KR20050008235A - Additive for drink containing mugwort essential oil and mugwort prolysis essence - Google Patents
Additive for drink containing mugwort essential oil and mugwort prolysis essence Download PDFInfo
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- KR20050008235A KR20050008235A KR1020030048100A KR20030048100A KR20050008235A KR 20050008235 A KR20050008235 A KR 20050008235A KR 1020030048100 A KR1020030048100 A KR 1020030048100A KR 20030048100 A KR20030048100 A KR 20030048100A KR 20050008235 A KR20050008235 A KR 20050008235A
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- mugwort
- artemisia
- beetle
- essential oil
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- 240000006891 Artemisia vulgaris Species 0.000 title claims abstract description 106
- 235000003261 Artemisia vulgaris Nutrition 0.000 title claims abstract description 106
- 239000000341 volatile oil Substances 0.000 title claims abstract description 20
- 239000000654 additive Substances 0.000 title claims abstract description 18
- 230000000996 additive effect Effects 0.000 title claims abstract description 16
- 239000000284 extract Substances 0.000 claims abstract description 23
- 235000013361 beverage Nutrition 0.000 claims description 23
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- 241000833327 Omonadus floralis Species 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 235000003826 Artemisia Nutrition 0.000 abstract description 2
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- 241001168878 Artemisia rubripes Species 0.000 abstract 1
- 235000003451 Artemisia rubripes Nutrition 0.000 abstract 1
- 241001249148 Artemisia scoparia Species 0.000 abstract 1
- 235000003069 Artemisia scoparia Nutrition 0.000 abstract 1
- 241001168874 Artemisia stolonifera Species 0.000 abstract 1
- 235000003449 Artemisia stolonifera Nutrition 0.000 abstract 1
- 241001168873 Artemisia sylvatica Species 0.000 abstract 1
- 235000003448 Artemisia sylvatica Nutrition 0.000 abstract 1
- 238000000034 method Methods 0.000 description 22
- 239000000779 smoke Substances 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- 238000004821 distillation Methods 0.000 description 9
- 238000001256 steam distillation Methods 0.000 description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 6
- 239000001301 oxygen Substances 0.000 description 6
- 229910052760 oxygen Inorganic materials 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- 239000004480 active ingredient Substances 0.000 description 5
- 239000010659 mugwort oil Substances 0.000 description 5
- CUFNKYGDVFVPHO-UHFFFAOYSA-N azulene Chemical compound C1=CC=CC2=CC=CC2=C1 CUFNKYGDVFVPHO-UHFFFAOYSA-N 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 230000001737 promoting effect Effects 0.000 description 3
- 229930004725 sesquiterpene Natural products 0.000 description 3
- 150000004354 sesquiterpene derivatives Chemical class 0.000 description 3
- 241000894007 species Species 0.000 description 3
- 229930024421 Adenine Natural products 0.000 description 2
- GFFGJBXGBJISGV-UHFFFAOYSA-N Adenine Chemical compound NC1=NC=NC2=C1N=CN2 GFFGJBXGBJISGV-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 206010023126 Jaundice Diseases 0.000 description 2
- 208000004880 Polyuria Diseases 0.000 description 2
- 241001122767 Theaceae Species 0.000 description 2
- 229960000643 adenine Drugs 0.000 description 2
- 230000001093 anti-cancer Effects 0.000 description 2
- 230000017531 blood circulation Effects 0.000 description 2
- OEYIOHPDSNJKLS-UHFFFAOYSA-N choline Chemical compound C[N+](C)(C)CCO OEYIOHPDSNJKLS-UHFFFAOYSA-N 0.000 description 2
- 229960001231 choline Drugs 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 230000029087 digestion Effects 0.000 description 2
- 230000001882 diuretic effect Effects 0.000 description 2
