KR20110056156A - A hair restorer comprising extract of rice straw and green perilla pod and method for producing it - Google Patents

A hair restorer comprising extract of rice straw and green perilla pod and method for producing it Download PDF

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Publication number
KR20110056156A
KR20110056156A KR1020090112866A KR20090112866A KR20110056156A KR 20110056156 A KR20110056156 A KR 20110056156A KR 1020090112866 A KR1020090112866 A KR 1020090112866A KR 20090112866 A KR20090112866 A KR 20090112866A KR 20110056156 A KR20110056156 A KR 20110056156A
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KR
South Korea
Prior art keywords
weight
perilla
rice straw
pod
hair
Prior art date
Application number
KR1020090112866A
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Korean (ko)
Inventor
강종규
정성호
Original Assignee
(주)믹스앤매치
강종규
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Application filed by (주)믹스앤매치, 강종규 filed Critical (주)믹스앤매치
Priority to KR1020090112866A priority Critical patent/KR20110056156A/en
Publication of KR20110056156A publication Critical patent/KR20110056156A/en

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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q7/00Preparations for affecting hair growth
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/48Thickener, Thickening system
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52Stabilizers
    • A61K2800/522Antioxidants; Radical scavengers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/596Mixtures of surface active compounds

Abstract

PURPOSE: A method for manufacturing a hair growth agent composition containing extract of rice straw and Preilla frutescens var. japonica pod is provided to ensure health hair growth effect. CONSTITUTION: A method for manufacturing a hair growth agent composition comprises: a step of mixing 90-99 weight% of rice straw and 1-10 weight% of Preilla frutescens var. japonica pod; a step of mixing a mixture of rice straw and Preilla frutescens var. japonica pod and water in the weight ratio of 1:15; a step of boiling for 6-7 hours and cooling; and a step of removing impurities.

Description

A hair restorer comprising extract of rice straw and green perilla pod and Method for producing it}

The present invention relates to a hair restorer composition containing rice straw and perilla pod extract as an active ingredient and a method for preparing the same. More specifically, the present invention relates to a hair restorer composition and a method for preparing the same, which are harmless to the human body and have excellent hair growth promoting effect by using an extract obtained by mixing and drying the rice straw and perilla pods left after harvesting in a solvent mixture.

Normal hair individually has a certain growth cycle of growth, stop, rest, hair loss and regeneration. If this balance is broken, hair loss will proceed. The mechanism of hair loss is not yet known, but in general, excessive sebum production due to abnormal endocrine system such as hormonal imbalance, abnormal circulatory system such as autonomic nervous system, blood circulation disorder, malnutrition of hair root, allergy, bacterial infection and genetic factors, Aging and environmental stress such as mental stress, air pollution, and food are presumed to be the main causes. Recently, a lot of hair loss occurs in young people due to hair beauty such as perm, dyeing, and drying. Hair loss can cause a lot of mental pain for the parties, so it needs to be recognized as a kind of disease.

Therefore, various drug therapies and hair transplantation methods have been developed so far to treat hair loss, but there is no clear method or drug for treating hair loss. Most of the hair regrowths currently being developed and marketed have a temporary or limited hair regrowth effect, and there is a big risk of side effects in long-term use. Therefore, the development of herbal medicines using herbal medicines has been attempted, but most of the obvious effects have not been confirmed. Korean Patent Publication No. 10-1996-0013351 describes a woolen composition containing ginkgo biloba extract and ketoconazole. It describes a hair regrowth promoting agent that uses the formulated liquid, and Patent Publication No. 10-2004-0001683 describes a natural hair regrowth comprising a mixed extract of pine needles, ginkgo leaves, mulberry root, ganoderma lucidum, walnut, jujube, black beans, etc. have. Although a hair regrowth using herbal medicines has been attempted in the past, there has been no attempt to develop rice straw and perilla pod extracts as a hair regrowth.

The inventors of the present invention tried to test the hair growth effect of the extract during the search for recycling methods of rice straw and perilla pods, which are representative farm wastes, and as a result, confirmed that the hair growth promoting effect does not occur to the human body and completed the present invention. Was done.

