight of a yulmu extract and 0.5 to 2.0 parts by weight of a burdock extract, no.

The term " extract " as used herein refers to a solvent in which the active ingredient contained in the extraction material has been transferred by contacting the solvent with the extraction material under specific conditions.

When the variation of the blending ratio of each of the above extracts is large, the hair improving effect derived from the active ingredient of each of the extracts is not adequately exhibited. Therefore, the blending ratio can be appropriately controlled in consideration of the working environment and the quality of the final product, Preferably, the extracts can be mixed in equal proportions so that the efficacy of each extract is integrated to maximize the hair-improving effect.

The type of the solvent for preparing the extract is not particularly limited, and various solvents may be used as needed. In general, when extracting an active ingredient with an ethanol aqueous solution as a solvent, a step of evaporating the solvent separately is required, so that the manufacturing process is complicated, and various chemical components such as alcohol The useful active ingredient may be destroyed or lost during the volatilization process.

Therefore, according to one embodiment, at least one selected from the group consisting of the extract of Soso, the extract of Rhizobium, the extract of Yomun, and the extract of Burdock can be extracted with alkaline ionized water.

The alkaline ionized water refers to water containing an alkaline mineral. It is typically prepared by electrolysis of drinking water and has a hydrogen ion concentration (pH) of about 8.0 to 12.0. The alkaline ionized water is rapidly absorbed by the human body and is combined with the acidic waste matter to be discharged to the outside of the human body. It is also known to prevent and treat adult diseases and promote the generation of the brain and bone of the fetus when pregnant women drink, and alleviate morning sickness.

When the alkaline ionized water is extracted as a solvent, the extractability of the oil-soluble active ingredient is increased due to addition of the alkaline water lipolytic property in addition to general water-soluble hot water extraction. Since the component is not extracted, the effect of improving the hair of the hair treating composition can be further enhanced.

The alkaline ionized water is produced in the negative electrode when the negative (-) electrode and the positive (+) electrode are placed in a water bath and electrolyzed, and the extract is prepared using the alkaline ionized water as a solvent.

If the mixed extract of Sasa, Rhododendron, Rhizoma, and Burmese is less than 50.0 parts by weight based on 100 parts by weight of the total amount of the hair treatment composition, the excellent efficacy of the active ingredient contained in the mixed extract may not be exerted adequately, The specific gravity of the other additives contained in the product for commercialization is excessively low, so that the desired feeling or property can not be realized.

The amino acid complex refers to a complex composition comprising at least one amino acid, which is a basic constituent unit of a protein, and the type or mixing ratio of the amino acid to be mixed is not particularly limited and may be varied according to need. The amino acid complex imparts moisturizing power to the skin and imparts radiance to the hair, thereby improving the feeling of use of the hair treatment composition and minimizing irritation to the skin.

Refers to water or dilute ethanol containing peptides obtained by hydrolyzing the hydrolyzed silk silk fiber with acid or alkali, and is often used for skin or hair conditioning agents. The hydrolyzed silk is a constituent of a protein, which is safe for human body, imparts shine and elasticity to hair, and restores damaged hair.

The above-mentioned flavoring agent refers to a substance to be added to flavor by putting into foods or cosmetics and has excellent volatility at room temperature, and may be added as needed for commercialization of the hair treating composition. The kind of the above-mentioned flavoring agent is not particularly limited, and aromatic chemicals, essential oils, natural extracts, distillates, isolated components, aromas, resinous resins and the like can be used.

Ceramide, which accounts for about 40% or more of intercellular lipid that constitutes the stratum corneum of the skin, is an essential ingredient to show the structure and function of the stratum corneum. It has a hydrophilic group and a lipophilic group, It prevents you from doing. The ceramides have a function of forming a water film on the hair to suppress evaporation of water and protect the hair, so that the ceramide can be added as a raw material for a moisturizer.

The excipient refers to a substance to be added in order to impart appropriate hardness or shape to the drug or to make it easy to handle with a certain volume and weight when the amount of the main agent is insufficient, Is not particularly limited, but lactose, starch, dextrin, glycerin, cellulose and the like can be used.

The Purified Water refers to purified water in which impurities are removed through distillation or an ion exchange resin, and may be added to supply water to the hair and to dissolve the active ingredient of the various additives or the extract. In the case of conventional water, unnecessary components are contained, and propagation of germs is facilitated, so that the hair treating composition has high possibility of decay and oxidation, and therefore, it is preferable to use purified water of high purity.

The hair treatment composition may contain various additives such as an emulsifier, a preservative, a diluent, and a pigment in consideration of the functions and uses of the hair treatment composition as well as the additives.

The composition for hair treatment may be formulated into, but not limited to, shampoo, rinse, pomade, paste, cream, treatment, serum, hair lotion or essence.

In the respective formulations, components other than the above-mentioned essential ingredients can be appropriately selected and blended by those skilled in the art depending on the use of the external preparation, the purpose of use, and the like.