- 230000035622 drinking Effects 0.000 description 2
- 239000003517 fume Substances 0.000 description 2
- 230000023597 hemostasis Effects 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 208000017520 skin disease Diseases 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 230000001256 tonic effect Effects 0.000 description 2
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 1
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 description 1
- PPOCFSJSVCAFQQ-UHFFFAOYSA-N 4,7,7-trimethylbicyclo[2.2.1]heptan-3-one Chemical compound C1CC2(C)C(=O)CC1C2(C)C.C1CC2(C)C(=O)CC1C2(C)C PPOCFSJSVCAFQQ-UHFFFAOYSA-N 0.000 description 1
- 241000226665 Anaphalis Species 0.000 description 1
- 241001148566 Antennaria <beetle> Species 0.000 description 1
- 241000132092 Aster Species 0.000 description 1
- 206010006326 Breath odour Diseases 0.000 description 1
- WEEGYLXZBRQIMU-UHFFFAOYSA-N Eucalyptol Chemical compound C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 description 1
- 208000018522 Gastrointestinal disease Diseases 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- USMNOWBWPHYOEA-UHFFFAOYSA-N alpha-thujone Natural products CC1C(=O)CC2(C(C)C)C1C2 USMNOWBWPHYOEA-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229960000074 biopharmaceutical Drugs 0.000 description 1
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 description 1
- 229940116229 borneol Drugs 0.000 description 1
- 229930007050 cineol Natural products 0.000 description 1
- 229960005233 cineole Drugs 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 235000020510 functional beverage Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- -1 glycerin fatty acid ester Chemical class 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 239000008236 heating water Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 235000021579 juice concentrates Nutrition 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- SIXLXDIJGIWWFU-UHFFFAOYSA-N pyritinol Chemical compound OCC1=C(O)C(C)=NC=C1CSSCC1=CN=C(C)C(O)=C1CO SIXLXDIJGIWWFU-UHFFFAOYSA-N 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/10—Drying, dehydrating
Landscapes
- Non-Alcoholic Beverages (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
Description
본 발명은 쑥정유와 쑥연기진액을 이용한 음료수 첨가제에 관한 것으로서,보다 상세하게는 쑥에서 추출한 쑥정유 또는 쑥연기진액을 단독 또는 2종이상 50% 이하로 함유하고 있는 음료수 첨가제에 관한 것이다.The present invention relates to a beverage additive using mugwort essential oil and mugwort smoke extract, and more particularly, to a beverage additive containing mugwort essential oil or mugwort extract made from mugwort alone or in two or more forms of 50% or less.
쑥에는 사람에 유익한 성분이 다수 포함되어 있어 예로부터 널리 이용되어 왔으며, 쑥에 포함된 유효 성분을 생약학적 방법으로 연구한 결과 쑥에 포함된 다양한 유효성분들이 혈액순환촉진, 이뇨작용, 강장작용, 지혈, 피부질환치료, 건위, 황달 치료, 항암작용 등의 효과를 나타내는 것으로 보고되고 있다.Mugwort contains many beneficial ingredients for humans and has been widely used since ancient times.As a result of researching active ingredients contained in mugwort by biopharmaceutical methods, various active ingredients in mugwort are promoted blood circulation, diuretic effect, tonic action, It has been reported to show the effects of hemostasis, skin disease treatment, health, jaundice treatment, anticancer action.
흔히 쑥이라 불리울수 있는 식물로는 지구 북반구에 200여종이 있고 국내에는 38종이 보고되고 있으나, 흔히 통칭하는 쑥은 종이 명확하지가 않고 쑥속(Artemisia)과 유사종인 떡쑥(Anaphalis, Antennaria)과 쑥부장이(Aster)로 구별할 수 있다. 이들 쑥에 속하는 식물들은 독특한 향기와 맛을 가지고 있어 종래로 부터 식용 또는 약용으로 널리 사용되어 왔다.Plants that can be called wormwood are 200 species in the northern hemisphere and 38 species have been reported in Korea. However, the common name of wormwood is not clear, but the species commonly known as Artemisia are anaphalis (antennaria) and wormwood worms. (Aster) can be distinguished. Plants belonging to these wormwood have a unique aroma and taste has been widely used for food or medicinal in the past.
