KR20150052077A - 1-클로로-3,3,3-트리플루오로프로펜의 제조 공정에서 유용한 반응기 및 교반기 - Google Patents
1-클로로-3,3,3-트리플루오로프로펜의 제조 공정에서 유용한 반응기 및 교반기 Download PDFInfo
- Publication number
- KR20150052077A KR20150052077A KR1020157006160A KR20157006160A KR20150052077A KR 20150052077 A KR20150052077 A KR 20150052077A KR 1020157006160 A KR1020157006160 A KR 1020157006160A KR 20157006160 A KR20157006160 A KR 20157006160A KR 20150052077 A KR20150052077 A KR 20150052077A
- Authority
- KR
- South Korea
- Prior art keywords
- reactor
- agitator
- seal
- psig
- stirrer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- LDTMPQQAWUMPKS-OWOJBTEDSA-N (e)-1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)\C=C\Cl LDTMPQQAWUMPKS-OWOJBTEDSA-N 0.000 title claims abstract description 9
- 238000000034 method Methods 0.000 title abstract description 20
- 230000008569 process Effects 0.000 title abstract description 19
- 229910045601 alloy Inorganic materials 0.000 claims abstract description 25
- 239000000956 alloy Substances 0.000 claims abstract description 25
- 238000006243 chemical reaction Methods 0.000 claims abstract description 14
- 238000005260 corrosion Methods 0.000 claims abstract description 14
- VVWFZKBKXPXGBH-UHFFFAOYSA-N 1,1,1,3,3-pentachloropropane Chemical compound ClC(Cl)CC(Cl)(Cl)Cl VVWFZKBKXPXGBH-UHFFFAOYSA-N 0.000 claims abstract description 13
- 230000007797 corrosion Effects 0.000 claims abstract description 13
- 230000004888 barrier function Effects 0.000 claims abstract description 9
- 239000000919 ceramic Substances 0.000 claims abstract description 9
- 239000012530 fluid Substances 0.000 claims abstract description 9
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims abstract description 8
- 239000004810 polytetrafluoroethylene Substances 0.000 claims abstract description 8
- 239000004809 Teflon Substances 0.000 claims abstract description 6
- 229920006362 Teflon® Polymers 0.000 claims abstract description 6
- 229910052751 metal Inorganic materials 0.000 claims abstract description 5
- 239000002184 metal Substances 0.000 claims abstract description 5
- 230000003068 static effect Effects 0.000 claims abstract description 3
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims description 8
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 8
- 238000000576 coating method Methods 0.000 claims description 7
- 229910001026 inconel Inorganic materials 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 229910000990 Ni alloy Inorganic materials 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 5
- 229910000856 hastalloy Inorganic materials 0.000 claims description 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 17
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 16
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 14
- 239000000463 material Substances 0.000 description 9
- PEAPPOBOUGGQHL-UHFFFAOYSA-N 1-chloro-3,3,3-trifluoroprop-1-ene;1,1,1,3,3-pentafluoropropane Chemical compound FC(F)(F)C=CCl.FC(F)CC(F)(F)F PEAPPOBOUGGQHL-UHFFFAOYSA-N 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 7
- 239000003054 catalyst Substances 0.000 description 7
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 7
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 7
- 229910052759 nickel Inorganic materials 0.000 description 6
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 5
- 229910052750 molybdenum Inorganic materials 0.000 description 5
- 239000011733 molybdenum Substances 0.000 description 5
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 4
- 229920006169 Perfluoroelastomer Polymers 0.000 description 4
- 239000006227 byproduct Substances 0.000 description 4
- 230000009977 dual effect Effects 0.000 description 4
- NPURPEXKKDAKIH-UHFFFAOYSA-N iodoimino(oxo)methane Chemical compound IN=C=O NPURPEXKKDAKIH-UHFFFAOYSA-N 0.000 description 4
- 239000007791 liquid phase Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000000376 reactant Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 229910001203 Alloy 20 Inorganic materials 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 3
- 229910052804 chromium Inorganic materials 0.000 description 3