For example, when the composition is a paste, a cream or a gel, an animal fiber, a plant fiber, a wax, a paraffin, a starch, a tracer, a cellulose derivative, polyethylene glycol, silicon, bentonite, silica, talc or zinc oxide Can be used.

In addition, when the composition is a powder or a spray, lactose, talc, silica, aluminum hydroxide, calcium silicate or polyamide powder may be used as a carrier component. In particular, chlorofluorohydrocarbons, propane, butane Or a propellant such as dimethyl ether.

When the composition is a solution or an emulsion, a solvent, a solvent or an emulsifying agent may be used as a carrier component. Examples of the solvent include water, ethanol, isopropanol, ethyl carbonate, ethyl acetate, benzyl alcohol, benzyl benzoate, 1,3-butyl glycol oil, glycerol aliphatic ester, polyethylene glycol or fatty acid esters of sorbitan can be used.

In addition, when the composition is in the form of a suspension, the carrier component may be a liquid diluent such as water, ethanol or propylene glycol, a suspending agent such as ethoxylated isostearyl alcohol, polyoxyethylene sorbitol ester and polyoxyethylene sorbitan ester, Cellulose, aluminum metahydroxide, bentonite, agar or tracant, etc. may be used.

Method for manufacturing composition for hair treatment

Fig. 2 is a flow chart of a method for manufacturing a composition for hair treatment according to an embodiment. Fig.

As shown in FIG. 1, the method for preparing a hair treating composition comprises the steps of: preparing an extract for Hwaseo, gujwang, yulmu, and burdock; mixing the extract at a certain mixing ratio; and mixing the mixed extract with other additives Step < / RTI >

The kind of the solvent for preparing the extract is not particularly limited and various solvents may be used as needed. Preferably, the extract is at least one selected from the group consisting of the extract of Soso, the extract of Rhizobia, It can be extracted with alkaline ionized water.

According to one embodiment, the extracts of Hashuo, Rhizophora, Rhodophyta, Rhodiola and Burmese mixed extracts are dried at about 1 to 20 times, preferably about 10 to 15 times, Of alkaline ionized water as a solvent.

Each of the dried raw materials may be finely pulverized or pulverized prior to extraction in consideration of extraction efficiency.

At this time, the temperature and time for extraction are not particularly limited, but can be set at 1 to 60 캜, preferably 20 to 40 캜 for 1 to 30 days, preferably 1 to 15 days, Or at a temperature of 70 to 120 DEG C, preferably 80 to 100 DEG C for about 30 minutes to 2 days, preferably about 1 hour to 1 day.

Since the extraction temperature greatly affects the extraction speed, the extraction temperature can be appropriately adjusted in consideration of the quality of the product, the use, the working environment, and the productivity.

Hereinafter, the present invention will be described in more detail by way of examples.

Manufacturing example 1-1. Sewage Preparation of extract

500 g of dried seaweed was added to 5 kg of alkaline ionized water, and the mixture was heated at 60 ° C for 6 hours for extraction, filtered through 400 mesh filter cloth, cooled to room temperature, allowed to stand at 5 to 15 ° C for 5 days and then aged and filtered through a 0.45 mm filter. The filtrate was concentrated in a rotary evaporator under reduced pressure to remove the solvent to obtain 14.3 g of a sulfo extract.

Manufacturing example 1-2. Manufacture of hibiscus extract

16.2 g of a crude extract was obtained in the same manner as in Preparation Example 1-1, except that rhizome was used as an extracting raw material.

Manufacturing example 1-3. Preparation of yulmu extract

12.2 g of yulmu extract was obtained in the same manner as in Preparation Example 1-1, except that yulmu was used as an extraction raw material.

Manufacturing example 1-4. Manufacture of burdock extract

14.0 g of burdock extract was obtained in the same manner as in Preparation Example 1-1, except that burdock was used as the raw material for extraction.

Manufacturing example 2. Preparation of mixed extract

Mixed extracts were prepared by mixing the extracts of Hashuo, Rhizophora, Radix, and Burdock of Preparation Examples 1-1 to 1-4 at a ratio of 1.5: 1.5: 1.5: 1.5.

Example . Preparation of composition for hair treatment

The composition for hair treatment was prepared according to the following Table 1. The amino acid complexes were prepared by mixing valine, glutamic acid, cysteine, lysine, and tryptophan at the same weight ratio. In each of the examples, the same amount of purified water was added to the mixed extract instead of the mixed extract.