쑥의 이용법 중에서 음료수로 이용하는 것도 시도되었다. 예를 들어 한국 공개특허 특1998-0000186호, "쑥음료수의 제조방법"은 쑥의 유효성분을 물을 이용하여 추출한 다음 이를 이용하여 음료수의 형태로 가공하는 방법에 관한 것이다. 굳이 인용한 발명의 예가 아니더라도 쑥을 차 형태로 가공하여 우려내서 마시는 방법은 종래에 많이 이용되어온 방법이다.The use of mugwort as a drink was also tried. For example, Korean Laid-Open Patent Publication No. 1998-0000186, "Method of manufacturing mugwort drink water" relates to a method of extracting the active ingredient of mugwort using water and then processing it into the form of a drink using the same. Even if it is not an example of the invention, it is a method that has been widely used in the past by processing the mugwort in the form of tea.
그러나, 쑥을 분말 형태나 원형 그대로 하여 우려내는 방법은 개인이 집에서 음용하기에 큰 불편함이 없으나, 쑥 음료수를 산업적으로 대량생산하여 유통시키는데는 많은 어려움이 따른다. 물론, 티백 형태로 가공하여 유통시킬수는 있으나, 이런 방식의 음용법은 물과 컵이 따로 준비되어야 하므로 자판기나 냉장 음료 형태로판매할수는 없다. 이런 난점을 극복하는 방법은 쑥에서 추출물을 채취하여 이를 음료수 형태로 가공하는 방법이 가장 바람직하다.However, the method of extracting the mugwort as it is in powder form or in the original form does not have a great inconvenience for individuals to drink at home, but there are many difficulties in industrially mass producing and distributing mugwort beverages. Of course, it can be processed and distributed in the form of tea bags, but this method of drinking is not sold in the form of vending machines or refrigerated beverages because water and cups must be prepared separately. The method of overcoming this difficulty is most preferably a method of extracting the extract from the mugwort and processing it into a beverage form.
최근, 쑥의 추출물을 채취하여 다양하게 활용하는 기술들이 보고되어 왔으며, 음료수에 이용하기 적당한 쑥추출물 제조방법으로, 한국특허 특1995-0004327호에 기술된 수증기 증류법을 이용한 쑥속 식물 추출물의 제조 방법이 이미 공지된 바 있다.In recent years, techniques have been reported to take a variety of extracts of the mugwort, a method of producing a mugwort extract suitable for use in beverages, the method of producing a mugwort plant extract using the steam distillation method described in Korea Patent No. 199595-0004327 It is already known.
또 다른 한국특허 특0181751호에는 고농도 에탄올을 이용하여 위장질환 치료제용 쑥추출물이 보고된 바 있다. 이외에도 수증기 증류법으로 쑥의 정유를 채취한 후 이를 이용한 구강위생 증진용 조성물, 즉, 구취 억제제를 보고한 한국 공개특허 특2002-0067332호의 예도 있다.Another Korean Patent No. 0181751 has reported a mugwort extract for treating gastrointestinal diseases using high concentration of ethanol. In addition, there is an example of Korean Patent Laid-Open Publication No. 2002-0067332 which reports a composition for enhancing oral hygiene, that is, a bad breath inhibitor, after collecting essential oil of mugwort by steam distillation.
수증기 증류법에 기초한 쑥 정유 추출법은 물을 가열하여 얻은 수증기를 쑥에 통과시켜 쑥의 정유 성분을 수증기와 함께 증발 시키는 방법으로서, 에탄올 등의 용매를 이용하여 침출하는 방법에 비하여 쑥에 포함되어 있는 유효성분을 분리하는데 있어서 매우 탁월한 방법이다. 즉, 용매를 이용하여 쑥의 유효성분을 추출하면 사용한 용매에 대한 각 성분의 용해도가 다르기 때문에 일부 성분이 미추출된 상태로 남는 것이 일반적이나, 수증기 증류법을 사용하면 이런 점을 극복할수 있기 때문이다.The mugwort essential oil extraction method based on steam distillation is a method of evaporating the essential oil components of mugwort with water vapor by passing steam obtained by heating water through mugwort, which is more effective than the method of leaching with a solvent such as ethanol. It is an excellent way to separate the components. That is, when extracting the active ingredient of mugwort using a solvent, it is common for some components to remain unextracted because the solubility of each component in the solvent used is different, but this can be overcome by using steam distillation. .
이러한 방법으로 얻어진 쑥정유의 주요 성분을 일률적으로 열거하기는 매우 어렵지만, 약전 등의 문헌에 의하면 대체로 시네올 (cineol), 투존 (α- thujon), 세스퀴터핀 (sesquiterpene), 세스퀴터핀 알콜 (sesquiterpene alchol), 아데닌(adenine), 콜린(choline), 아쥴렌(azulene), 보네올(borneol), 캠퍼 (camphor) 등이 공통적으로 포함되어 있다.Although it is very difficult to uniformly list the main components of mugwort oil obtained in this way, the pharmacopeias and the like generally indicate that cineol, α-thujon, sesquiterpene, sesquiterpene alcohol ( sesquiterpene alchol, adenine (adenine), choline (choline), azulene (azulene), bonol (borneol), camphor (camphor) and the like are commonly included.
쑥의 정유는 쑥의 종류에 따라 다르지만 대체로 중량 대비 0.02% 정도 함유되어 있으며, 구성 성분은 최소 100 종 이상의 다양한 생화합물로 이루어져 있고 이들의 함량과 종류는 쑥의 산지, 정유제조의 전처리방법, 증류법 등 다양한 요인에 따라 달라진다.The essential oils of wormwood are different depending on the type of wormwood, but they generally contain about 0.02% by weight, and the constituents consist of at least 100 kinds of various biological compounds. It depends on various factors.
쑥의 추출물을 제조하는 또 다른 방법으로 쑥연기를 이용하는 방법도 가능하다. 즉, 쑥을 공기중에서 연소시키거나, 산소가 제한된 환경에서 건류(pyrolysis)시키면 쑥에 포함되어 있는 성분들이 연기의 형태로 추출되며, 이를 냉각시켜 수집하면 쑥연기진액을 얻을 수 있다.Another way to prepare the extract of mugwort is using a mugwort. In other words, when wormwood is burned in the air or pyrolysis in an oxygen-limited environment, the components contained in the wormwood are extracted in the form of smoke.
물론, 쑥연기를 이용하여 수집한 추출물은 용매 추출물이나 수증기 추출물에서 얻은 정유와는 그 구성성분에서 많은 차이를 보인다. 이는 연소나 열분해 과정에서 새로운 물질들이 생성되기 때문으로, 최근 식용과 농업용으로 널리 이용되는 목초액이 이와 유사한 과정을 거쳐 제조된 제품이라 할 수 있지만, 쑥연기진액을 이용한 음료수의 제조방법은 아직까지 보고되지 않은 상태이다. 다만, 한국특허 10-0345774에 쑥의 훈연을 이용하기 위한 추출장치가 공개되어 있으나, 이는 부황과 뜸의 불편함을 대체할수 있는 수단으로서 발표된 것이다.Of course, the extract collected using wormwood shows a lot of difference in its components from the essential oil obtained from the solvent extract or steam extract. This is because new materials are produced during the combustion or pyrolysis process, and wood vinegar, which is widely used for edible and agricultural products, is a product produced through a similar process. It is not. However, Korean Patent No. 10-0345774 discloses an extracting device for using wormwood smoke, but this is announced as a means to replace the inconvenience of puffiness and moxibustion.
따라서, 상기한 종래 기술들을 살펴보건대 쑥에서 추출한 정유(essential oil)을 이용하여 세제 등의 생활 용품과 위생용품 등을 제조하는 방법은 이미 여러 차례 보고된 바가 있으나, 쑥연기진액을 이용한 음료수의 제조방법에 관한 한 아직까지 그 종례가 없었다.Therefore, the above-described conventional techniques have been reported several times how to prepare household goods such as detergents and sanitary products using essential oils extracted from mugwort, but preparation of beverages using mugwort essence. As far as the method is concerned, there is no such case.