Disclosure of Invention It is an object of the present invention to find out the hair growth effect of rice straw and perilla pods, which have not been utilized as a conventional medicine, and to provide a hair growth agent containing the same as an active ingredient and having excellent hair growth effect and no side effects, and a method for preparing the same. It is a further object of the present invention to provide said composition and its preparation method formulated in a convenient form.

In order to achieve the above object, the present invention provides a hair restorer composition containing rice straw and perilla pod extract as an active ingredient. Specifically, the rice straw and perilla pod extract is prepared by mixing the rice straw and perilla pod mixture with a solvent to boil and then removing impurities. The solvent may be, but is not limited to, water, ethanol, 1,3-butylene glycol, propylene glycol, isopropanol, and the like. Preferably the rice straw and perilla pods are used to be finely cut to facilitate mixing.

Preferably, the rice straw and perilla pod mixture is mixed at a ratio of 90 to 99% by weight of rice straw and 1 to 10% by weight of perilla pod, and more preferably mixed at a ratio of 95% by weight of straw and 5% by weight of perilla pods. will be. Preferably, but not limited to, the rice straw and perilla pod extract is a mixture of the rice straw and perilla pod mixture in a weight ratio of 1:15 with the solvent.

The composition may be formulated in various forms such as solution, sol, gel, emulsion or ointment. Although not limited thereto, preferably, the composition may be formulated in the form of a shampoo by additionally including an antioxidant, a surfactant, and a thickener in addition to the rice straw and perilla pod extract. In addition, the formulated composition in the form of a shampoo may further contain a flavoring agent. Preferably, the formulated composition in the form of the shampoo is 75.1 ~ 93.4% by weight of the rice straw and perilla pod extract (ratio when the total composition is 100%, the same as below), 0.1 to 0.9% by weight antioxidant, surfactant 5 It is formulated by mixing -20 weight%, 0.5-1 weight% of thickeners, and 1-3 weight% of flavors. There is no restriction on the kind of the antioxidants, surfactants, thickeners and flavoring agents, and in general, any substance used in the preparation of a shampoo can be used in the formulation of the composition according to the present invention. For example, but not limited thereto, the antioxidant is grape fruit Seed Extract (GSE), the surfactant is cococododo (Cocoamidopropyl Betaine) and disodium lauryl sulfosuccinate (Disodium Lauryl Sulfosuccinate ), The thickener may be a polyquater (Polyquaternium), and the flavoring agent may be melon flavor oil.

In another aspect, the present invention provides a method for preparing a hair restorer composition containing rice straw and perilla pods. Specifically, the method, the step of mixing 90 ~ 99% by weight straw and 1 ~ 10% by weight perilla pods; Mixing the rice straw and perilla pod mixture with water at a weight ratio of 1:15; Boiling the mixture for 6 to 7 hours and then cooling the mixture; And removing impurities from the cooled mixture. Preferably, but not limited to, the mixing of the rice straw and perilla pods is composed of 95% by weight of straw and 5% by weight of perilla pods. Preferably, the step of mixing the rice straw and perilla pods is dried by grinding the rice straw and perilla pods and mixed.

In addition, the present invention provides a method for preparing a hair regrowth composition, in which an antioxidant, a surfactant, a thickener, and a flavoring agent are mixed with the mixture from which the impurities are removed to form a shampoo. Although not limited thereto, the formulation step preferably comprises 75.1 to 99.4% by weight of the mixture from which the impurities are removed, 0.1 to 0.9% by weight of antioxidants, 5 to 20% by weight of surfactants, 0.5 to 1% by weight of thickeners, and flavoring agents 1 It is to mix -3 weight%. There is no restriction on the kind of the antioxidants, surfactants, thickeners and flavoring agents, and in general, any substance used in the preparation of a shampoo can be used in the formulation of the composition according to the present invention. For example, the antioxidant is Grape fruit Seed Extract (GSE), the surfactant is Cocoamidopropyl Betaine and disodium lauryl Sulfosuccinate, the thickening agent Polyquaternium, and the flavoring agent may be melon flavor oil.

The hair regrowth composition containing the rice straw and perilla pod extract according to the present invention as an active ingredient shows an effect that healthy hair grows when used continuously for about 3 months on average, and is manufactured from natural products and has no side effects even when used for a long time. Can be used as

Hereinafter, the present invention will be described in more detail with reference to the following examples. These examples are only to illustrate the invention by way of example, it will be apparent to those skilled in the art that the scope of the present invention is not limited by the following examples.