- 239000011651 chromium Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 238000005191 phase separation Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- LDTMPQQAWUMPKS-UHFFFAOYSA-N 1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C=CCl LDTMPQQAWUMPKS-UHFFFAOYSA-N 0.000 description 2
- 229910000599 Cr alloy Inorganic materials 0.000 description 2
- 229910000792 Monel Inorganic materials 0.000 description 2
- 239000000788 chromium alloy Substances 0.000 description 2
- BIJOYKCOMBZXAE-UHFFFAOYSA-N chromium iron nickel Chemical compound [Cr].[Fe].[Ni] BIJOYKCOMBZXAE-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910001293 incoloy Inorganic materials 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- MSSNHSVIGIHOJA-UHFFFAOYSA-N pentafluoropropane Chemical compound FC(F)CC(F)(F)F MSSNHSVIGIHOJA-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 229910000601 superalloy Inorganic materials 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- OQISUJXQFPPARX-UHFFFAOYSA-N 2-chloro-3,3,3-trifluoroprop-1-ene Chemical class FC(F)(F)C(Cl)=C OQISUJXQFPPARX-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 229910000881 Cu alloy Inorganic materials 0.000 description 1
- 229910000640 Fe alloy Inorganic materials 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- ZVQOOHYFBIDMTQ-UHFFFAOYSA-N [methyl(oxido){1-[6-(trifluoromethyl)pyridin-3-yl]ethyl}-lambda(6)-sulfanylidene]cyanamide Chemical compound N#CN=S(C)(=O)C(C)C1=CC=C(C(F)(F)F)N=C1 ZVQOOHYFBIDMTQ-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- OANFWJQPUHQWDL-UHFFFAOYSA-N copper iron manganese nickel Chemical compound [Mn].[Fe].[Ni].[Cu] OANFWJQPUHQWDL-UHFFFAOYSA-N 0.000 description 1
- YOCUPQPZWBBYIX-UHFFFAOYSA-N copper nickel Chemical compound [Ni].[Cu] YOCUPQPZWBBYIX-UHFFFAOYSA-N 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- NHGVZTMBVDFPHJ-UHFFFAOYSA-N formyl fluoride Chemical compound FC=O NHGVZTMBVDFPHJ-UHFFFAOYSA-N 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000005304 joining Methods 0.000 description 1
- 239000011968 lewis acid catalyst Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 239000003380 propellant Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000005482 strain hardening Methods 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
- UONOETXJSWQNOL-UHFFFAOYSA-N tungsten carbide Chemical compound [W+]#[C-] UONOETXJSWQNOL-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/051—Stirrers characterised by their elements, materials or mechanical properties
- B01F27/053—Stirrers characterised by their elements, materials or mechanical properties characterised by their materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/006—Baffles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0073—Sealings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/06—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
- B01J3/08—Application of shock waves for chemical reactions or for modifying the crystal structure of substances
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
- C07C21/185—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine tetrafluorethene
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00004—Scale aspects
- B01J2219/00006—Large-scale industrial plants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00027—Process aspects
- B01J2219/0004—Processes in series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00121—Controlling the temperature by direct heating or cooling
- B01J2219/00123—Controlling the temperature by direct heating or cooling adding a temperature modifying medium to the reactants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00162—Controlling or regulating processes controlling the pressure
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
- B01J2219/0218—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components of ceramic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
- B01J2219/0263—Ceramic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
- B01J2219/0277—Metal based
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Accessories For Mixers (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261697373P | 2012-09-06 | 2012-09-06 | |
| US61/697,373 | 2012-09-06 | ||