종래의 기술에서 언급한 바와 같이 쑥 분말을 그대로 이용하면 대량생산과 시판에 어울리는 음료수 형태로 제조하기에는 많은 어려움이 있는 것도 사실이다. 이에 본 발명에서는 쑥음료수를 산업화 하는 방안으로서 수증기 증류법으로 추출한 쑥 정유와 건류법으로 추출한 쑥연기진액을 배합한 음료수 첨가제를 제시하고자 한다. 따라서, 본 발명의 목적은 쑥에서 추출한 정유와 연기진액을 배합하여 혈액순환촉진, 이뇨작용, 강장작용, 지혈, 피부질환치료, 건위, 황달 치료, 항암작용 등의 기능을 가지는 기능성 음료수 첨가제를 제공하는데 있다.As mentioned in the prior art, it is also true that using mugwort powder as it is, there are many difficulties in preparing a beverage form suitable for mass production and commercial use. Therefore, the present invention proposes a beverage additive containing mugwort essential oil extracted by steam distillation and mugwort smoke extract extracted by the distillation method as a method of industrializing mugwort beverage. Accordingly, an object of the present invention is to provide a functional beverage additive having the functions of promoting blood circulation, diuretic effect, tonic action, hemostasis, skin disease treatment, health, jaundice treatment, anticancer activity by combining essential oil and smoke smoke extract extracted from mugwort It is.
< 도 1은 본 발명에 따른 수증기 증류장치의 개략도 >1 is a schematic diagram of a steam distillation apparatus according to the present invention.
10 : 수집기 11 : 쑥 12 : 스팀자켓10: Collector 11: Wormwood 12: Steam Jacket
13 : 압력 용기 14 : 증기공급기 15 : 보온파이프13 pressure vessel 14 steam supply 15 heat insulation pipe
16, 17 : 유량조절밸브 18 : 냉각파이프 19 : 응축기16, 17: flow control valve 18: cooling pipe 19: condenser
< 도 2는 본 발명에 따른 쑥연기진액 추출장치 개략도 >2 is a schematic view of the mugwort smoke extract extractor according to the present invention>
21 : 쑥 22 : 건류장치 23 : 냉각기 24 : 냉각수공급장치21: mugwort 22: distillation unit 23: cooler 24: cooling water supply device
25 : 수집기 26 : 전원 27 : 전열선 28 : 산소공급제어장치25 collector 26 power source 27 heating wire 28 oxygen supply control device
상기한 목적을 달성하기 위한 본 발명의 주요 기술적 내용은 수증기 증류법으로 얻은 쑥정유와 건류법으로 얻은 연기진액을 이용하여 음료수 첨가제를 제공하는데 있다.The main technical content of the present invention for achieving the above object is to provide a beverage additive by using the smoke extract obtained by steam distillation method and mugwort oil obtained by steam distillation.
본 발명의 쑥정유는 도 1의 압력 용기의 내부에 충전된 쑥을 105oC, 1 기압의 수증기로 30분 내지 4시간 1차 증류하고, 140oC, 2 기압의 수증기로 30분 내지 4시간 2차 증류하여 얻어진다.The mugwort oil of the present invention is first distilled mugwort filled in the interior of the pressure vessel of Figure 1 with 105 ° C, 1 atm of steam for 30 minutes to 4 hours, and 30 minutes to 4 at 140 ° C, 2 atm of steam It is obtained by time distillation.
도 1은 본 쑥의 정유 성분을 추출하기 위한 수증기 증류 장치의 개략도 이다. 도 1을 참조하면, 쑥(11)은 스팀자켓(12)이 설치된 압력 용기(13)의 내부에 치밀하게 충전된다. 수증기는 증기공급기(14)에서 스팀자켓(12)과 압력용기(13)의 내부로 보온 파이프(15)를 통하여 공급된다. 이때, 공급되는 수증기의 양은 유량조절 밸브(16,17)에 의하여 조절된다.1 is a schematic view of a steam distillation apparatus for extracting essential oil components of the mugwort. Referring to FIG. 1, the mugwort 11 is densely filled in the pressure vessel 13 in which the steam jacket 12 is installed. Water vapor is supplied from the steam supplier 14 to the steam jacket 12 and the pressure vessel 13 through the heat insulating pipe 15. At this time, the amount of water vapor supplied is controlled by the flow control valve (16, 17).
충전된 쑥을 통과하면서 유효성분을 추출한 수증기는 냉각 파이프(18)가 설치된 응축기(19)로 보내지며, 여기에서 수증기와 정유가 응축되어 수집기(10)에 수집된다.Water vapor from which the active ingredient is extracted while passing through the filled mugwort is sent to the condenser 19 in which the cooling pipe 18 is installed, where the water vapor and the essential oil are condensed and collected in the collector 10.