Example  1. Preparation of a hair regrowth composition containing rice straw and perilla pod extract as an active ingredient

(1) Mixed straw and perilla pods

The rice straw was made of rice straw of general rice grown in Seongyeon-myeon, Seosan-si, the central region of Korea, and the perilla pod was used after harvesting the perilla grown in the same area. The rice straw and perilla pods were dried until there was no weight change. First, rice straw is placed on the rice paddy planted after harvesting, dried in nature for about 1 month, and then tied again with a diameter of about 50cm and dried for another 15 days on the paddy pad so that the moisture content is less than 10%. Perilla pods were harvested from the perilla and dried in the natural state so that the moisture content was less than 10%.

Rice straw was used by mixing 50% by weight dried for more than 1 year and 50% dried in the year, the perilla pod used 100% dried in the year. The dried rice straw and perilla pods were cut and mixed to about 50-80 mm with a rice straw cutter and used. Experiments were carried out while changing the mixing ratio during the mixing, in this example, a mixture of 95% by weight of straw and 5% by weight of perilla pods was used. :

(2) Preparation of rice straw and perilla pod extract

The mixture was mixed with water at a weight ratio of 1:15, heated to 100 ° C. for 6 to 7 hours, and then cooled naturally. In addition, by setting the weight ratio of the mixture and water 1: 15 (15 times), 1.5: 15 (10 times), 2: 15 (7.5 times), and the like, the extract was produced and used at 70% of the water weight ratio. However, there was no significant difference in effect.

In order to remove impurities from the cooled extract, the extract was first collected with a water separator, filtered through a cloth, and then cooled in a container to be cooled, followed by cooling, and only the supernatant was collected and filtered by gauze.

(3) formulation

In order to use the composition of the present invention in the form of a shampoo, substances such as surfactants were formulated by mixing in the ratio shown in Table 1.

division Added amount (percentage) Hair regrowth Extract  87-76.5% Surfactants Cocoamidopropyl Betaine 5-10% Disodium laurylsulfosuccinate
(Disodium Lauryl Sulfosuccinate)
5-10%
Thickener Polyquaternium-10 0.5-1% Antioxidant Grapefruit Seed Extract
(Grape Fruiteed Extract.GSE)
0.5%
Flavor Melon extract
(Melon Frognance oil)
2%

It was further prepared with the following composition for other forms of formulation.

Experimental Example 1

87.0 parts of rice straw and perilla pod extract extracted by the above method in the reaction mixture tank 5.0 parts by weight of cocobetaine, 5.0 parts by weight of disodium lauryl sulfosuccinate, 0.5 parts by weight of polyquater, 0.5 parts by weight of grapefruit seed extract, flavoring agent 2.0 parts by weight of the melon extract was mixed and stirred to prepare a hair regrowth in solution.

Experimental Example 2

70.0 parts by weight of straw and perilla pod extracts extracted by the above method in the reaction mixture tank 10.0 parts by weight of cocobetaine, 10.0 parts by weight of disodium lauryl sulfosuccinate, 1.0 parts by weight of polyquater, 0.5 parts by weight of grapefruit seed extract, flavoring agent 2.0 parts by weight of the melon extract was mixed and stirred to prepare a hair regrowth in the form of a solution.

[Experimental Example 3]

10.0 parts by weight of rice straw and perilla pod extract extracted by the above method in the reaction mixture tank 1.0 parts by weight of polyoxyethylene alkali ether sulfate sulfate, 1.0 parts by weight of polyoxyethylene hardened castor oil, 8.0 parts by weight of glycerin, 8.0 parts by weight of vitamin concentrate, licorice extract 3.0 5 parts by weight of purified water, 58.0 parts by weight of purified water, 0.2 parts by weight of menthol, 8.0 parts by weight of ethanol, 2.2 parts by weight of mineral oil, 0.3 parts by weight of perfume, and 0.3 parts by weight of antioxidant were prepared to prepare a hair emulsion in the form of a hair emulsion.

