KR20040017981A - Manufacturing method of soap using a persimmon extract - Google Patents

Manufacturing method of soap using a persimmon extract Download PDF

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KR20040017981A
KR20040017981A KR1020020050243A KR20020050243A KR20040017981A KR 20040017981 A KR20040017981 A KR 20040017981A KR 1020020050243 A KR1020020050243 A KR 1020020050243A KR 20020050243 A KR20020050243 A KR 20020050243A KR 20040017981 A KR20040017981 A KR 20040017981A
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soap
persimmon
extract
persimmon extract
weight
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KR1020020050243A
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Korean (ko)
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이의종
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(주)씨앤씨엘티디
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Priority to KR1020020050243A priority Critical patent/KR20040017981A/en
Publication of KR20040017981A publication Critical patent/KR20040017981A/en

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/045Compositions of detergents based essentially on soap containing compounding ingredients other than soaps containing substances which prevent the deterioration of soaps, e.g. light or heat stabilisers or antioxidants
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/44Perfumes; Colouring materials; Brightening agents ; Bleaching agents
    • C11D9/442Perfumes

Abstract

PURPOSE: A method for preparing a soap by using persimmon extract and a soap prepared by the method are provided, to obtain a soap showing a deodorizing effect, an antibacterial effect and a whitening effect without using chemical materials. CONSTITUTION: The method comprises the step of compression-molding the soap composition consisting of 100 parts by weight of a soap base and 0.2-5 parts by weight of persimmon extract. Preferably the persimmon extract is obtained by pulverizing an immature persimmon and juicing the pulverized one. Also the PERMON BM-519 containing the persimmon extract is used as the persimmon extract.

Description

감추출물을 이용한 비누의 제조방법{Manufacturing method of soap using a persimmon extract}Manufacturing method of soap using persimmon extract {Manufacturing method of soap using a persimmon extract}

본 발명은 감추출물을 이용한 비누의 제조방법에 관한 것으로서, 보다 상세하게는 미숙한 감의 감추출물을 이용하여 비누를 제조함으로서 소취효과와 미생물 증식억제 효과뿐만 아니라 뛰어난 미백효과를 얻을 수 있는 감추출물을 이용한 비누의 제조방법에 관한 것이다.The present invention relates to a method for preparing soap using persimmon extract, and more particularly, by preparing soap using immature persimmon extract, a deodorant and microbial proliferation inhibitory effect as well as an excellent whitening effect can be obtained. It relates to a method for producing a soap using.

일반적으로 미용비누는 우지와 야자유 등의 지방산을 60∼70℃로 가열 용해한 후 80∼90℃에서 알칼리염을 첨가하여 비누화 반응을 실시한 다음, 상층부분만을 취하여 그 속에 잔류되어 있는 글리세린과 수산화나트륨 등을 진한 소금물로 제거하고, 이를 진공건조하여 수분함량이 13% 내외인 통상의 비누베이스를 얻고, 상기 비누베이스에 산화방지제, 보색제, 향료 등을 배합한 다음 성형하게 되면 비누가 완성되게 된다.In general, cosmetic soaps are dissolved by heating and dissolving fatty acids such as Uji and palm oil at 60-70 ℃, followed by saponification reaction by adding alkali salts at 80-90 ℃, and then taking only the upper layer and glycerin and sodium hydroxide. This was removed with concentrated brine, and vacuum dried to obtain a normal soap base having a moisture content of about 13%. The soap base is completed by combining an antioxidant, a color supplement, a perfume, and the like with the soap base.

그러나, 상기와 같이 제조된 비누는 지방산과 수산화나트륨의 비누화 반응에 의해 제조됨에 따라 수용액에서 알칼리성을 나타내게 되는데, 이러한 알칼리성 화장비누로 자주 세정을 하게되면 피부의 피지성분이 제거됨에 따라 수분증발이 과도하게 일어나 피부상피세포가 각질화되어 피부가 거칠어지고 건조해지는 단점이 있다.However, the soap prepared as described above shows alkalinity in aqueous solution as it is prepared by saponification reaction of fatty acid and sodium hydroxide. When frequent washing with such alkaline makeup soap removes sebum components of the skin, water evaporation is excessive. The skin epithelial cells are keratinized so that the skin becomes rough and dry.