| US13/826,023 US9018428B2 (en) | 2012-09-06 | 2013-03-14 | Reactor and agitator useful in a process for making 1-chloro-3,3,3-trifluoropropene |
| US13/826,023 | 2013-03-14 | ||
| PCT/US2013/057186 WO2014039358A1 (en) | 2012-09-06 | 2013-08-29 | Reactor and agitator useful in a process for making 1-chloro-3,3,3-trifluoropropene |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR20150052077A true KR20150052077A (ko) | 2015-05-13 |
Family
ID=50188407
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020157006160A Abandoned KR20150052077A (ko) | 2012-09-06 | 2013-08-29 | 1-클로로-3,3,3-트리플루오로프로펜의 제조 공정에서 유용한 반응기 및 교반기 |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US9018428B2 (enExample) |
| EP (1) | EP2892644A4 (enExample) |
| JP (2) | JP2015534499A (enExample) |
| KR (1) | KR20150052077A (enExample) |
| CN (1) | CN104853839A (enExample) |
| CA (1) | CA2882815A1 (enExample) |
| IN (1) | IN2015DN01846A (enExample) |
| MX (1) | MX349897B (enExample) |
| WO (1) | WO2014039358A1 (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9156752B2 (en) * | 2011-01-04 | 2015-10-13 | Honeywell International Inc. | High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same |
| US9000240B2 (en) | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
| CN104016305B (zh) * | 2014-05-26 | 2016-06-22 | 浙江衢化氟化学有限公司 | 一种从氢氟烃粗品中回收氟化氢的方法 |
| CN106492721B (zh) * | 2016-10-17 | 2018-10-02 | 浙江省海洋水产研究所 | 一种提取贝类毒素搅拌器 |
| FR3066926B1 (fr) * | 2017-06-06 | 2020-05-22 | Arkema France | Procede de modification de la distribution en fluor dans un compose hydrocarbure. |
| FR3066927B1 (fr) * | 2017-06-06 | 2019-06-21 | Arkema France | Procede de modification de la distribution en fluor dans un compose hydrocarbure. |
| WO2019139563A1 (en) * | 2018-01-09 | 2019-07-18 | Honeywell International Inc. | Apparatus and seal system for agitating chemicals within a reactor vessel having a fluoropolymer-coated agitator |
| CN110947350A (zh) * | 2019-12-05 | 2020-04-03 | 清远市鑫辉化工有限公司 | 一种用于制备消光剂的反应釜 |
| CN111229151B (zh) * | 2020-04-08 | 2021-09-10 | 哈尔滨强石新材料技术开发股份有限公司 | 一种聚羧酸盐大体积混凝土高效缓凝减水剂制备系统 |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2608593A (en) * | 1946-08-13 | 1952-08-26 | Robert D Fowler | Fluorination process |
| US2585644A (en) * | 1946-11-25 | 1952-02-12 | Atomic Energy Commission | Process for producing fluorocarbons |
| US3877706A (en) | 1973-10-23 | 1975-04-15 | Philadelphia Gear Corp | Mechanical seal assembly for glass-lined mixer tanks |
| US3999980A (en) * | 1975-05-09 | 1976-12-28 | The United States Of America As Represented By The Secretary Of The Interior | Fluxless recovery of metallic aluminum from wastes |
| US4197531A (en) * | 1978-04-27 | 1980-04-08 | Borg-Warner Corporation | Mechanical seal leakage alarm |
| US4202553A (en) * | 1978-11-03 | 1980-05-13 | Ceramic Coating Company | Seal cartridge for agitator shaft of a chemical reactor |
| JPH05299231A (ja) * | 1992-04-17 | 1993-11-12 | Daikin Ind Ltd | 磁性流体 |
| JPH09273635A (ja) * | 1996-04-05 | 1997-10-21 | Eagle Ind Co Ltd | メカニカルシール |
| WO1997037956A1 (en) * | 1996-04-10 | 1997-10-16 | E.I. Du Pont De Nemours And Company | Process for the manufacture of halogenated propanes containing end-carbon fluorine |
| BE1011765A3 (fr) | 1998-02-26 | 2000-01-11 | Solvay | Procede d'hydrofluoration d'hydrocarbures. |
| JP4403611B2 (ja) * | 1999-08-24 | 2010-01-27 | Ｎｏｋ株式会社 | 軸シール |
| JP2001108113A (ja) * | 1999-10-08 | 2001-04-20 | Nok Corp | 軸シール |
| DE10163171A1 (de) * | 2001-12-21 | 2003-07-03 | Solvay Fluor & Derivate | Neue Verwendung für Legierungen |
| US6844475B1 (en) * | 2003-08-08 | 2005-01-18 | Honeywell International Business Machines | Low temperature production of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) |
| KR101233673B1 (ko) * | 2004-08-26 | 2013-02-15 | 이글 고오교 가부시키가이샤 | 메카니컬 실링장치 |
| US20070118003A1 (en) * | 2005-11-21 | 2007-05-24 | Honeywell International Inc. | Method for preparing 1,1,1,3,3-pentafluoropropane |
| US8168837B2 (en) | 2008-05-15 | 2012-05-01 | Honeywell International Inc. | Process for separating hydrogen fluoride from organic feedstocks |
| EP2349962B1 (en) | 2008-11-19 | 2020-02-26 | Arkema Inc. | Process for the manufacture of hydrochlorofluoroolefins |