[Experimental Example 4]

10.0 parts by weight of rice straw and perilla pod extract extracted by the above method in the reaction mixture tank 2.0 parts by weight of oxybenzone, 1.0 parts by weight of polyoxyethylene cured castor oil, 6.0 parts by weight of glycerin, 4.0 parts by weight of vitamin concentrate, 4.0 parts by weight of licorice extract, petrolatum A hair restorer in the form of an ointment was prepared by stirring 70.0 parts by weight, 2.2 parts by weight of mineral oil, 0.4 parts by weight of perfume, and 0.4 parts by weight of antioxidant.

Example  2. Efficacy test of hair restorer composition containing rice straw and perilla pod extract as active ingredient

Hair loss composition of the shampoo form prepared in Example 1 to 5 male hair loss patients randomly landed in the country to 1 ~ 2 times a day, hair loss in the hair root portion and the two generators by 5ml once It was tested by trituration. After 1, 2, 3 and 4 months from the start of the test, the hair growth state of the application site was observed (Table 2).

case name age Hair loss period Hair loss site and diameter Application period One Jong Kyu Kang 54 4 years ago Around 5cm of round head hair loss 2009.5.4 ~ 2 Jongcheol Lee 68 15 years ago 5cm hair loss progress in front of tofu 2007.10 ~ 3 Jae Song Choi 53 4 years ago Around 10cm of normal tofu 2009.8.10 ~ 4 Songseok Pavilion 57 17 years ago Hair loss in the tofu normal 2009.8.10 ~ 5 Sangmin Park 44 22 years ago Tofu Front Center 15cm Length 15cm Hair Loss 2009.10.09 ~ * Clinical Trial Information *
1. Kang Jong-gyu (occupation: company management) lived in Dunsan-dong, Seo-gu, Daejeon, 54
2. Lee Jong-cheol (Employment: Labor) 68-year-old living in Yangdae-dong, Seosan-si
3. Choi Jae-Song (Occupation: Company Management) Resides in Wolpyeong-dong, Seo-gu, 53
4. Song Seok-gwan (Job: Unemployed) 57 years old
5. Sangmin Park (occupation: restaurant management) 44 years old resides in Geumsan-eup, Geumsan-gun, Chungnam
 effect case 1 month 2 months 3 months 4 months One Effect sign Downy lot Downy bold Gained much weight 2 No effect Little hair growth Hair growth Hair growth continues and hair growth increases 3 Fluffy hair growth Hair growth increased Hair Regrowth and Growth Many parts cover 4 Hair growth Hair growth Hair Regrowth and Growth Haircut haircut 5 2 From Company
Downy occurrence
Hair growth and thick hair
Growth

As described above, as a result of applying the hair regrowth composition according to the present invention to the depilated tofu was confirmed the effect of hair regrowth. In other words, there are some differences depending on the patient, but when the rice straw and perilla pod extract was shampooed every day, there was a case of hair growth within one month, and when the continuous use for at least three to four months, This increased, the hair was also thickened, hair loss was also reduced, it was confirmed that the same healthy hair growth as normal.

The hair growth mechanism of the rice straw and perilla pod extract of the present invention has not yet been accurately identified, but in consideration of the effects on the skin shown by the extract in other experiments, the blood of the subcutaneous tissue and the hair root is improved and the blood flow is normalized. It is expected to induce normal hair growth by recovering to a healthy scalp state. On the other hand, since the use of the hair regrowth is important, the presence of side effects is a particularly important factor in the commercialization, as a result of the continuous use of the hair regrowth composition of the present invention in a number of application cases, no adverse effects were observed.

Claims (15)