특히, 각질화로 인해 모공이 막히는 현상이 발생하여 피지가 피부표면으로 배출되지 않고 모공내에 잔류하게 되는데, 이때 혐기성 균(예를 들어 여드름균으로 잘 알려진Propinoibacterium acne) 등이 침투하여 염증을 유발시키고 피부를 붉게 만든다.In particular, keratinization causes pores to become clogged, so that sebum remains in the pores instead of being discharged to the skin surface. At this time, anaerobic bacteria (for example, propinoibacterium acne , also known as acne bacteria) penetrate and cause inflammation and skin. Make red.

또, 피부표면에 피지가 잘 배출된다 하더라도 세정 후 일정 시간이 경과하면 공기중의 미생물이 표피세포 표면에 번식하여 피지를 산패시키므로서 피부로부터 냄새가 나는 것이 보통이었다.Even if sebum is well discharged from the surface of the skin, it is common that a certain time after washing, the microorganisms in the air multiply on the surface of the epidermal cells, causing the sebum to dissipate and smelling from the skin.

그에 따라 피부에서 발명하는 냄새를 억제하기 위하여 다양한 기술이 개시된바 있으며, 미국특허 제4,322,308호에서는 2,4',4-트리클로로-2-하이드록시디페닐 에테르 및 3,4',4'-트리클로로 카바닐라이트와 3-트리플루오로메틸-4, 4'-디클로로카아바닐라이드를 혼합사용하여 소취효과를 증대시키는 기술을 개시하고 있다.Accordingly, various techniques have been disclosed to suppress odors invented in the skin, and US Pat. No. 4,322,308 discloses 2,4 ', 4-trichloro-2-hydroxydiphenyl ether and 3,4', 4'- A technique of increasing the deodorizing effect by using a mixture of trichloro carbanite and 3-trifluoromethyl-4, 4'-dichlorocarbanilide is disclosed.

그러나 상기 미국특허 제4,322,308호의 기술에서 사용된 원료들은 모두 화학물질을 사용함에 따라 소취효과는 우수하나 피부에 자극을 줄 수 있는 단점을 가지고 있다.However, all of the raw materials used in the technique of US Patent No. 4,322,308 are excellent in deodorizing effect by using chemicals but have the disadvantage of irritating the skin.

이에 본 발명은 화학물질을 사용하지 않고 미숙한 감의 감추출물을 이용하여 비누를 제조함으로서 소취효과와 미생물 증식억제 효과뿐만 아니라 뛰어난 미백효과를 얻을 수 있는 감추출물을 이용한 비누의 제조방법을 제공하는데 그 목적이 있다.Accordingly, the present invention provides a method for preparing a soap using a sensitizer extract which can obtain excellent whitening effect as well as a deodorizing effect and microbial growth inhibitory effect by preparing a soap using a persimmon extract of immature persimmon without using chemicals. The purpose is.

상기한 목적을 달성하기 위하여 본 발명은The present invention to achieve the above object

수분함량이 12∼15%인 비누베이스 주성분과, 향료, 색소, 살균제, 소염제, 산화방지제, 방부제에서 선택되는 적어도 1종 이상의 첨가물을 포함하는 비누 조성물을 압착 성형하여 비누를 제조하는 방법에 있어서,In the method for producing soap by compression molding a soap composition comprising a main ingredient of soap base having a moisture content of 12 to 15% and at least one additive selected from fragrances, colorants, fungicides, anti-inflammatory agents, antioxidants and preservatives,

상기 비누 조성물이 비누베이스 100중량부에 대하여 감에서 얻어진 감추출물 0.2 내지 5중량부 포함함을 특징으로 하는 감추출물을 이용한 비누의 제조방법을 제공한다.The soap composition provides 0.2 to 5 parts by weight of the persimmon extract obtained from persimmon per 100 parts by weight of the soap base.

또한 본 발명은 상기 제조방법에 의해 제조됨을 특징으로 하는 소취기능을 갖는 비누를 제공한다.In another aspect, the present invention provides a soap having a deodorizing function characterized in that it is produced by the above production method.

이하 본 발명을 보다 상세하게 설명하면 다음과 같다.Hereinafter, the present invention will be described in more detail.