Further, as a comparative example, a composition not containing the mixed extract was prepared

Compounding ingredient Example 1
(weight%) Example 2
(weight%) Example 3
(weight%) Example 4
(weight%) Example 5
(weight%) Comparative Example
(weight%) Mixed extract 50.00 60.00 70.00 80.00 90.00 0 Alkaline ionized water 0 0 0 0 0 90 Amino acid complex 2.50 2.50 2.50 2.50 2.50 2.5 Hydration
Silk protein 1.00 1.00 1.00 1.00 1.00 1.00 Flavoring agent a very small amount a very small amount a very small amount a very small amount a very small amount a very small amount Ceramide a very small amount a very small amount a very small amount a very small amount a very small amount a very small amount Excipient handful handful handful handful handful handful Purified water Balance Balance Balance Balance Balance Balance system 100.00 100.00 100.00 100.00 100.00 100.00

Experimental Example 1. Evaluation of skin irritation

In order to examine the degree of skin irritation in the above Examples and Comparative Examples, the skin irritation degree was evaluated by patch test for 50 days for each male and female experimenter for 2 days.

The evaluation criteria are classified into stimulus (0), normal (1), and non-stimulus (2), and the average values are shown in Table 2.

division Example 1
(weight%) Example 2
(weight%) Example 3
(weight%) Example 4
(weight%) Example 5
(weight%) Comparative Example
(weight%) After 1 day 1.15 1.18 1.19 1.16 1.25 0.97 Two days later 1.10 1.17 1.10 1.08 1.17 0.93

As shown in Table 2, the comparative example was shown to be more irritating than the example, and no significant difference was shown between the respective examples.

Experimental Example 2. Moisture resistance evaluation

Standard hair (L * value 16 ~ 17), which had been damaged by decolorizing human hair with a bleaching agent for 30 minutes, was prepared and stored for 24 hours under constant temperature and humidity conditions (24 ± 2 ° C., 45 ± 5% RH) And the product of the comparative example was applied, and the increase in the intensity in the region of 1430 to 1670 nm in which the hair moisture (-OH group) changed after 24 hours was measured.

division Example 1
(weight%) Example 2
(weight%) Example 3
(weight%) Example 4
(weight%) Example 5
(weight%) Comparative Example
(weight%) Moisture area
(%) 45.3 46.5 49.1 47.7 48.1 7.9

The near-infrareds spectroscopy (NIR) wavelength range varies depending on the adjacent molecular arrangement, rotation, and vibration. Therefore, the moisture content of the hair was evaluated by changing the area before and after the treatment. As the area increased, the moisture content in the hair increased .

The moisture content of the composition for hair treatment, which did not contain the mixed extract, was only 7.9% as compared to that before application. Thus, the results were significantly different from those of Examples 1 to 5, and the superior moisture- .

It will be understood by those skilled in the art that the foregoing description of the present invention is for illustrative purposes only and that those of ordinary skill in the art can readily understand that various changes and modifications may be made without departing from the spirit or essential characteristics of the present invention. will be. It is therefore to be understood that the above-described embodiments are illustrative in all aspects and not restrictive. For example, each component described as a single entity may be distributed and implemented, and components described as being distributed may also be implemented in a combined form.

The scope of the present invention is defined by the appended claims, and all changes or modifications derived from the meaning and scope of the claims and their equivalents should be construed as being included within the scope of the present invention.

Claims

A composition for treating hair comprising an extract of Sasa extract, Rhodiola extract, Rhodiola extract and Burdock root extract as active ingredients.

The method according to claim 1,
2.0 to 5.0 parts by weight of the extract of Soso, 0.5 to 2.0 parts by weight of a zoosporangia extract, 0.5 to 2.0 parts by weight of an extract of yomu, and 0.5 to 2.0 parts by weight of a burdock extract as an active ingredient.

The method according to claim 1,
Wherein the total weight of the Sucrose extract, Rhizopus extract, Rhizome extract and Burdock extract is 50.0 to 95.0 parts by weight based on 100 parts by weight of the composition for hair treatment.

The method of claim 3,
The composition for hair treatment may further comprise at least one selected from the group consisting of an amino acid complex, a hydrolyzed silk, a flavoring agent, a ceramide, an excipient, and purified water, Composition.

The method according to claim 1,
Wherein at least one selected from the group consisting of the extracts of Sasa extract, Rhodiola extract, Rhodiola extract and burdock extract is extracted with an alkaline ionized water.

The composition for hair treatment according to any one of claims 1 to 5, wherein the composition is selected from the group consisting of shampoo, rinse, pomade, paste, cream, treatment, serum, hair lotion or essence.

A step of preparing an extract of Soso, an extract of Rhizobium, an extract of Yumu, and a burdock extract;
Mixing 2.0 to 5.0 parts by weight of the above-prepared sucralose extract, 0.5 to 2.0 parts by weight of a zoosulfur extract, 0.5 to 2.0 parts by weight of a yulmu extract, and 0.5 to 2.0 parts by weight of a burdock extract; And
Mixing said mixed extract with at least one member selected from the group consisting of an amino acid complex, a hydrolyzed silk, a flavoring agent, a ceramide, an excipient, and purified water,
Wherein at least one selected from the group consisting of the above-mentioned Sasa extract, Siberian extract, Yumu extract and burdock extract is extracted with alkaline ionized water.