KR20020089607A - Method for manufacturing the detergent like soap using rice straw - Google Patents

Method for manufacturing the detergent like soap using rice straw Download PDF

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Publication number
KR20020089607A
KR20020089607A KR1020010028371A KR20010028371A KR20020089607A KR 20020089607 A KR20020089607 A KR 20020089607A KR 1020010028371 A KR1020010028371 A KR 1020010028371A KR 20010028371 A KR20010028371 A KR 20010028371A KR 20020089607 A KR20020089607 A KR 20020089607A
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rice straw
soap
straw
rice
detergent
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KR1020010028371A
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Korean (ko)
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최영미
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최영미
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Publication of KR20020089607A publication Critical patent/KR20020089607A/en

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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/10—Mixing; Kneading
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/02—Preparations for cleaning the hair
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/046—Salts
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2065—Polyhydric alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/06—Inorganic compounds
    • C11D9/08—Water-soluble compounds
    • C11D9/10—Salts
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/06—Inorganic compounds
    • C11D9/18—Water-insoluble compounds

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)
  • Cosmetics (AREA)

Abstract

PURPOSE: Provided is a process for producing a cleanser like soap useful for whitening effect and skin regeneration by using rice-straw, the ashes of the rice-straw remaining after burning can be used as a compost of the crops. CONSTITUTION: The process comprises the steps of: washing and drying the rice-straw; burning the rice-straw; refining the ashes of the rice-straw and extracting alkali salts and discharging and storing the left ashes to use as the compost; producing the cleanser containing soap and shampoo by mixing 5-15wt.% of the extracted alkali salts, 2-5wt.% of water, 20-40wt.% of a high aliphatic acid forming synthetic ester, and 50-70wt.% of glycerol and then heating the mixture at 100-200deg.C and solidifying.

Description

볏짚을 이용하여 비누와 같은 세제를 제조하는 방법{Method for manufacturing the detergent like soap using rice straw}Method for manufacturing the detergent like soap using rice straw}

본 발명은 비누제조방법에 관한 것으로서, 보다 특정적으로는 볏짚을 이용하여 비누와 같은 세제를 제조하는 방법에 관한 것이다.The present invention relates to a soap manufacturing method, and more particularly to a method for producing a detergent such as soap using rice straw.

경작지에서 쌀을 수확하면 남게 되는 볏짚은 예전에는 초가지붕의 이엉, 가마니, 새끼 또는 소의 여물 등으로 다양하게 사용되었으나, 근래에는 그의 활용도가 현격히 감소하였다. 근래에 볏짚은 논밭의 퇴비로도 사용되고 있으나, 화학비료에 비해 사용도가 만족스럽지 못한 것이 사실이다. 볏짚을 퇴비로 사용함에 있어서도, 그의 부식 속도가 느리기 때문에 퇴비 또는 거름으로도 부적합한 면이 있다.Rice straw left after harvesting rice in arable land was used in various ways as thatch, bale, foal or cattle trough of the thatched roof, but in recent years its utilization has decreased considerably. Recently, rice straw has been used as a compost in rice fields, but it is true that the use of rice straw is not satisfactory compared to chemical fertilizers. Even when rice straw is used for composting, its corrosion rate is low, so it is unsuitable for composting or manure.

볏짚의 주요 구성성분은 세룰로오스가 36%, 리그닌이 20%, 펜토산 22%, 조단백질 6% 및 회분이 13% 정도이다. 여기서, 리그닌은 볏짚의 부식 속도를 늦추는 중요한 요소가 된다. 리그닌은 셀룰로오스 및 헤미셀룰로오스와 함께 목질의 실질을 이루고 있는 성분으로서, 화학구조는 C18H24O11과 C40H45O18사이라고 추정되고 있다.The major components of rice straw are 36% cellulose, 20% lignin, 22% pentosan, 6% crude protein and 13% ash. Here, lignin is an important factor in slowing the corrosion rate of rice straw. Lignin, together with cellulose and hemicellulose, constitutes the substantial substance of wood, and its chemical structure is estimated to be between C 18 H 24 O 11 and C 40 H 45 O 18 .

근래에 들어 볏짚 또는 쌀겨 등이 인체에 유익하다는 것과 그의 활용에 대한 연구보고가 잇따르고 있는 실정이다. 본 발명은 볏짚이 가지는 이러한 유익한 점을 비누와 같은 세제에 활용하는 것을 목적으로 한다.Recently, rice straw or rice bran is beneficial to the human body and research reports on its use are continuing. The object of the present invention is to utilize these advantages of rice straw in detergents such as soap.

한편, 고래로부터 세제용으로 사용해왔던 재료로는, 짚이나 기타 초목을 태운 재를 걸러서 얻는 잿물이 있다. 이는 재에 포함되어 있는 수산화나트륨과 같은알칼리염(금속염)의 기능을 이용한 것이다.On the other hand, a material that has been used for detergents from whales is a lye obtained by filtering ashes of straw or other vegetation. This utilizes the function of alkali salts (metal salts) such as sodium hydroxide contained in the ash.

본 발명은 위와 같은 현실에 있는 볏짚의 활용도를 증대시키는 시키는 한편, 이를 이용하여 비누와 같은 세제의 원료를 제조하는 방법을 제공하는 것을 목적으로 한다. 본 발명의 다른 목적은 볏짚이 가지는 고유성분을 비누의 제조에 이용함으로써 미백효과 및 피부재생에 뛰어난 효과를 가지는 비누를 제공하는 것을 목적으로 한다.An object of the present invention is to increase the utilization of rice straw in the above reality, and to provide a method for producing a raw material of a detergent such as soap using the same. Another object of the present invention is to provide a soap having an excellent effect on the whitening effect and skin regeneration by using the inherent ingredients of rice straw in the production of soap.

도 1은 본 발명에 따른 각 단계를 설명하는 순서도이다.1 is a flow chart illustrating each step according to the present invention.

상기한 목적은, 볏짚을 세척 및 건조하는 볏짚 준비단계; 상기 볏짚을 연소하는 연소단계; 연소 후 잔류하게 되는 볏짚의 재(灰)를 정제하여 알칼리염을 정제 추출하며, 남은 재는 농작물용 퇴비로 사용할 수 있도록 배출 저장하는 알칼리염 추출단계; 추출된 상기 알칼리염을 사용하여 비누, 샴푸를 포함하는 세제를 제조하는 세제 제조단계를 포함하는 것을 특징으로 하는 볏짚을 이용한 비누 등 세제 제조방법에 의해 달성된다.The above object is, rice straw preparation step of washing and drying rice straw; A combustion step of burning the rice straw; Alkali salt extraction step to purify the ash of the straw remaining after combustion to purify the alkaline salt, the remaining ash is discharged and stored to be used as a compost for crops; Using the extracted alkali salt is achieved by a detergent manufacturing method such as soap using rice straw, characterized in that it comprises a detergent manufacturing step of preparing a detergent comprising a soap, shampoo.

본 발명에 의하면, 상기 볏짚의 재는 퇴비용으로 사용하도록 하며, 상기 세제는 물비누, 가루비누 또는 고형의 미용비누 등의 제조를 위해 활용될 수 있다.According to the present invention, the ash of the rice straw is to be used as a composting cost, the detergent may be utilized for the production of water soap, powdered soap or solid cosmetic soap.

이하, 본 발명의 실시예를 도 1에 도시된 순서도를 참조로 하여 더욱 상세히설명한다.Hereinafter, an embodiment of the present invention will be described in more detail with reference to the flowchart shown in FIG. 1.

<볏짚 준비단계>Rice Straw Preparation

볏짚 준비단계(S100)에서는 볏짚을 연소하기 적당한 정도로 세척 및 건조시킨다. 세척은 볏짚에 부착된 흙 등의 불순물을 분리하기 위한 과정이며, 건조방법은 자연건조도 무방하겠지만, 건조로를 통한 강제 건조도 가능할 것이다. 또한, 용이한 취급과 연소를 위해 분쇄단계가 부가될 수 있다. 본 실시예에서는 단지 볏짚에 관하여 설명되고 있지만, 반드시 이에 한정되지 아니하고 보릿짚 또는 밀짚도 가능하다.In the rice straw preparation step (S100), the rice straw is washed and dried to a suitable degree for burning. Washing is a process for separating impurities such as soil attached to rice straw, and the drying method may be natural drying, but forced drying through a drying furnace may be possible. In addition, a grinding step can be added for easy handling and combustion. Although only the rice straw is described in the present embodiment, barley straw or straw is not necessarily limited thereto.

<볏짚 연소단계>Rice straw burning stage

위 단계에서 준비된 볏짚을 연소로에 투입하여 화염에 의해 직접적으로 연소하는 단계(S200)가 이어진다. 이 과정은 볏짚으로부터 재(灰)를 얻기 위한 단계로서, 이에 의해 볏짚의 부패에 저해요인이 되었던 리그닌이 볏짚을 구성하는 다른 물질들과 함께 연소되게 된다.The rice straw prepared in the above step is put into a combustion furnace to directly burn by flame (S200). This process is to obtain ash from rice straw, whereby lignin, which has been a deterrent to rice straw's decay, is burned along with other materials that make up rice straw.

<알칼리염 추출단계><Alkali Salt Extraction Step>

알칼리염 추출단계(S300)는 위 단계(S200)에서 획득한 재를 물에 담그어 그 웃물을 걸러낸 것 즉, 잿물을 획득하기 위한 단계이다. 볏짚의 재는 주로 알칼리성을 가지는 탄산칼륨(K2CO3), 수산화나트륨(NaOH) 등을 포함하는데 이에 의해 잿물이 세정작용을 하게 되는 것으로서 이와 같은 사항은 고래로부터 확인된 사항이다.Alkaline salt extraction step (S300) is a step for obtaining the lye, that is, filtered the water by dipping the ash obtained in the above step (S200) in water. The ash of rice straw mainly contains alkaline potassium carbonate (K 2 CO 3 ), sodium hydroxide (NaOH), etc. The lye is washed by this, which is confirmed by whales.

본 발명에 의하면 알칼리 수용액을 더욱 정제하여 알칼리 용액의 농도를 변경시켜 사용할 수 있으며, 염석과정을 통해 잔류물질을 추출함으로써 획득되는 정도 높은 알칼리염을 사용할 수도 있다.According to the present invention, the alkali aqueous solution may be further purified to change the concentration of the alkaline solution, and an alkali salt having a high degree obtained by extracting the residual material through the salting process may be used.

< 세제 제조단계 ><Detergent Manufacturing Step>

세제 제조단계(S400)는 위 단계(S300)에서 추출된 알칼리 수용액 또는 염을 사용하여 비누를 포함하는 세제를 가공하는 과정으로서, 다양한 방법으로 구현될 수 있다. 가장 기본적인 방법은 추출된 알칼리수용액과 원료유지를 혼합하여 알칼리비누를 제조하는 방법일 것이다. 원료유지는 우지, 야자유, 팜유, 미강유(米糠油)가 사용될 수 있으며, 콩기름, 면실유, 어유(魚油) 또는 피마자유에서 구할 수 있는 경화유 및 각종 지방산 등이 사용될 수 있다.Detergent manufacturing step (S400) is a process of processing a detergent containing a soap using an aqueous alkali solution or salt extracted in the above step (S300), it can be implemented in various ways. The most basic method may be a method of preparing an alkaline soap by mixing the extracted alkaline aqueous solution and the raw material oil and fat. Raw material oil may be used, such as Uji, palm oil, palm oil, rice bran oil, may be used for soybean oil, cottonseed oil, fish oil or castor oil and hardened oil and various fatty acids.

본 발명의 일 실시예에 따르면, 정제 추출된 알칼리염 5W% - 15W%, 물 2W% - 5W%, 합성 에스테르를 이루게 하는 고급지방산 20W% - 40W% 및 3가 알코올인 글리세롤 50W% - 70W%를 주성분으로 혼합하고, 이 혼합물을 100℃ - 200℃ 정도로 가열하여 고형화시킴으로써 비누를 제조할 수 있다. 고형화된 비누원재는 소정의 커팅공정에 의해 요망하는 모양으로 가공될 수 있다. 여기에 종래 비누의 제조에 사용되는 향료 등을 첨가할 수 있음은 물론이다.According to one embodiment of the invention, the purified extracted alkali salt 5W%-15W%, water 2W%-5W%, 20W%-40W% higher fatty acids to form a synthetic ester and glycerol 50W%-70W% trihydric alcohol Can be prepared by mixing as a main component and solidifying by heating the mixture to about 100 ℃-200 ℃. The solidified soap raw material can be processed into a desired shape by a predetermined cutting process. It is of course possible to add a fragrance or the like used in the manufacture of conventional soap.

본 발명의 다른 실시예에 의하면, 위에서 예시한 비누(또는 미용비누)의 제조에 미세하게 분쇄된 볏짚 파우더를 전체 혼합물에 대하여 0.02W% - 20W% 정도 배합시킬 수 있다. 또한, 볏짚을 연소하여 얻은 재를 위의 볏짚 파우더와 함께 또는 선택적으로 0.02W% - 10W% 정도 배합시킬 수 있다. 이러한 볏짚은 피부 맛사지에 뛰어한 효과를 제공하게 된다.According to another embodiment of the present invention, the finely ground rice straw powder may be blended in an amount of 0.02W% to 20W% with respect to the entire mixture. In addition, the ash obtained by burning rice straw may be combined with the rice straw powder or optionally 0.02W% -10W%. This rice straw will provide an excellent effect on the skin massage.

본 발명의 또 다른 실시예에 의하면, 상기 알칼리염을 온천수와 같은 인체에 유익한 담수, 향료 기타 일반 액상 세제 또는 물비누 등을 제조할 때 사용되어 온 재료를 배합하여 샴푸, 액상 세제 또는 물비누를 제조할 수 있다.According to another embodiment of the present invention, to prepare a shampoo, liquid detergent or water soap by combining the alkali salt with materials that have been used in the production of fresh water, fragrance and other general liquid detergent or water soap, such as hot water, which is beneficial to the human body. Can be.

본 발명의 또 다른 실시예에 의하면, 볏짚을 연소함으로써 발생되는 열을 난방장치에 인출하여 사용할 수 있다. 그 난방장치는 비닐하우스의 난방에 이용할 수 있으며, 가용으로 사용할 수도 있다. 그러므로 본 발명에 의하면, 볏짚 건조장치 및 연소장치, 나트륨염 정제장치, 비누 등 세제의 제조장치, 연소열을 이용한 난방장치를 하나의 시스템으로 구성할 수 있다.According to another embodiment of the present invention, heat generated by burning rice straw can be used by drawing out a heating device. The heating system can be used to heat the plastic house, or it can be used as available. Therefore, according to the present invention, a straw straw drying apparatus and a combustion apparatus, a sodium salt refining apparatus, a manufacturing apparatus for detergents such as soap, and a heating apparatus using combustion heat can be configured as one system.

이와 같이, 본 발명은 볏짚을 연소하여 여기에서 추출되는 비누 등 세제의 원료를 구함으로써, 볏짚을 퇴비로 활용할 수 있게 하는 데 핵심적인 기술적 사상이 있으며, 또한 볏짚을 비누 파우더를 직접 비누에 배합 적용하는 것에 그 기술적 특징이 있다 하겠다.As described above, the present invention has a core technical idea of making rice straws compostable by combusting rice straw to obtain raw materials of detergents such as soap extracted therefrom, and applying rice straw directly to soap powder. There are technical features to doing that.

본 발명에 의하면, 연소 및 추출과정 후 남게 되는 재는 바로 퇴비로 사용할수 있다. 그러므로 볏짚을 퇴비로 사용함에 있어서, 부패지연에 따른 문제가 없게 된다.According to the present invention, the ash remaining after the combustion and extraction process can be used as compost. Therefore, when using rice straw as compost, there is no problem of delayed decay.

또한, 볏짚으로부터 추출한 알칼리 용액을 비누를 포함하는 세제의 제조에 활용함으로써 볏짚의 활용도를 배가시키게 된다. 또한, 볏짚을 연소시킴으로써 발생되는 연소열을 난방장치로 활용함으로써 시스템의 효율을 제고할 수 있다. 또한, 이렇게 제조된 비누는 볏짚이 가지는 고유성분에 의해 미백효과 및 피부재생효과가 뛰어나게 된다.In addition, by utilizing the alkaline solution extracted from the rice straw in the manufacture of detergents containing soap, the utilization of rice straw is doubled. In addition, the efficiency of the system can be improved by utilizing the heat of combustion generated by burning rice straw as a heating device. In addition, the soap thus prepared is excellent in the whitening effect and skin regeneration effect by the inherent ingredients of rice straw.

Claims (3)

볏짚을 세척 및 건조하는 볏짚 준비단계; 상기 볏짚을 연소하는 연소단계; 연소 후 남게 되는 볏짚의 재(灰)를 정제하여 알칼리염을 정제 추출하며, 남은 재는 농작물용 퇴비로 사용할 수 있도록 배출 저장하는 알칼리염 추출단계; 추출된 상기 알칼리염을 사용하여 비누, 샴푸를 포함하는 세제를 제조하는 세제 제조단계를 포함하는 것을 특징으로 하는 볏짚을 이용한 비누 등 세제 제조방법.Rice straw preparation step of washing and drying rice straw; A combustion step of burning the rice straw; An alkali salt extraction step of purifying ash of the straw remaining after combustion to purify the alkali salt, and extracting and storing the remaining ash to be used as compost for crops; Detergent manufacturing method such as soap using rice straw, characterized in that it comprises a detergent manufacturing step of preparing a detergent comprising a soap, shampoo using the extracted alkali salt. 제 1항에 있어서, 상기 세제 제조단계는 정제 추출된 알칼리염 5W% - 15W%, 물 2W% - 5W%, 및 합성 에스테르를 이루게 하는 고급지방산 20W% - 40W%, 및 글리세롤 50W% - 70W%를 주성분으로 혼합하여 혼합물을 조성한 후 이 혼합물을 100℃ - 200℃로 가열하여 고형화함으로써 비누를 제조하는 것을 특징으로 하는 볏짚을 이용한 비누 등 세제 제조방법.The method of claim 1, wherein the detergent preparation step is 5W% -15W% of purified salt, 2W% -5W% of water, and 20W% -40W% of fatty fatty acid to form a synthetic ester, and 50W% -70W% of glycerol. After preparing a mixture by mixing as a main component to prepare a soap by heating the mixture to 100 ℃-200 ℃ solid soap, characterized in that for producing soap using rice straw. 제 2항에 있어서, 상기 혼합물에 0.02W% - 20W% 정도의 분쇄 준비된 볏짚 파우더 및/또는 연소 후 잔류하는 볏짚의 재를 0.02W% - 10W% 정도 더 배합하는 것을 특징으로 하는 볏짚을 이용한 비누 등 세제 제조방법.The rice straw soap according to claim 2, further comprising 0.02W%-20W% of rice straw powder prepared for crushing and / or ash of rice straw remaining after combustion, in an amount of 0.02W%-10W%. Detergent manufacturing method.
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20020067479A (en) * 2002-08-01 2002-08-22 황규옥 Functional soap bar using agricultural by-products and the process for preparing the same
WO2017059873A1 (en) * 2015-10-08 2017-04-13 Meaad Amina Mohamed Ahmed A soap made of rice straw

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KR950018418A (en) * 1993-12-31 1995-07-22 임경희 Manufacturing method of washing liquid
KR970006250A (en) * 1995-07-21 1997-02-19 안용식 Manufacturing method and apparatus for substitute soil for crop sowing
KR20010089866A (en) * 2000-03-24 2001-10-12 김점선 Manufacturing method of liquid soap affiliated for protecting environment

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR920018208A (en) * 1991-03-19 1992-10-21 전정숙 Glossy soap manufacturing method
KR920018212A (en) * 1991-03-28 1992-10-21 정해순 Manufacturing method of pollution-free natural liquid detergent
KR950005971A (en) * 1993-08-12 1995-03-20 김복동 Manufacturing method of multi-purpose complete pollution-free cleaner
KR950018418A (en) * 1993-12-31 1995-07-22 임경희 Manufacturing method of washing liquid
KR970006250A (en) * 1995-07-21 1997-02-19 안용식 Manufacturing method and apparatus for substitute soil for crop sowing
KR20010089866A (en) * 2000-03-24 2001-10-12 김점선 Manufacturing method of liquid soap affiliated for protecting environment

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20020067479A (en) * 2002-08-01 2002-08-22 황규옥 Functional soap bar using agricultural by-products and the process for preparing the same
WO2017059873A1 (en) * 2015-10-08 2017-04-13 Meaad Amina Mohamed Ahmed A soap made of rice straw

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