본 발명에서는 비누베이스를 주성분으로 하는 통상의 비누조성물을 이용하여 비누를 제조하는 과정에서 상기 비누조성물에 감에서 얻어지는 감추출물이 더 포함되도록 한 다음 이를 이용하여 통상의 방법으로 비누를 제조한 것에 그 특징이 있다.In the present invention, in the process of producing a soap using a conventional soap composition containing a soap base as a main component to further include a persimmon extract obtained from persimmon in the soap composition and then to prepare a soap by the conventional method There is a characteristic.

일반적으로 미숙한(덜 익은) 감에서 얻어진 감추출물은 냄새를 흡수하여 분해하는 우수한 소취기능을 가지고 있을 뿐만 아니라 산소공급을 차단하여 호기성 세균의 육성증식을 저해하는 항균기능을 가지고 있다는 것이 알려져 있다.In general, it is known that persimmon extracts obtained from immature (unripe) persimmons not only have an excellent deodorizing function of absorbing and decomposing odors, but also have an antibacterial function of inhibiting the growth of aerobic bacteria by blocking oxygen supply.

따라서, 본 발명에서 감의 감추출물의 이러한 작용을 감안하여 비누 제조과정에서 감추출물을 첨가함으로서 항균 및 소취효과가 뛰어난 비누를 제조할 수 있었다.Therefore, in view of the action of the persimmon extract of persimmon in the present invention by adding the persimmon extract in the soap manufacturing process it was possible to produce a soap with excellent antibacterial and deodorant effect.

상기 감추출물로는 미숙한 감을 분쇄한 후 착즙하여 얻어진 액상의 감추출물을 사용하거나, 상기 액상의 감추출물을 동결건조하여 얻어진 분말상의 감추출물을 사용할 수도 있다.As the persimmon extract, a liquid persimmon extract obtained by pulverizing immature persimmon and then juiced may be used, or a powdery persimmon extract obtained by freeze-drying the liquid persimmon extract may be used.

또한, 상기 미숙한 감에서 얻어진 액상 또는 분말상의 감추출물을 비누를 제조하는 과정에서 직접 투입할 수 있으나, 통상의 방법으로 제조된 감추출물을 포함하는 원료를 비누의 제조과정에서 투입하여 비누를 제조할 수도 있다. 상기 감추출물을 포함하는 원료로는 일본국특허공보 평3-61457호에서 제시하는 감의 추출액을 유효성분으로 하는 소취제를 사용하거나, 미국특허 제6,139,842호에서 제시하는 감추출액을 포함하는 소취조성물을 사용할 수 있다. 또한, 감추출물을 포함하는 원료로 페르몬 비엠-519(PERMON BM-519; 일본 SMC 사 제품명)을 사용할 수도 있다.In addition, the liquid or powdery persimmon extract obtained from the immature persimmon can be added directly in the process of manufacturing soap, but the raw material containing the persimmon extract prepared by a conventional method in the manufacturing process of the soap to prepare a soap You may. As a raw material containing the persimmon extract, a deodorant composition using a deodorant as an active ingredient of the persimmon extract disclosed in Japanese Patent Publication No. Hei 3-61457 or a persimmon extract disclosed in US Pat. No. 6,139,842 is used. Can be used. In addition, FERMON BM-519 (manufactured by Japan SMC) may be used as a raw material containing persimmon extract.

상기와 같이 감추출물을 포함하는 원료를 투입하는 경우에는 액상 또는 분말상의 감추출물을 직접 비누제조공정에서 투입하는 경우와 마찬가지로 감추출물만의 첨가량이 비누베이스 100중량부에 대하여 0.2 내지 5중량부가 되도록 첨가하면 충분한 항균소취 효과를 얻을 수 있다.When the raw material containing the persimmon extract is added as described above, the amount of only the persimmon extract is added to 0.2 to 5 parts by weight based on 100 parts by weight of the soap base, as in the case where the liquid or powdery persimmon extract is directly added in the soap manufacturing process. When added, sufficient antibacterial deodorizing effect can be obtained.

