KR20040017202A

KR20040017202A - Anti-bacterial soap containing essential oil of pine tree therein and manufacturing method thereof

Info

Publication number: KR20040017202A
Application number: KR1020020050252A
Authority: KR
Inventors: 신충선
Original assignee: 신충선
Priority date: 2002-08-20
Filing date: 2002-08-20
Publication date: 2004-02-26

Abstract

PURPOSE: Provided is an antibacterial soap containing an essential oil extracted from pine needles as a natural antibacterial and anti-insect agent, which removes a broad spectrum of bacteria efficiently and has substantially no toxicity. CONSTITUTION: The antibacterial soap comprises 70-75% of a beef tallow, 24-29% of a coconut oil, 0.5-0.8% of a dye and glycerin and 1.2-1.5% of an essential oil extracted from pine needles. In the soap, the essential oil of pine needles is extracted by mixing pine needles with distilled water, triturating the mixture and then distilling. The antibacterial soap is prepared by extracting fatty acids from a beef tallow, adding a small amount of sodium hydroxide to the fatty acids, heating the mixture, adding sodium chloride, and further adding 1.2-1.5% of an essential oil of pine needles.

Description

Anti-bacterial soap containing essential oil of pine tree therein and manufacturing method

본 발명은 소나무잎 정유가 함유된 항균 비누에 관한 것으로서, 보다 상세하게는 기능성 천연 항균, 항충물질이 함유됨으로서 인체에 유해한 세균을 제거할 수 있는 항균비누에 관한 것이다.The present invention relates to an antibacterial soap containing pine leaf essential oil, and more particularly, to an antibacterial soap that can remove bacteria harmful to the human body by containing a functional natural antibacterial and antiseptic material.

방향성 식물에서 추출된 정유(Essential Oil)는 향료 및 향신료로서 뿐만 아니라 방충제, 방부제, 해충구제 심지어 목욕제의 보조제로 첨가하여 사용되며, 그 정유성분의 구조와 규모가 다양하고 휘발성이 강하며 흡입 및 자극성이 강하여 신체적 정신적 조절기능을 강화하여 피로회복, 진정, 스트레스 해소 등 현대병을 치유할 수 있는 가능성이 있으며, 최근에는 아로마테라피(Aroma Therapy)라는 새로운 치료분야에서 응용되고 있어서 여러 가지 약리 작용을 기대할 수 있다.Essential oils extracted from aromatic plants are used not only as fragrances and spices, but also as additives for insect repellents, preservatives, pest control and even bathing agents.The essential oils vary in structure and scale, are highly volatile, inhalable and irritant. It is strong and has the potential to cure modern illnesses such as fatigue recovery, sedation and stress relief by strengthening physical and mental control functions. Recently, it is applied in a new treatment field called Aroma Therapy, and various pharmacological effects can be expected. have.

종래에 사용되는 미용비누는 유지에 수산화나트륨 용액을 가하여 비누화 한 후 진한 염화나트륨 용액을 가하여 희석하면 비누가 물위로 뜨게 되는데, 이것을 수거하여 여기에 향료와 보습제 등을 소량 배합하여 제조하였기 때문에 항균성 비누로서는 한계가 있었다.Conventional soaps used in the prior art are soaped by adding sodium hydroxide solution to fats and oils, and diluted with concentrated sodium chloride solution, and the soap floats on water.They are collected and mixed with a small amount of fragrances and moisturizers. There was a limit.

또한, 일상 생활 중에 접하게 되는 세균의 종류는 다양하기 때문에 광범위한 스펙트럼을 갖는 항균성 비누의 개발을 위해서는 보다 다양한 항균 물질의 활용이 필요하다.In addition, since the types of bacteria encountered in daily life are various, it is necessary to utilize more various antimicrobial substances in order to develop an antimicrobial soap having a broad spectrum.

본 발명은 상술한 종래 기술의 문제점을 해결하기 위해 안출된 것으로서, 본 발명의 목적은 독성이 거의 없으며 안정성이 큰 방향족 화합물로 구성되는 플라보노이드 성분의 천연 항균, 항충물질을 가지는 소나무잎 정유가 함유됨으로써 보다 광범위한 항균효과를 발휘하는 항균비누를 제공하는 것이다.The present invention has been made to solve the above-mentioned problems of the prior art, the object of the present invention is to contain a pine leaf essential oil having a natural antibacterial, anti-insectant of flavonoid components composed of aromatic compounds with little toxicity and high stability It is to provide an antibacterial soap exhibiting a broader antibacterial effect.

상기와 같은 목적을 달성하기 위하여, 본 발명에 따른 항균비누는 우지 70-75%, 야자유 24-29%, 염료 및 글리세린 0.5-0.8%, 소나무잎 정유 1.2-1.5%를 포함하여 조성된 것을 특징으로 한다. 한편, 상기 소나무잎 정유는 솔잎과 증류수를 2:1의 비율로 혼합하여 분쇄한 다음 증류함으로써 추출된다.In order to achieve the above object, the antibacterial soap according to the present invention is characterized by comprising 70-75% Uji, palm oil 24-29%, dyes and glycerin 0.5-0.8%, pine leaf essential oil 1.2-1.5% It is done. On the other hand, the pine leaf essential oil is extracted by mixing and grinding the pine needles and distilled water in a ratio of 2: 1 and then distilled.

또한, 본 발명에 따른 항균비누의 제조방법은 우지에서 추출된 지방산에, 소량의 수산화나트륨을 배합하여 가열하고, 여기에 염화나트륨을 배합하여 형성되는 종래의 미용비누에 소나무잎 정유 1.2-1.5%를 더 배합하는 것을 특징으로 한다.In addition, the method for producing an antibacterial soap according to the present invention is 1.2-1.5% of pine leaf essential oil in a conventional beauty soap formed by mixing a small amount of sodium hydroxide with a fatty acid extracted from tallow, and adding sodium chloride thereto. It is characterized by further compounding.

구체적으로, 본 발명에 따른 항균비누의 제조방법은, 우지 70-75%에, 야자유를 25-30%의 비율로 혼합하고 수세과정을 거쳐 불순물을 제거하는 단계와, 상기 우지와 야자유 혼합물을 가수분해하여 지방산을 추출하는 단계와, 상기 지방산에 수산화 나트륨을 첨가하여 가열 중화하는 단계와, 상기 지방산과 수산화 나트륨 화합물에 염화나트륨을 첨가하고, 수세한 후 정치시키는 단계와, 염료 및 글리세린 0.5-0.8%과, 소나무잎 정유 1.2-1.5%를 배합하는 단계를 포함하여 이루어진다.Specifically, the method for producing an antibacterial soap according to the present invention comprises the steps of mixing the palm oil at a ratio of 25-30% to 70-75% of tallow, and removing impurities by washing with water, and mixing the tallow and palm oil mixture with water. Decomposing the fatty acid by decomposition, heating and neutralizing by adding sodium hydroxide to the fatty acid, adding sodium chloride to the fatty acid and the sodium hydroxide compound, washing with water and standing still, dyes and glycerin 0.5-0.8% And, pine leaf essential oils containing 1.2-1.5% compounding step.

이하, 본 발명의 바람직한 실시예를 상세하게 설명한다.Hereinafter, preferred embodiments of the present invention will be described in detail.

상기 목적을 달성하기 위한 본 발명에 따른 소나무잎 정유를 함유한 항균 비누는 우지 70-75%, 야자유 24-29%, 염료, 글리세린 0.5-0.8%, 소나무(적송) 잎 정유 1.2-1.5%를 포함하여 형성된다. 상기 소나무잎 정유의 추출은 적송의 솔잎과 증류수를 2:1의 비율로 혼합하여 분쇄한 다음, 슐츠(Schultz) 등의 방법에 따라 개량형 수증기 추출기 (Simultaneous distillation ＆ extraction)(SDE) 장치를 사용하여 2시간 증류하는 방식으로 이루어진다. 추출 용매로는 에틸 에테르(ethyl ether)와 엔 펜탄(n-pentane)을 대략 1:1로 혼합한 혼합액을 증류하여 사용한다. 또한, 이와 같이 증류된 추출 용매를 무수 황산 나트륨으로 탈수한 다음 감압 농축하였다.Antibacterial soap containing pine leaf essential oil according to the present invention for achieving the above object is Uji 70-75%, palm oil 24-29%, dye, glycerin 0.5-0.8%, pine (red pine) leaf essential oil 1.2-1.5% It is formed to include. Extracting the essential oil of pine needles is pulverized by mixing the pine needles and distilled water of the red pine in a ratio of 2: 1, and then using a modified steam extractor (SDE) apparatus according to Schultz et al. It is made by distillation for 2 hours. As an extraction solvent, a mixed solution of ethyl ether and n-pentane mixed approximately 1: 1 is used by distillation. In addition, the extraction solvent thus distilled was dehydrated with anhydrous sodium sulfate and then concentrated under reduced pressure.

한편, 본 발명에 따른 항균비누의 제조방법을 공정순서에 따라 설명하면 다음과 같다.On the other hand, the method for producing an antibacterial soap according to the present invention will be described according to the procedure.

1) 먼저, 비누의 기본 원료가 되는 우지 70-75%에, 비누의 기포력을 증진시키고 윤기를 더 해주며 조밀한 조직을 만들기 위하여 야자유를 25-30%의 비율로 혼합하여 수세과정을 거쳐 불순물을 제거해 낸다.1) First, wash water by mixing palm oil at a ratio of 25-30% to Uji 70-75%, which is the basic raw material of soap, to enhance the bubble power, add luster, and make dense tissue. Eliminate impurities.

2) 다음으로, 우지와 야자유 혼합유에 가수분해하여 지방산과 글리세린으로 분리한 후 글리세린을 추출해 낸다.2) Next, hydrolyze in mixed oil of Uji and palm oil, separate it into fatty acid and glycerin, and extract glycerin.

3) 색상개선과 순수한 지방산을 얻기 위하여, 위에서와 같이 분리된 지방산을 진공상태에서 기화과정을 거쳐 증류시킨다.3) In order to improve color and obtain pure fatty acids, the separated fatty acids are distilled through evaporation under vacuum.

4) 증류결과 얻어진 순수한 지방산에 수산화 나트륨을 가하여 가열 중화시킨다.4) Add sodium hydroxide to the pure fatty acid obtained by distillation and neutralize it by heating.

5) 중화된 지방산과 수산화 나트륨 화합물 용액에 염화나트륨을 가하면 비누가 콜로이드 용액 위에 뜨게 되는데 불순물 제거를 위하여 2-3회 수세하여 48시간 정치시킨다.5) When sodium chloride is added to the neutralized fatty acid and sodium hydroxide compound solution, the soap floats on the colloidal solution. It is washed 2-3 times and removed for 48 hours to remove impurities.

6) 이를 진공 건조로에서 건조하여 수분함량이 14% 이내로 되도록 조절한다.6) This is dried in a vacuum drying furnace to adjust the moisture content to within 14%.

7) 상기 6단계에서 얻어진 결과물에 공지의 비누 첨가물인 염료 및 글리세린 0.5-0.8%과, 본 발명의 목적을 얻기 위하여 소나무잎 정유 1.2-1.5%를 배합한다.7) 0.5-0.8% of the known soap additive, dye and glycerin, and 1.2-1.5% of pine leaf essential oil are blended with the resultant obtained in the sixth step.

8) 마지막으로, 상기 7단계에서 얻어진 결과물을 압출하여 절단한 후 성형하여 마무리 작업하면 항균비누의 제조가 완료된다.8) Finally, the resultant obtained in step 7 is extruded, cut, molded and finished to complete the production of antibacterial soap.

이와 같은 방법으로 제조된 항균 비누는 항균 효과가 뛰어난 베타마이신(β-myrcene), 리모넨(1-limonene), 베타펠란드렌(β-phellandrene)와 같은 생리활성물질로 인하여 항균작용 발현의 요소가 될 수 있어 스타피로코커스 아우로스(Staphylococcus aureus), 슈도모나스 아루기누사(Pseudomonas aeruginosa)에 대하여 항균 억제효과를 기대할 수 있다.Antimicrobial soaps prepared in this way have a high antimicrobial effect, and the elements of the antimicrobial activity are expressed by bioactive substances such as betamycin (β-myrcene), limonene (1-limonene) and beta-phellandrene. Antibacterial inhibitory effect can be expected for Staphylococcus aureus and Pseudomonas aeruginosa.

본 발명에 따른 소나무잎 정유를 함유한 항균비누는 일상 생활 중 접하게 되는 세균을 보다 적극적으로 제거할 수 있는 효과가 있다. 따라서, 본 발명에 따른향균비누를 사용함으로써 수준 높은 위생을 필요로 하는 작업장 등에서 보다 수준높은 청결을 유지할 수 있다. 이상에서 본 발명은 기재된 구체예에 대해서만 상세히 기술되었지만, 본 발명의 기술사상 범위 내에서 다양한 변형 및 수정이 가능함은 당업자에게 있어서 명백한 것이다.Antibacterial soap containing the essential oil of pine leaf according to the present invention has an effect that can more actively remove the bacteria encountered in everyday life. Therefore, by using the antibacterial soap according to the present invention it is possible to maintain a higher level of cleanliness in the workplace and the like requiring a high level of hygiene. While the invention has been described in detail only with respect to the described embodiments, it will be apparent to those skilled in the art that various modifications and variations are possible within the spirit of the invention.

Claims

Antibacterial soap, characterized in that it comprises 70-75% Uji, palm oil 24-29%, dyes and glycerin 0.5-0.8%, pine leaf essential oil 1.2-1.5%.

The method of claim 1,

The pine leaf essential oil is an antibacterial soap, characterized in that the extract by pulverizing and then pulverized by mixing the ratio of pine needles and distilled water 2: 1.

In a method of producing a soap by blending a small amount of sodium hydroxide with a fatty acid extracted from the tallow and heating, and adding sodium chloride to it,

Antibacterial soap manufacturing method characterized in that further formulated with pine leaf essential oil 1.2-1.5%.

The method of claim 3, wherein

Mixing 70-75% of tallow, palm oil at a ratio of 25-30% and washing with water to remove impurities;

Hydrolyzing the tallow and palm oil mixture to extract fatty acids;

Heat neutralizing by adding sodium hydroxide to the fatty acid;

Adding sodium chloride to the fatty acid and sodium hydroxide compound and washing with water after washing; And

Dye and glycerin 0.5-0.8%, pine leaf essential oil manufacturing method comprising the step of blending 1.2-1.5% essential oil.