| US8263734B2 (en) * | 2009-02-13 | 2012-09-11 | Chevron Phillips Chemical Company Lp | System and method for reducing off-gassing of polyphenylene sulfide |
| KR101684333B1 (ko) * | 2009-03-24 | 2016-12-08 | 알케마 인코포레이티드 | 불화수소로부터 ｒ１２３３의 분리 |
| CN102369375B (zh) * | 2009-10-02 | 2014-11-05 | 伊格尔工业股份有限公司 | 机械密封装置 |
| US8618340B2 (en) | 2009-11-03 | 2013-12-31 | Honeywell International Inc. | Integrated process for fluoro-olefin production |
| JP2011194301A (ja) * | 2010-03-18 | 2011-10-06 | Nichiyo Engineering Kk | 亜臨界水処理装置及び方法 |
| US8704017B2 (en) | 2010-09-03 | 2014-04-22 | Honeywell International Inc. | Continuous low-temperature process to produce trans-1-chloro-3,3,3-trifluoropropene |
| US9000240B2 (en) | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
-
2013
- 2013-03-14 US US13/826,023 patent/US9018428B2/en active Active
- 2013-08-29 EP EP13834867.7A patent/EP2892644A4/en not_active Withdrawn
- 2013-08-29 CA CA2882815A patent/CA2882815A1/en not_active Abandoned
- 2013-08-29 WO PCT/US2013/057186 patent/WO2014039358A1/en not_active Ceased
- 2013-08-29 MX MX2015002868A patent/MX349897B/es active IP Right Grant
- 2013-08-29 CN CN201380046477.7A patent/CN104853839A/zh active Pending
- 2013-08-29 KR KR1020157006160A patent/KR20150052077A/ko not_active Abandoned
- 2013-08-29 JP JP2015531131A patent/JP2015534499A/ja active Pending
-
2015
- 2015-03-05 IN IN1846DEN2015 patent/IN2015DN01846A/en unknown
- 2015-03-26 US US14/669,463 patent/US9993796B2/en active Active
-
2018
- 2018-02-28 JP JP2018034427A patent/JP6549266B2/ja active Active
Also Published As
| Publication number | Publication date |
|---|---|
| WO2014039358A1 (en) | 2014-03-13 |
| MX2015002868A (es) | 2015-07-14 |
| US20150196887A1 (en) | 2015-07-16 |
| JP2018104458A (ja) | 2018-07-05 |
| MX349897B (es) | 2017-08-18 |
| JP2015534499A (ja) | 2015-12-03 |
| US9993796B2 (en) | 2018-06-12 |
| EP2892644A4 (en) | 2016-07-20 |
| CN104853839A (zh) | 2015-08-19 |
| US20140066670A1 (en) | 2014-03-06 |
| CA2882815A1 (en) | 2014-03-13 |
| EP2892644A1 (en) | 2015-07-15 |
| US9018428B2 (en) | 2015-04-28 |
| IN2015DN01846A (enExample) | 2015-05-29 |
| JP6549266B2 (ja) | 2019-07-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR20150052077A (ko) | 1-클로로-3,3,3-트리플루오로프로펜의 제조 공정에서 유용한 반응기 및 교반기 | |
| US7345209B2 (en) | Processes for synthesis of 1,3,3,3-tetrafluoropropene | |
| US20060094911A1 (en) | Noncatalytic manufacture of 1,1,3,3,3-pentafluoropropene from 1,1,1,3,3,3-hexafluoropropane | |
| US5902912A (en) | Process for preparing hydrofluorocarbons | |
| US7700815B2 (en) | Method for producing fluorinated organic compounds | |
| JP5884130B2 (ja) | ２−クロロ−３，３，３−トリフルオロプロペンの液相フッ素化で２−クロロ−１，１，１，２−テトラフルオロプロペンを製造する方法 | |
| HUE034794T2 (en) | Process for the preparation of 2,3,3,3-tetrafluoropropene | |
| KR20020073193A (ko) | 수소함유 플루오르화 탄화수소의 제조방법 | |
| US11629110B2 (en) | Process for manufacture of 2,3-dichloro-1,1,1-trifluoropropane | |
| EP3696156B1 (en) | New process for the manufacture of fluoroaryl compounds and derivatives | |
| CN102282113B (zh) | 制备氟烯烃化合物的方法 | |
| JP7112012B2 (ja) | １，１，２－トリフルオロエタン（ｒ－１４３）及び／又は（ｅ，ｚ）－１，２－ジフルオロエチレン（ｒ－１１３２（ｅ，ｚ））を含む反応ガスの製造方法 | |
| CN111138292B (zh) | 制造1,1,1-三氟-2-氯乙烷和/或三氟乙胺的方法 | |
| CN110536879B (zh) | Hcfc-123和/或hcfc-122的制造方法 | |
| CN111377795B (zh) | 通过直接氟化制备氟苯的工艺 | |
| JP2009530354A (ja) | １，１，１，３，３−ペンタフルオロプロパンの製造方法 | |
| JP2001261593A (ja) | 含水素フッ素化炭化水素の製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0105 | International application |
Patent event date: 20150310 Patent event code: PA01051R01D Comment text: International Patent Application |
|
| PG1501 | Laying open of application | ||
| PA0201 | Request for examination |
Patent event code: PA02012R01D Patent event date: 20180822 Comment text: Request for Examination of Application |
|
| E902 | Notification of reason for refusal | ||
| PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 20191022 Patent event code: PE09021S01D |
|
| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration |
Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 20200623 |
|
| PC1904 | Unpaid initial registration fee |