이때 감추출물의 첨가량이 비누베이스 100중량부에 대하여 0.2중량부 미만일 경우 충분한 소취 및 항균 기능을 얻을 수 없으며, 그 첨가량이 비누베이스 100중량부에 대하여 5중량부를 초과할 경우 감성분이 과량함 유되어 피부를 변색시켜 미백효과를 저해할 수 있다는 문제점이 있으므로 감추출물은 비누베이스 100중량부에대하여 0.2 내지 5중량부 첨가하는 것이 바람직하다.At this time, when the amount of the persimmon extract is less than 0.2 part by weight based on 100 parts by weight of the soap base, sufficient deodorization and antimicrobial functions cannot be obtained. Since there is a problem in that discoloration of the skin may inhibit the whitening effect, it is preferable to add 0.2 to 5 parts by weight with respect to 100 parts by weight of the soap base.

본 발명에서는 유효성분인 감추출물과 함께 주성분으로서 통상의 비누베이스를 사용하는데, 상기 비누베이스는 지방산을 60∼70℃로 가열 용해한 후 80∼90℃에서 알칼리염을 첨가하여 비누화 반응을 실시하고, 상층부분만을 취하여 진한 소금물로 수회 세척한 후 이를 진공 건조하여 수분함량이 13%정도가 되도록 하면 용이하게 얻을 수 있다.In the present invention, a normal soap base is used as a main component together with the extract as an active ingredient. The soap base is dissolved by heating the fatty acid at 60 to 70 ℃, and then subjected to a saponification reaction by adding an alkali salt at 80 to 90 ℃, Take only the upper part and wash it with concentrated brine several times, and then vacuum-dry it to easily obtain the moisture content of about 13%.

이때, 상기 비누베이스로는 지방산계 비누베이스, 합성 계면활성제 비누베이스 또는 상기 지방산계 비누베이스와 합성계면활성제 비누베이스가 혼합된 것을 사용할 수 있다.In this case, the soap base may be a fatty acid soap base, a synthetic surfactant soap base or a mixture of the fatty acid soap base and the synthetic surfactant soap base.

지방산계 비누베이스는 야자유, 팜유, 대두유, 피마자유, 올리브유, 팜핵유 등에서 선택되는 식물유와 우지, 돈지, 어유 등에서 선택되는 동물 유지를 단독 또는 혼합하여 이를 알칼리염과 비누화반응을 통해 용이하게 얻을 수 있다. 합성 계면활성제 비누베이스로는 소듐라우릴설포네이트, 알킬벤제설포네이트의 소듐염, 소듐코코일이세티오네이트, 아실글루타메이트의 알칼리금속염 등에서 선택되는 통상의 것을 사용할 수 있다. 또한 상기 지방산계 비누베이스와 합성계면활성제 비누베이스를 각각 혼합하여 사용할 수도 있다.Fatty acid soap base can be easily obtained through alkali salts and saponification reactions by mixing or mixing animal oils selected from palm oil, palm oil, soybean oil, castor oil, olive oil, palm kernel oil and animal fats selected from tallow, pork and fish oil. have. As the synthetic surfactant soap base, a conventional one selected from sodium lauryl sulfonate, sodium salt of alkylbenzesulfonate, sodium cocoyl isethionate, and alkali metal salt of acyl glutamate can be used. In addition, the fatty acid soap base and the synthetic surfactant soap base may be used in combination.

본 발명에 따른 비누 조성물은 비누베이스와 감 추출물이외에도 향료, 색소, 살균제, 소염제, 산화방지제, 방부제에서 선택된 것을 적어도 1종 이상 첨가할 수 있다.In addition to the soap base and persimmon extract, the soap composition according to the present invention may be added at least one selected from fragrances, pigments, fungicides, anti-inflammatory agents, antioxidants, preservatives.

또한 미백효과를 극대화하기 위하여 녹두, 감초, 천궁, 죽염, 박하, 유근피,만년청, 은행, 고삼, 애엽, 행인 등에서 선택되는 한방성분을 첨가하여 비누를 제조할 수도 있다.In addition, in order to maximize the whitening effect, soap may be prepared by adding herbal ingredients selected from mung bean, licorice, cheonggung, bamboo salt, peppermint, yugeunpi, mancheongcheong, ginkgo, ginseng, leaf, almond.

이와 같은 조성을 갖는 비누 조성물을 이용하여 통상의 방법으로 압축성형하게 되면 용이하게 비누를 제조할 수 있으며, 특히 본 발명에 따라 제조된 비누의 경우 소취 및 항균효과를 가질 뿐만 아니라 미백효과를 겸하여 얻을 수 있다.The soap composition having such a composition can be easily prepared by compression molding in a conventional manner, and in particular, the soap prepared according to the present invention can have a deodorizing and antibacterial effect as well as a whitening effect. have.

이하 본 발명을 하기한 실시예를 통하여 보다 상세하게 설명하기로 하나, 이는 본 발명의 이해를 돕기 위하여 제시된 것일 뿐, 본 발명이 이에 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail with reference to the following examples, which are only presented to aid the understanding of the present invention, but the present invention is not limited thereto.

<실시예 1><Example 1>

비누베이스100중량부에 감추출물 0.5중량부 향료 0.5중량부 첨가하여 혼합기에서 충분히 교반한 다음, 통상의 비누 제조기계에서 압출 성형하여 비누를 제조하였다. 이때, 상기 비누베이스는 우지와 야자유에 가성소다를 첨가하여 얻어지는 것으로 수분함량이 14%가 되도록 조절한 것을 사용하였으며, 감추출물은 미숙한 감을 분쇄한 후 착즙하여 얻은 즙을 사용하였다.To 100 parts by weight of soap base 0.5 parts by weight of the extract extract 0.5 parts by weight of fragrance was sufficiently stirred in a mixer, followed by extrusion molding in a conventional soap manufacturing machine to prepare a soap. At this time, the soap base was obtained by adding caustic soda to Uji and palm oil, and used to adjust the moisture content to 14%, and the extract was used to extract juice after crushing immature persimmon.

상기 제조된 비누의 소취성과 항균성 및 미백효과를 다음과 같이 측정하고 그 결과를 하기 표 1에 나타내었다.Deodorant and antimicrobial and whitening effects of the prepared soap were measured as follows and the results are shown in Table 1 below.

- 소취성 --Deodorant-

20 내지 50대 성인남녀 각각 20명을 냄새를 판단하는 판정자로 선정하였고, 이와는 별도로 20 내지 50대 성인남녀 각각 50명을 소취효과에 대한 시험대상자로 선정하였다. 이들 시험대상자의 겨드랑이에 몸냄새 유발물질인이소바레익산(losvaleic acid)를 직경 4㎝크기의 원형태로 도포한 후 제조된 비누를 사용하여 세정하도록 하였다. 세정 직후, 판정자들로 하여금 시험대상자의 겨드랑이의 냄새를 맡게한 후 냄새 강도에 따라 0점(냄새가 전혀 나지 않음)에서 4점(냄새가 매우 심하게 남)을 주도록 하였으며, 그 평균값을 소취효과로 나타내었다. 점수가 작을수록 소취효과가 우수한 것으로 판정하였다.20 adult men and women in their 20s and 50s were selected as judges to judge odors, and 50 adult men and women in their 20s and 50s were selected as test subjects for the deodorizing effect. Body odor causing substance isovareic acid (losvaleic acid) was applied to the subject's armpits in a circular shape having a diameter of 4 cm, and then washed using the prepared soap. Immediately after cleaning, the judges were allowed to smell the subject's armpits, and then, depending on the odor intensity, the judges gave a score of 0 (no smell at all) to 4 points (smelling very badly), and the average value was deodorized. Indicated. The smaller the score, the better the deodorant effect was.

- 항균성 -Antibacterial

상기 제조된 비누에 대한 항균성은 널리 공지된 Calfskin Test방법에 따라 실시하였으며, 다음 균주에 대하여 배양되는 정도를 0점(성장억제력이 없음)에서 4점(완전히 성장을 억제함)까지 5단계로 등급을 표시하여 시험하였다. 이때, 점수가 높을수록 항균성이 우수한 것으로 판정하였다. 배양과정에서 사용된 균주는S. arueusATCC 9144,E. coliATCC 10536,P. vulgarisATCC 6896이다.The antimicrobial activity of the prepared soap was carried out according to the well-known Calfskin Test method, and the degree of incubation for the next strain was graded in five stages from 0 (no growth inhibition) to 4 (completely inhibiting growth). Tested by marking. At this time, it was determined that the higher the score, the better the antimicrobial activity. Strains used in the culture were S. arueus ATCC 9144, E. coli ATCC 10536, and P. vulgaris ATCC 6896.