본 발명의 쑥연기진액은 도 2의 건류 장치를 통하여 추출된다. 도 2를 참조하여 쑥연기진액의 제조 방법을 설명하면, 쑥(21)은 건류장치(22)내부에 충전되며, 충전된 쑥은 건류장치의 하층에 설치된 전열선(27)에 의해서 가열된다. 가열시 온도는 쑥의 건조 상태에 따라 조절이 가능한데, 대체로 20일 이상 냉암소에서 잘 건조된 쑥의 경우 200oC 내지 500oC 의 온도 범위에서 건류하면 쑥연기진액을 얻어낼 수 있다.Mugwort smoke extract of the present invention is extracted through the distillation apparatus of FIG. Referring to Figure 2 describes the manufacturing method of mugwort smoke extract, mugwort 21 is filled in the distillation unit 22, the filled mugwort is heated by a heating wire 27 installed in the lower layer of the distillation unit. When heating the temperature can be adjusted according to the dry state of the mugwort, mugwort dried juice in the dark place for more than 20 days in the dry range in the temperature range of 200 o C to 500 o C can obtain a mugwort fume.
이때, 건류장치 내부의 산소 농도는 산소공급제어장치(28)을 통하여 조절 할 수 있다. 산소공급제어장치는 대기중 공기와 압축가스형태의 질소를 이용하여 건류장치 내부의 산소농도를 조절하며, 이러한 방법으로 산소 농도를 조절하는 것은 이 분야에서는 통상적으로 이용되는 기술이므로 자세한 서술을 생략한다.At this time, the oxygen concentration inside the distillation apparatus can be adjusted through the oxygen supply control device 28. Oxygen supply control device adjusts the oxygen concentration inside the distillation unit by using air in the air and nitrogen in the form of compressed gas, and adjusting the oxygen concentration in this way is a commonly used technique in this field, and thus detailed description thereof is omitted. .
가열된 쑥에서 발생한 쑥연기진액은 냉각기(23)에서 응축되어 액상으로 수집된다. 냉각기에 필요한 냉각수는 별도의 냉각수 공급장치(24)를 통하여 공급한다.Mugwort fume generated from the heated mugwort is condensed in the cooler 23 is collected in the liquid phase. Cooling water required for the cooler is supplied through a separate coolant supply device (24).
이하 실시예를 통하여 본 발명의 음료수 첨가제에 관하여 보다 상세히 설명한다.Hereinafter, the beverage additive of the present invention will be described in more detail with reference to the following examples.
실시예 1 : 쑥정유와 쑥연기진액을 함유한 음료수 첨가제의 제조Example 1 Preparation of Drink Additives Containing Mugwort Essential Oil and Mugwort Smoke Extract
냉암소에서 40일간 건조한 인진쑥 200kg을 도1의 증류기 내부에 충전한 다음, 증기공급기에서 105oC, 1기압의 수증기를 압력용기 내부의 쑥 충전층과 스팀 재킷에 동시에 공급하면서 2시간 동안 응축되어 나오는 정유 성분을 수집하였고, 이어 수증기의 온도를 140oC, 2기압으로 하여 나머지 정유성분을 2시간 동안 추출하였다. 쑥연기진액은 상기 인진쑥 200kg을 도 2의 건류장치를 이용하여 400oC로 4시간 동안 건류하여 추출하였다.After filling 200 kg of dried Jinjin mugwort in a dark place for 40 days in the stiller of Fig. 1, the steam supply condensed for 2 hours while simultaneously supplying 105 o C and 1 atm steam to the mugwort packed bed and steam jacket inside the pressure vessel. The essential oil component was collected, and then the remaining essential oil components were extracted for 2 hours at a temperature of 140 ° C. and 2 atm. Mugwort smoke extract was dried by distilling the 200 kg of the Jinjin mugwort with 400 o C for 4 hours using the distillation apparatus of FIG.
상기한 방법으로 추출한 쑥정유 50중량% 와 쑥연기진액 50 중량%를 교반 혼합하여 음료수 첨가제를 제조하였다.Drinking additive was prepared by stirring and mixing 50% by weight of mugwort oil and 50% by weight of mugwort essence extract extracted by the above method.
실시예 2 : 제조한 음료수 첨가제를 이용한 유화수 형태의 쑥음료수 제조Example 2 Preparation of mugwort drink water in the form of emulsified water using the prepared beverage additive
정제수 1L에 상기한 방법으로 제조된 음료수 첨가제 50g을 식품 첨가물로 허용된 글리세린 지방산에스테르 10g을 유화제로서 함께 투입한 다음, 강하게 교반하여 본 발명의 음료수 첨가제가 균일하게 분산된 유화수를 제조하였다. 제조된 유화수에 설탕 50g을 추가로 투입하여 쑥정유와 쑥연기진액이 유화된 형태의 쑥음료수를 제조하였다.50 g of a beverage additive prepared by the above-described method in 1 L of purified water was added together with 10 g of a glycerin fatty acid ester allowed as a food additive as an emulsifier, followed by vigorous stirring to prepare an emulsified water in which the beverage additive of the present invention was uniformly dispersed. 50g of sugar was added to the prepared emulsified water to prepare mugwort beverages in the form of emulsified mugwort oil and mugwort juice concentrate.
실시예 3 : 제조한 음료수의 관능 평가Example 3 sensory evaluation of the prepared beverage
음료수의 맛과 기능에 대한 관능을 각각 10인으로 구성된 3개의 군으로 나누어 평가하였다. 각 군의 평가인에게 제조한 쑥 음료수를 200mL씩 시음케 한 후 그 결과를 수집하였다. 평가 결과는 매우 만족스러울 경우를 5점으로 하였고, 보통을 3점, 불만족스러울 경우를 1점으로 하여 5단계로 표시하였다.The taste and function of beverages were evaluated by dividing them into three groups of 10 people each. After tasting 200 mL of mugwort beverages prepared for each group of evaluators, the results were collected. The evaluation result was 5 points for very satisfactory, and 5 points for 3 points for normal and 1 point for unsatisfactory.
다음의 표1은 그 결과를 나타낸 것이다.Table 1 below shows the results.
본 발명에서 제시한 쑥정유와 쑥연기진액을 이용한 음료수 첨가제를 이용하여 쑥음료수를 제조한 결과, 피로회복 효과와 소화촉진효과는 물론 맛과 향기가 뛰어난 쑥음료수를 제조할 수 있었다.As a result of preparing the mugwort beverage using the beverage additive using the mugwort essential oil and the mugwort smoke extract suggested in the present invention, it was possible to prepare the mugwort beverage having excellent taste and aroma as well as a fatigue recovery effect and a digestion promoting effect.
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| CN103445264A (en) * | 2013-09-18 | 2013-12-18 | 韦以宗 | Capillary artemisia sauce drink |
| KR102325985B1 (en) * | 2021-02-01 | 2021-11-12 | 윤화순 | Moxa cautery concentrate cake and process for preparing the same |
| KR20220141544A (en) * | 2021-04-13 | 2022-10-20 | 윤화순 | Moxa cautery concentrate cake patch and process for preparing the same |
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| KR101381723B1 (en) * | 2012-09-06 | 2014-04-10 | 주식회사 아워홈 | Manufacturing method of liquid flavor with direct thermal-reaction system |
| KR101478215B1 (en) * | 2013-12-20 | 2015-01-02 | 주식회사 아워홈 | Liquid flavor manufacturing device with direct thermal-reaction system |
| KR102348309B1 (en) * | 2021-06-15 | 2022-01-11 | 조경숙 | Eco-friendly all-in-one distillation extractor that produces natural fragrance distilled extract |
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| CN103445264A (en) * | 2013-09-18 | 2013-12-18 | 韦以宗 | Capillary artemisia sauce drink |
| KR102325985B1 (en) * | 2021-02-01 | 2021-11-12 | 윤화순 | Moxa cautery concentrate cake and process for preparing the same |
| KR20220141544A (en) * | 2021-04-13 | 2022-10-20 | 윤화순 | Moxa cautery concentrate cake patch and process for preparing the same |
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