Hair repellent composition containing rice straw and perilla pod extract as an active ingredient. The method of claim 1, wherein the rice straw and perilla pod extract extract is boiled by mixing the rice straw and perilla pod mixture with water to remove the impurities, characterized in that the hair removal composition. According to claim 2, wherein the rice straw and perilla pod mixture is a hair regrowth composition, characterized in that the mixture of rice straw 90 ~ 99% by weight and perilla pod 1 ~ 10% by weight. The hair restorer composition of claim 3, wherein the rice straw and perilla pod mixture is mixed at a ratio of 95% by weight straw and 5% by weight of perilla pods. The hair repellent composition according to any one of claims 2 to 4, wherein the rice straw and perilla pod extract is obtained by mixing the rice straw and perilla pod mixture with water at a weight ratio of 1:15. The hair regrowth composition according to any one of claims 1 to 4, wherein the composition is formulated in a shampoo form, further comprising an antioxidant, a surfactant, and a thickener in addition to the rice straw and perilla pod extract. 7. The hair regrowth composition according to claim 6, wherein the composition further comprises a flavoring agent. The method according to claim 7, wherein the composition of the rice straw and perilla pod extract 75.1 ~ 93.4% by weight (when the total composition is 100%, the same as below), 0.1 to 0.9% by weight antioxidant, 5 to 20 surfactant Hair-repellent composition comprising a weight percent, 0.5-1 weight% thickener, and 1-3 weight% flavoring agent. The method of claim 8, wherein the antioxidant is grapefruit seed extract (Grape fruit Seed Extract (GSE), the surfactant is cococododo (Cocoamidopropyl Betaine) and disodium Lauryl Sulfosuccinate, the increase The agent is a polyquater (Polyquaternium), and the flavourant composition is characterized in that the melon flavor oil. Mixing 90 to 99% by weight of rice straw and 1 to 10% by weight of perilla pods; Mixing the rice straw and perilla pod mixture with water at a weight ratio of 1:15; Boiling the mixture for 6 to 7 hours and then cooling the mixture; And Removing impurities from the cooled mixture. 11. The method according to claim 10, wherein the mixing of the rice straw and perilla pods is characterized in that the mixture of 95% by weight straw and 5% by weight of perilla pods. The method according to claim 10 or 11, wherein the mixing of the rice straw and perilla pods is characterized in that the rice straw and perilla pods are dried and then pulverized and mixed. 11. The method of claim 10, further comprising the step of formulating in the form of a shampoo by mixing an antioxidant, a surfactant, a thickener and a flavoring agent in the mixture from which the impurities are removed. The method according to claim 13, wherein the formulation step comprises 75.1 to 99.4% by weight of the mixture from which the impurities are removed, 0.1 to 0.9% by weight of antioxidants, 5 to 20% by weight of surfactants, 0.5 to 1% by weight of thickeners and 1 to 3 flavoring agents. Manufacturing method characterized by mixing the weight%. 15. The method of claim 14, wherein the antioxidant is grapefruit seed extract (Grape fruit Seed Extract (GSE), the surfactant is cococododo (Cocoamidopropyl Betaine) and disodium Lauryl Sulfosuccinate, the increase The agent is a polyquater (Polyquaternium), and the flavoring agent is a hair repellent composition, characterized in that the melon flavor oil.
KR1020090112866A 2009-11-20 2009-11-20 A hair restorer comprising extract of rice straw and green perilla pod and method for producing it KR20110056156A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101324733B1 (en) * 2013-03-15 2013-11-05 (주)가교테크 Excellent environment and health in baby food substitutes, anthelmintic, detoxification and fermentation effects using rice straw extract liver protection, improve liver disease, anti-cancer, antibacterial, diuretic, milk products, digestive function, and a method of manufacturing the same
DE112016006721T5 (en) 2016-07-05 2018-12-20 Ho Young Yoon A method of making a composition for preventing hair loss and promoting hair growth
KR20230007855A (en) 2021-07-06 2023-01-13 (주)젠셀 Cosmetic composition for promoting hair growth containing natural ingredients and menufacturing method thereof
KR20230162436A (en) 2022-05-20 2023-11-28 윤호영 The natural hair growth composition and its manufacturing method

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101324733B1 (en) * 2013-03-15 2013-11-05 (주)가교테크 Excellent environment and health in baby food substitutes, anthelmintic, detoxification and fermentation effects using rice straw extract liver protection, improve liver disease, anti-cancer, antibacterial, diuretic, milk products, digestive function, and a method of manufacturing the same
DE112016006721T5 (en) 2016-07-05 2018-12-20 Ho Young Yoon A method of making a composition for preventing hair loss and promoting hair growth
KR20230007855A (en) 2021-07-06 2023-01-13 (주)젠셀 Cosmetic composition for promoting hair growth containing natural ingredients and menufacturing method thereof
KR20230162436A (en) 2022-05-20 2023-11-28 윤호영 The natural hair growth composition and its manufacturing method

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