- 미백효과 --Whitening effect-

20 내지 30세 사이의 여성 50인을 선정하여 제조된 비누를 나누어주고 60일간 사용하도록 한 후 미백효과 여부를 평가하였다(미백효과가 매우 우수하다:5점, 미백효과가 우수하다:3점, 미백효과가 나쁘다:1점, 미백효과가 매우 나쁘다:0점)50 women between 20 and 30 years of age were selected and handed out for 60 days of use, after which the whitening effect was evaluated (whitening effect is very good: 5 points, whitening effect is excellent: 3 points, Whitening effect is bad: 1 point, whitening effect is very bad: 0 points)

<실시예 2><Example 2>

감 추출물을 0.2중량부 첨가한 것을 제외하고는 상기 실시예 1과 동일한 방법으로 실시하여 비누를 제조한 다음 소취성과 항균성 및 미백효과를 측정하여 그 결과를 하기 표 1에 나타내었다.Except for the addition of 0.2 parts by weight of persimmon extract was carried out in the same manner as in Example 1 to prepare a soap and then to measure the deodorant and antimicrobial and whitening effect is shown in Table 1 below.

<실시예 3><Example 3>

감 추출물을 5.0중량부 첨가한 것을 제외하고는 상기 실시예 1과 동일한 방법으로 실시하여 비누를 제조한 다음 소취성과 항균성 및 미백효과를 측정하여 그 결과를 하기 표 1에 나타내었다.Except for the addition of 5.0 parts by weight persimmon extract was carried out in the same manner as in Example 1 to prepare a soap and then to measure the deodorant and antimicrobial and whitening effect is shown in Table 1 below.

<실시예 4><Example 4>

감 추출물 대신 감추출물을 5% 함유하는 페르몬 비엠-519(PERMON BM-519; 일본 SMC 사 제품명) 5중량부(실제 감추출물 첨가량은 0.25중량부임)를 첨가한 것을 제외하고는 상기 실시예 1과 동일한 방법으로 실시하여 비누를 제조한 다음 소취성과 항균성 및 미백효과를 측정하여 그 결과를 하기 표 1에 나타내었다.Example 1 except that 5 parts by weight of FERMON BM-519 (PERMON BM-519; product name of Japanese SMC Co., Ltd.) containing 5% of persimmon extract instead of persimmon extract (actual extract is 0.25 parts by weight) was added. The soap was prepared by the same method and then the deodorizing property and the antibacterial and whitening effect were measured and the results are shown in Table 1 below.

<비교예 1>Comparative Example 1

감 추출물을 0.1중량부 첨가한 것을 제외하고는 상기 실시예 1과 동일한 방법으로 실시하여 비누를 제조한 다음 소취성과 항균성 및 미백효과를 측정하여 그 결과를 하기 표 1에 나타내었다.Except for the addition of 0.1 parts by weight persimmon extract was carried out in the same manner as in Example 1 to prepare a soap and then to measure the deodorant and antimicrobial and whitening effect is shown in Table 1 below.

<비교예 2>Comparative Example 2

감 추출물을 10중량부 첨가한 것을 제외하고는 상기 실시예 1과 동일한 방법으로 실시하여 비누를 제조한 다음 소취성과 항균성 및 미백효과를 측정하여 그 결과를 하기 표 1에 나타내었다.Except for the addition of 10 parts by weight of persimmon extract was carried out in the same manner as in Example 1 to prepare a soap and then to measure the deodorant and antimicrobial and whitening effect is shown in Table 1 below.

