KR20130114601A - 오불화인 및 불화 수소의 공비성 조성물 - Google Patents
오불화인 및 불화 수소의 공비성 조성물 Download PDFInfo
- Publication number
- KR20130114601A KR20130114601A KR1020127033810A KR20127033810A KR20130114601A KR 20130114601 A KR20130114601 A KR 20130114601A KR 1020127033810 A KR1020127033810 A KR 1020127033810A KR 20127033810 A KR20127033810 A KR 20127033810A KR 20130114601 A KR20130114601 A KR 20130114601A
- Authority
- KR
- South Korea
- Prior art keywords
- azeotropic composition
- composition
- azeotropic
- weight percent
- fluoride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 168
- 238000000034 method Methods 0.000 claims abstract description 19
- 229910013870 LiPF 6 Inorganic materials 0.000 claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 claims abstract description 6
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 73
- 229910000040 hydrogen fluoride Inorganic materials 0.000 claims description 69
- 238000009835 boiling Methods 0.000 claims description 19
- 150000001875 compounds Chemical class 0.000 claims description 15
- 229910052731 fluorine Inorganic materials 0.000 claims description 9
- 239000007795 chemical reaction product Substances 0.000 claims description 8
- 239000011737 fluorine Substances 0.000 claims description 8
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 5
- 229910052698 phosphorus Inorganic materials 0.000 claims description 5
- 239000011574 phosphorus Substances 0.000 claims description 5
- 239000006227 byproduct Substances 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- 238000004821 distillation Methods 0.000 claims description 3
- VVRKSAMWBNJDTH-UHFFFAOYSA-N difluorophosphane Chemical compound FPF VVRKSAMWBNJDTH-UHFFFAOYSA-N 0.000 claims 9
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 1
- 239000007788 liquid Substances 0.000 description 15
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 7
- PQXKHYXIUOZZFA-UHFFFAOYSA-M lithium fluoride Chemical compound [Li+].[F-] PQXKHYXIUOZZFA-UHFFFAOYSA-M 0.000 description 7
- 239000013078 crystal Substances 0.000 description 6
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 5
- 229910001416 lithium ion Inorganic materials 0.000 description 5
- OBCUTHMOOONNBS-UHFFFAOYSA-N phosphorus pentafluoride Chemical group FP(F)(F)(F)F OBCUTHMOOONNBS-UHFFFAOYSA-N 0.000 description 5
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
- -1 lithium hexafluorophosphate Chemical compound 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/10—Halides or oxyhalides of phosphorus
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/36—Azeotropic distillation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/455—Phosphates containing halogen
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/005—Lithium hexafluorophosphate
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Sealing Material Composition (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US36012610P | 2010-06-30 | 2010-06-30 | |
| US61/360,126 | 2010-06-30 | ||
| US13/097,836 US8883707B2 (en) | 2010-06-30 | 2011-04-29 | Azeotrope-like composition of PF5 and HF |
| US13/097,836 | 2011-04-29 | ||
| PCT/US2011/041945 WO2012012107A2 (en) | 2010-06-30 | 2011-06-27 | Azeotrope-like composition of pf5 and hf |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR20130114601A true KR20130114601A (ko) | 2013-10-17 |
Family
ID=45399848
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020127033810A Withdrawn KR20130114601A (ko) | 2010-06-30 | 2011-06-27 | 오불화인 및 불화 수소의 공비성 조성물 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8883707B2 (enExample) |
| EP (1) | EP2595916A4 (enExample) |