구분division 감추출물(중량부)Persimmon extract (part by weight) 소취효과Deodorant effect 항균성Antimicrobial activity 미백효과Whitening effect S.arueusS.arueus E.coliE.coli P.vulgarisP.vulgaris 실시예 1Example 1 0.50.5 3.53.5 44 44 44 4.24.2 실시예 2Example 2 0.20.2 3.13.1 33 33 33 4.64.6 실시예 3Example 3 55 3.83.8 44 44 44 3.83.8 실시예 4Example 4 0.250.25 3.63.6 44 44 44 4.34.3 비교예 1Comparative Example 1 0.10.1 1.71.7 1One 00 00 4.64.6 비교예 2Comparative Example 2 1010 3.83.8 44 44 44 2.42.4

상기 표 1에서 보는 바와 같이 본 발명의 바람직한 범위내에서 감추출물을 첨가하여 비누를 제조한 실시예 1 내지 4의 경우 항균성과 소취효과 및 미백효과가 매우 뛰어남을 확인할 수 있다.As shown in Table 1, it can be seen that the antimicrobial, deodorizing and whitening effects of Examples 1 to 4 were prepared by adding a sensitized extract within the preferred range of the present invention to soap.

상기에서 설명한 바와 같이 본 발명은 화학물질을 사용하지 않고 미숙한 감의 감추출물을 이용하여 비누를 제조함으로서 소취효과와 미생물 증식억제 효과뿐만 아니라 뛰어난 미백효과를 얻을 수 있는 감추출물을 이용한 비누의 제조방법을 제공하는 유용한 발명이다.As described above, in the present invention, soap is prepared by using immature persimmon extract of immature persimmon without using chemicals. It is a useful invention to provide a method.

Claims (4)

수분함량이 12∼15%인 비누베이스 주성분과, 향료, 색소, 살균제, 소염제, 산화방지제, 방부제에서 선택되는 적어도 1종 이상의 첨가물을 포함하는 비누 조성물을 압착 성형하여 비누를 제조하는 방법에 있어서,In the method for producing a soap by compression molding a soap composition comprising a main ingredient of a soap base having a water content of 12 to 15% and at least one additive selected from fragrances, pigments, fungicides, anti-inflammatory agents, antioxidants, preservatives, 상기 비누 조성물이 비누베이스 100중량부에 대하여 감에서 얻어진 감추출물 0.2 내지 5중량부 포함함을 특징으로 하는 감추출물을 이용한 비누의 제조방법.Method for producing a soap using a persimmon extract, characterized in that the soap composition comprises 0.2 to 5 parts by weight persimmon extract obtained from persimmon per 100 parts by weight of the soap base. 청구항 1에 있어서, 상기 감추출물이 미숙한 감을 분쇄한 후 착즙하여 얻어진 것임을 특징으로 하는 감추출물을 이용한 비누의 제조방법.The method of claim 1, wherein the persimmon extract is obtained by pulverizing immature persimmon and then juice. 청구항 1에 있어서, 상기 감추출물로 감추출물을 포함하는 페르몬 비엠-519(PERMON BM-519; 일본 SMC 사 제품명)를 사용함을 특징으로 하는 감추출물을 이용한 비누의 제조방법.The method of claim 1, wherein FERMON BM-519 (PERMON BM-519; product name of Japan SMC Co., Ltd.) containing the extract is used as the sensitizer. 청구항 1 내지 청구항 3중 어느 한 항의 제조방법에 의해 제조됨을 특징으로 하는 소취성을 갖는 비누.Deodorizing soap, characterized in that produced by the method of any one of claims 1 to 3.
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WO2017204409A1 (en) * 2016-05-26 2017-11-30 가톨릭관동대학교산학협력단 Method for preparing scrubbing soap using persimmon peels and scrubbing soap prepared by means of same
WO2017204410A1 (en) * 2016-05-26 2017-11-30 가톨릭관동대학교산학협력단 Method for preparing whitening soap using persimmon stalks and whitening soap prepared by means of same

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JPH03193713A (en) * 1989-12-25 1991-08-23 Maremitsu Izumitani Tannin-containing composition
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JPS6187562A (en) * 1984-10-08 1986-05-02 鳥居 国司 Deodorant preparation containing perssimon extract as effective component
JPH03193713A (en) * 1989-12-25 1991-08-23 Maremitsu Izumitani Tannin-containing composition
JPH0558876A (en) * 1991-08-29 1993-03-09 Masaichi Sakurashita Production of vegetable extract bathing agent
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* Cited by examiner, † Cited by third party
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WO2017204409A1 (en) * 2016-05-26 2017-11-30 가톨릭관동대학교산학협력단 Method for preparing scrubbing soap using persimmon peels and scrubbing soap prepared by means of same
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