| JP (1) | JP2013536144A (enExample) |
| KR (1) | KR20130114601A (enExample) |
| CN (1) | CN102958830A (enExample) |
| WO (1) | WO2012012107A2 (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8815058B2 (en) * | 2010-06-30 | 2014-08-26 | Honeywell International Inc. | Extractive distillation of AsF5 and PF5 using HF |
| US20150093316A1 (en) * | 2013-09-30 | 2015-04-02 | Honeywell International, Inc. | Purification of pf5 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2830105A (en) * | 1955-03-25 | 1958-04-08 | Shell Dev | Extraction of meta dialkylbenzenes with hf-pf5 |
| US3431087A (en) * | 1962-02-23 | 1969-03-04 | Dow Chemical Co | Method for the preparation of high purity nitronium salts |
| US5100639A (en) | 1990-03-02 | 1992-03-31 | E. I. Du Pont De Nemours And Company | Process for purifying hydrogen fluoride |
| FR2768427B1 (fr) | 1997-06-06 | 1999-10-29 | Atochem Elf Sa | Procede de fabrication d'hexafluorophosphate de lithium |
| KR100288825B1 (ko) | 1998-12-31 | 2001-05-02 | 박대치 | 육불화인산리튬의 제조방법 |
| DE10031566A1 (de) | 2000-06-28 | 2002-01-10 | Bayer Ag | Verfahren zur Abtrennung von Arsenverbindungen aus Fluorwasserstoff |
| US6475971B2 (en) | 2001-01-24 | 2002-11-05 | Honeywell International Inc. | Azeotrope-like composition of 1,2-dichloro-3,3,3-trifluoropropene and hydrogen fluoride composition |
| WO2002098529A1 (en) | 2001-06-01 | 2002-12-12 | Honeywell International, Inc. | Azeotrope-like compositions of 1,1,1,3,3-pentafluorobutane and hydrogen fluoride |
| JP2003238161A (ja) | 2002-02-18 | 2003-08-27 | Central Glass Co Ltd | 六フッ化タングステンの精製法 |
| US7141094B2 (en) | 2003-11-05 | 2006-11-28 | Honeywell International Inc. | Azeotrope-like compositions of iodine heptafluoride and hydrogen fluoride |
| US7648682B2 (en) * | 2004-07-08 | 2010-01-19 | Air Products And Chemicals, Inc. | Wick systems for complexed gas technology |
| EP1652814A1 (de) * | 2004-10-27 | 2006-05-03 | Solvay Fluor GmbH | Verfahren zur Gastrennung |
| TW200808656A (en) * | 2006-04-27 | 2008-02-16 | Solvay Fluor Gmbh | Reversible water-free process for the separation of acid-containing gas mixtures |
| JP5254555B2 (ja) * | 2007-02-08 | 2013-08-07 | ステラケミファ株式会社 | 五フッ化リン及び六フッ化リン酸塩の製造方法 |
| CN101353161B (zh) * | 2007-07-27 | 2010-10-06 | 比亚迪股份有限公司 | 制备五氟化磷气体及采用该气体制备六氟磷酸锂的方法 |
| TW200944535A (en) | 2008-03-20 | 2009-11-01 | Sigma Aldrich Co | Purification and preparation of phosphorus-containing compounds |
-
2011
- 2011-04-29 US US13/097,836 patent/US8883707B2/en not_active Expired - Fee Related
- 2011-06-27 JP JP2013518515A patent/JP2013536144A/ja not_active Withdrawn
- 2011-06-27 KR KR1020127033810A patent/KR20130114601A/ko not_active Withdrawn
- 2011-06-27 EP EP11810081.7A patent/EP2595916A4/en not_active Withdrawn
- 2011-06-27 WO PCT/US2011/041945 patent/WO2012012107A2/en not_active Ceased
- 2011-06-27 CN CN2011800323676A patent/CN102958830A/zh active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| CN102958830A (zh) | 2013-03-06 |
| US8883707B2 (en) | 2014-11-11 |
| JP2013536144A (ja) | 2013-09-19 |
| US20120003138A1 (en) | 2012-01-05 |
| EP2595916A2 (en) | 2013-05-29 |
| EP2595916A4 (en) | 2014-05-07 |
| WO2012012107A3 (en) | 2012-04-12 |
| WO2012012107A2 (en) | 2012-01-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0105 | International application |
Patent event date: 20121226 Patent event code: PA01051R01D Comment text: International Patent Application |
|
| PG1501 | Laying open of application | ||
| PC1203 | Withdrawal of no request for examination | ||
| WITN | Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid |