KR20020067171A - Wild Vegetable and Manufacturing Method for Thereof and Manufacturing Method for Tablet with Wild Vegetable Extract Powder - Google Patents
Wild Vegetable and Manufacturing Method for Thereof and Manufacturing Method for Tablet with Wild Vegetable Extract Powder Download PDFInfo
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- KR20020067171A KR20020067171A KR1020010007582A KR20010007582A KR20020067171A KR 20020067171 A KR20020067171 A KR 20020067171A KR 1020010007582 A KR1020010007582 A KR 1020010007582A KR 20010007582 A KR20010007582 A KR 20010007582A KR 20020067171 A KR20020067171 A KR 20020067171A
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- 239000000284 extract Substances 0.000 title claims abstract description 99
- 239000000843 powder Substances 0.000 title claims abstract description 25
- 235000013311 vegetables Nutrition 0.000 title claims description 54
- 238000004519 manufacturing process Methods 0.000 title claims description 18
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- DLRVVLDZNNYCBX-UHFFFAOYSA-N Polydextrose Polymers OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(O)O1 DLRVVLDZNNYCBX-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000002904 solvent Substances 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 10
- 229930091371 Fructose Natural products 0.000 claims abstract description 9
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims abstract description 9
- 239000005715 Fructose Substances 0.000 claims abstract description 9
- 239000008213 purified water Substances 0.000 claims abstract description 9
- 229920001100 Polydextrose Polymers 0.000 claims abstract description 8
- 239000001259 polydextrose Substances 0.000 claims abstract description 8
- 229940035035 polydextrose Drugs 0.000 claims abstract description 8
- 235000013856 polydextrose Nutrition 0.000 claims abstract description 8
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 23
- 241001474374 Blennius Species 0.000 claims description 20
- 239000002253 acid Substances 0.000 claims description 20
- 235000013361 beverage Nutrition 0.000 claims description 17
- 239000001522 artemisia absinthium l. herb extract Substances 0.000 claims description 11
- 229940119569 wormwood extract Drugs 0.000 claims description 11
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 9
- 235000020230 cinnamon extract Nutrition 0.000 claims description 9
- 235000009051 Ambrosia paniculata var. peruviana Nutrition 0.000 claims description 8
- 235000003097 Artemisia absinthium Nutrition 0.000 claims description 8
- 240000001851 Artemisia dracunculus Species 0.000 claims description 8
- 235000017731 Artemisia dracunculus ssp. dracunculus Nutrition 0.000 claims description 8
- 235000003261 Artemisia vulgaris Nutrition 0.000 claims description 8
- 239000001138 artemisia absinthium Substances 0.000 claims description 8
- 235000019206 astragalus extract Nutrition 0.000 claims description 8
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 8
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 5
- 239000008103 glucose Substances 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 241001247821 Ziziphus Species 0.000 claims 2
- 239000000796 flavoring agent Substances 0.000 abstract description 9
- 235000019634 flavors Nutrition 0.000 abstract description 9
- 244000126002 Ziziphus vulgaris Species 0.000 abstract description 7
- 235000014680 Saccharomyces cerevisiae Nutrition 0.000 abstract description 6
- 239000003963 antioxidant agent Substances 0.000 abstract description 5
- 230000003078 antioxidant effect Effects 0.000 abstract description 5
- 241000527163 Aster scaber Species 0.000 abstract description 2
- 235000005276 Doellingeria scabra Nutrition 0.000 abstract description 2
- 241001113320 Ligularia fischeri Species 0.000 abstract description 2
- 241000196324 Embryophyta Species 0.000 abstract 4
- 239000000419 plant extract Substances 0.000 abstract 3
- 241000907784 Aster glehnii Species 0.000 abstract 1
- 244000080208 Canella winterana Species 0.000 abstract 1
- 235000008499 Canella winterana Nutrition 0.000 abstract 1
- 244000090125 Solidago odora Species 0.000 abstract 1
- 235000010394 Solidago odora Nutrition 0.000 abstract 1
- 235000008529 Ziziphus vulgaris Nutrition 0.000 abstract 1
- 229940017545 cinnamon bark Drugs 0.000 abstract 1
- 235000019645 odor Nutrition 0.000 description 20
- 241000282458 Ursus sp. Species 0.000 description 19
- 238000000605 extraction Methods 0.000 description 12
- 230000002378 acidificating effect Effects 0.000 description 8
- 230000001953 sensory effect Effects 0.000 description 8
- 244000000231 Sesamum indicum Species 0.000 description 7
- 235000003434 Sesamum indicum Nutrition 0.000 description 7
- 238000012360 testing method Methods 0.000 description 7
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 5
- 235000013305 food Nutrition 0.000 description 5
- 239000008187 granular material Substances 0.000 description 5
- 235000013824 polyphenols Nutrition 0.000 description 5
- 244000007021 Prunus avium Species 0.000 description 4
- 235000010401 Prunus avium Nutrition 0.000 description 4
- 235000014441 Prunus serotina Nutrition 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 239000004480 active ingredient Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 235000019629 palatability Nutrition 0.000 description 3
- 150000008442 polyphenolic compounds Chemical class 0.000 description 3
- 235000012046 side dish Nutrition 0.000 description 3
- 102000007330 LDL Lipoproteins Human genes 0.000 description 2
- 108010007622 LDL Lipoproteins Proteins 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 239000001525 mentha piperita l. herb oil Substances 0.000 description 2
- 238000000874 microwave-assisted extraction Methods 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 235000019477 peppermint oil Nutrition 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 235000013616 tea Nutrition 0.000 description 2
- 238000010953 Ames test Methods 0.000 description 1
- 231100000039 Ames test Toxicity 0.000 description 1
- 241000132092 Aster Species 0.000 description 1
- 241001061264 Astragalus Species 0.000 description 1
- 244000223760 Cinnamomum zeylanicum Species 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 241000237502 Ostreidae Species 0.000 description 1
- 244000131316 Panax pseudoginseng Species 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 238000000944 Soxhlet extraction Methods 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000000843 anti-fungal effect Effects 0.000 description 1
- 230000002790 anti-mutagenic effect Effects 0.000 description 1
- 235000006533 astragalus Nutrition 0.000 description 1
- 235000017803 cinnamon Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000010230 functional analysis Methods 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 239000008601 oleoresin Substances 0.000 description 1
- 235000020636 oyster Nutrition 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 235000021067 refined food Nutrition 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 210000004233 talus Anatomy 0.000 description 1
- 235000015192 vegetable juice Nutrition 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/08—Concentrating or drying of juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/30—Foods, ingredients or supplements having a functional effect on health
- A23V2200/302—Foods, ingredients or supplements having a functional effect on health having a modulating effect on age
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/30—Foods, ingredients or supplements having a functional effect on health
- A23V2200/308—Foods, ingredients or supplements having a functional effect on health having an effect on cancer prevention
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/02—Acid
- A23V2250/032—Citric acid
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
- A23V2250/2132—Other phenolic compounds, polyphenols
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/48—Ultrasonic treatment
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Non-Alcoholic Beverages (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
Description
본 발명은 우리나라 야산에서 자생하거나 재배하고 있는 산채중에서 참취 추출물, 곰취 추출물, 미역취 추출물 또는 섬쑥부쟁이 추출물을 함유한 산채음료, 산채음료의 제조방법 및 상기 산채추출물을 분말화 한 것을 유효성분으로 함유하는 타블렛의 제조방법에 관한 것이다.The present invention contains wild scent extract, bear squirt extract, seaweed odor extract or wormwood extract from the wild vegetables grown or grown in Yasan in Korea, the production method of sanchae beverages and powdered acid extracts as an active ingredient It relates to a method for producing a tablet.
과거 산채는 영양적인 면이나 기호적인 면에서 주목받지 못했으나 차나 채소 등에는 폴리페놀 성분이 함유되어 항산화성, 항암성, 진균성 등의 기능성이 있는 것으로 보고되고 있고 야생 산채도 이들과 같이 기능성 식품으로써 이용가치가 높을 것으로 기대되고 있다.In the past, wild vegetables have not received attention in terms of nutrition and taste, but teas and vegetables contain polyphenols and are reported to have antioxidant, anti-cancer, and fungal properties. Wild wild vegetables are also functional foods. As a result, the value of use is expected to be high.
산채류로서 국화과에 속하는 다년초인 곰취(Ligularia fischeri), 참취(Aster scaber), 미역취(Solidage virga-aurea), 섬쑥부쟁이(Aster glehni) 등 역시 항산화성등 기능성이 우수한 폴리페놀 성분이 함유되고 있을 가능성이 높다. 함 등은 국내에서 자생하는 산채의 착즙액에서 항 돌연변이성을 보고하였는데 곰취 및 참취 추출물 역시 Ames test 결과 높은 항 돌연변이성을 나타내었다고 하였다(함등, 한국식품영양과학회, 1997년). 또한 곰취를 물, 메탄올 및 에탄올로 추출하고 그 추출물의 저밀도 지방 단백질(low density lipoprotein, LDL)에 대한 산화 억제력 등을 측정한 결과 곰취의 메탄올 추출물에서 특히 높은 항산화 효과를 보였다고 하였다(정등, 한국식품과학회지, 1998).As a wild vegetable, the perennial herb, Ligularia fischeri , Aster scaber , Seaweed ( Solidage virga-aurea ), Aster glehni , etc., may also contain polyphenols with excellent functional properties such as antioxidants. This is high. Hamm et al. Reported antimutagenicity in Korean wild vegetable juices. The extracts of bear and tuna were also highly antimutagenic by Ames test (Hamdeung, Korean Society of Food and Nutrition, 1997). In addition, the extracts of bear odor were extracted with water, methanol and ethanol, and the antioxidant activity of low density lipoprotein (LDL) of the extract was measured. Journal of Science, 1998).
지금까지 산채류는 주로 나물 또는 기타 반찬에 첨가되는 부재료의 형태로 반찬으로 식사시 한 반찬의 형태로 섭취되었으나 이들을 음료나 차와 같은 기호식품의 형태로 가공한다면 보다 용이하게 기능성 성분을 섭취할 수 있을 것이며 또한 폴리페놀은 물이나 알코올에 쉽게 용해되므로 가공식품으로 적용하기에 용이할 것이나 아직까지 이러한 산채를 이용한 기호식품은 시중에 알려지지 않고 있다.Until now, wild vegetables have been consumed in the form of side dishes when eaten as a side dish, mainly in the form of subsidiary ingredients added to herbs or other side dishes, but if they are processed in the form of foods such as drinks or tea, functional ingredients can be easily consumed. In addition, polyphenols are easily soluble in water or alcohol, so they may be easily applied as processed foods. However, the favorite foods using such wild vegetables are not known on the market.
한편, 산채를 음료로 가공하는데 있어서 가장 우선적으로 고려해야 할 것은 추출 방법이라고 할 수 있으며 이때 효율적인 추출 방법을 선택하는 것이 중요한문제가 될 수 있다. 이미 오랫동안 환류 냉각 추출(reflux extraction) 방법이 산채를 비롯한 많은 식품의 추출 방법으로 이용되어 왔으나 추출하는데 2시간 이상의 긴 시간을 요하며, 또한 추출효율이 낮다는 것이 문제점으로 지적되어 왔다.On the other hand, the first thing to consider in the processing of wild vegetables into beverages can be said to be an extraction method, it may be an important problem to choose an efficient extraction method. Already, reflux extraction has been used for extraction of many foods including wild vegetables, but it has been pointed out that it takes longer than 2 hours to extract and low extraction efficiency.
마이크로파 추출(microwave-assisted extraction) 방법은 직접적으로 마이크로파가 식품의 내부에서 외부로 전달되는 방식이기 때문에 환류냉각 추출, Soxhlet 추출법 등 기존의 추출 방법보다 적은 용매를 사용하여 단시간에 효율적으로 추출 할 수 있으며 특히 전체 고형분보다 원하는 성분을 추출하는데 효과적인 것으로 알려져 있다. Pare 등은 박하 잎을 가지고 2시간 동안 수증기 증류하여 0.3%의 박하유를 얻은 반면 40초 동안의 마이크로웨이브 조사에 의해 0.30∼0.47%의 박하유를 얻었다고 하였다. 또한 인삼을 가지고 동일온도 및 용매조건에서 추출했을 때 8분 동안의 마이크로웨이브 추출에 의하여 기존의 8시간 추출에서와 같은 함량의 사포닌과 진세노이드(ginsenoid)를 갖는 올레오레진을 얻었다는 연구 결과도 보고되고 있다. 그러나 곰취, 참취, 미역취, 섬쑥부쟁이를 대상으로 한 마이크로파 추출방법, 산채 추출물의 기능성 분석 및 산채 추출물을 이용한 가공제품에 관한 연구는 거의 없는 실정이다.The microwave-assisted extraction method is a method in which microwaves are directly transferred from inside to outside of the food, so that extraction can be performed in a short time by using less solvent than conventional extraction methods such as reflux cooling extraction and Soxhlet extraction method. In particular, it is known to be effective in extracting the desired components rather than the total solids. Pare et al. Reported that peppermint oil of 0.3% was obtained by steam distillation with peppermint leaves for 2 hours while peppermint oil of 0.30 to 0.47% was obtained by microwave irradiation for 40 seconds. In addition, the results of the study showed that when extracted with ginseng at the same temperature and solvent conditions, oleoresin having saponin and ginsenoid of the same content as in the conventional 8-hour extraction was obtained by microwave extraction for 8 minutes. Is being reported. However, there are very few studies on the extraction of microwaves, the functional analysis of wild vegetable extracts, and processed products using wild vegetable extracts.
본 발명은 곰취, 참취, 미역취, 섬쑥부쟁이로부터 마이크로파를 이용하여 유효성분을 효율적으로 추출하고 이러한 산채 추출물을 함유하는 산채음료, 산채음료의 제조방법 및 상기 산채추출물을 분말화 한 것을 유효성분으로 함유한 타블렛의제조방법의 제공을 목적으로 한다.The present invention efficiently extracts the active ingredient from the bear odor, scented oyster, seaweed odor, wormwood using the microwave and the acidic beverage containing the acid extract, the production method of the acidic beverage and the powdered acid extract as an active ingredient An object of the present invention is to provide a method for producing a tablet containing.
도 1은 산채인 참취 추출물, 곰취 추출물, 미역취 추출물 또는 섬쑥부쟁이 추출물을 함유한 산채음료의 제조공정도 이다.1 is a manufacturing process diagram of the wild vegetable extract containing wild cherries extract, bear odor extract, seaweed odor extract or wormwood extract.
도 2는 도 1의 제조공정도 중 산채추출물을 분말화 한 것을 함유하는 타블렛의 제조공정도 이다.FIG. 2 is a manufacturing process diagram of a tablet containing the powdered acid extract of the manufacturing process diagram of FIG. 1.
본 발명은 산채 추출물을 함유하는 산채음료 및 산채음료의 제조방법과 전기의 산채추출물을 분말화 한 것을 함유하는 타블렛의 제조방법으로 이루어져 있다.The present invention consists of a method for producing an acidic beverage and an acidic beverage containing an acid extract and a method for producing a tablet containing the powdered acid extract of the previous.
먼저 본 발명의 산채 추출물을 함유하는 산채음료는 산채 추출물 0.3∼0.5 중량%, 정제수 80∼90 중량%, 황기추출물 0.2∼0.5 중량%, 대추추출물 0.1∼0.5 중량%, 계피추출물 0.01∼0.05 중량%, 설탕:고과당(1:1) 5∼12.0 중량%, 구연산 0.05∼0.2 중량% 포함하며 상기에서 산채 추출물은 곰취 추출물, 참취 추출물, 미역취 추출물 또는 섬쑥부쟁이 추출물을 나타낸다.First, the wild vegetable drink containing the wild vegetable extract of the present invention is 0.3-0.5% by weight of wild vegetable extract, 80-90% by weight of purified water, 0.2-0.5% by weight of Astragalus extract, 0.1-0.5% by weight of jujube extract, 0.01-0.05% by weight of cinnamon extract , Sugar: High fructose (1: 1) 5 to 12.0% by weight, citric acid 0.05 to 0.2% by weight, wherein the acid extract extract bear extract, sesame extract, seaweed extract or wormwood extract.
한편 산채음료의 제조방법은 산채를 수세하는 단계와;On the other hand, the manufacturing method of the wild vegetable drink and washing the wild vegetable;
물기를 제거하고 산채를 마쇄하는 단계와;Removing water and crushing the wild vegetables;
마쇄한 산채를 물, 50∼70% 에탄올 또는 메탄올 용매에 첨가한 후 100∼300W의 마이크로파 에너지를 1∼15분 동안 처리하여 추출물을 얻는 단계와;Adding crushed wild vegetables to water, 50-70% ethanol or methanol solvent, and then processing 100-300 W microwave energy for 1-15 minutes to obtain an extract;
산채 추출물을 여과하고 농축하는 단계와;Filtering and concentrating the wild vegetable extract;
상기 단계에서 얻은 산채 추출물 0.3∼0.5 중량%와 부재료로 정제수 80∼90 중량%, 황기추출물 0.2∼0.5 중량%, 대추추출물 0.1∼0.5 중량%, 계피추출물 0.01∼0.05 중량%, 설탕과 고과당이 1:1의 비로 혼합된 혼합물 5∼12.0 중량%, 구연산 0.05∼0.2 중량%를 혼합하는 단계를 포함하는 것을 특징으로 하며 상기에서 산채는곰취, 참취, 미역취 또는 섬쑥부쟁이를 나타낸다.0.3-0.5% by weight of the wild vegetable extract obtained in the above step and 80-90% by weight of purified water, 0.2-0.5% by weight of Astragalus extract, 0.1-0.5% by weight of jujube extract, 0.01-0.05% by weight of cinnamon extract, sugar and high fructose 5 to 12.0% by weight of the mixture in a ratio of 1: 1, 0.05 to 0.2% by weight of citric acid, characterized in that it comprises a step wherein the wild cherries, tuna odor, seaweed odor or wormwood.
상기 산채음료의 제조방법에서 산채 추출물인 곰취 추출물, 참취 추출물, 미역취 추출물 또는 섬쑥부쟁이 추출물을 0.3 중량% 미만 사용하면 산채의 향미나 항산화력이 낮은 문제가 있고, 0.5 중량% 초과 사용하면 맛과 향에서 거부감을 주는 문제가 있어 산채 추출물은 0.3∼0.5 중량%를 유지하는 것이 좋다.When the acid extract is less than 0.3% by weight of the extract of wild cherries, bear odor extract, sesame odor extract, seaweed odor extract or wormwood extract in the production method of the acidic beverage, there is a problem of low flavor or antioxidant power of acid extract, taste and There is a problem of rejection in the fragrance, it is good to keep the extract of 0.3 ~ 0.5% by weight.
정제수는 80 중량% 미만 사용하면 부적합한 향미에 문제가 있고, 90 중량% 초과 사용하면 향미가 약한 문제가 있어 정제수는 80∼90 중량%를 유지하는 것이 좋다.If the amount of purified water is less than 80% by weight, there is a problem of inadequate flavor, and if it is used more than 90% by weight, there is a problem of weak flavor, it is preferable to maintain the purified water 80 to 90% by weight.
황기 추출물은 0.2 중량% 미만 사용하면 황기의 향미가 낮아지는 문제가 있고, 0.5 중량% 초과 사용하면 산채추출물의 향미가 나타나지 않는 문제가 있어 황기 추출물은 0.3∼0.5 중량%를 유지하는 것이 좋다.Astragalus extract has a problem that the flavor of the astragalus is lowered when used less than 0.2% by weight, there is a problem that the flavor of the wild vegetable extract does not appear when using more than 0.5% by weight, the Astragalus extract is good to maintain 0.3 to 0.5% by weight.
대추 추출물은 0.1 중량% 미만 사용하면 단맛이 미약한 문제가 있고, 0.5 중량% 초과 사용하면 단맛이 너무 강해지는 문제가 있어 대추 추출물은 0.3∼0.5 중량%를 유지하는 것이 좋다.Jujube extract is less than 0.1% by weight, the sweetness of the problem is weak, and when used more than 0.5% by weight, the sweetness is too strong problem, jujube extract is good to maintain 0.3 ~ 0.5% by weight.
계피 추출물은 0.01 중량% 미만 사용하면 산채와의 풍미조화가 낮아지는 문제가 있고, 0.05 중량% 초과 사용하면 계피의 강한 자극성에 의해 산채음료의 기호성이 저하되는 문제가 있어 계피 추출물은 0.01∼0.05 중량%를 유지하는 것이 좋다.If the cinnamon extract is less than 0.01% by weight, there is a problem that the flavor coordination with the wild vegetables is lowered. If the cinnamon extract is used more than 0.05% by weight, the palatability of the acidic beverage is lowered due to the strong irritancy of the cinnamon, and the cinnamon extract is 0.01 to 0.05% by weight. It is good to keep%.
설탕과 고과당이 1:1의 비로 혼합된 혼합물은 5 중량% 미만 사용하면 감미가 약한 문제가 있고, 12 중량% 초과 사용하면 감미가 너무 강한 문제가 있어 적절한산채음료의 감미를 위해서는 설탕:고과당(1:1)은 5∼12 중량%를 유지하는 것이 좋다.A mixture of sugar and high fructose in a ratio of 1: 1 has a weak sweetness when used less than 5% by weight, and a sweetness is too strong when used more than 12% by weight. Fructose (1: 1) is preferably maintained at 5 to 12% by weight.
구연산은 0.05 중량% 미만 사용하면 음료의 적정 pH인 3.8∼3.9 수준의 조절에 어려운 문제가 있고, 0.2 중량% 초과 사용하면 신맛이 너무 강해 산채음료의 기호성을 저하시키는 문제가 있어 구연산은 0.05∼0.2 중량%를 유지하는 것이 좋다.When citric acid is used less than 0.05% by weight, it is difficult to control the level of 3.8 to 3.9, which is an appropriate pH of the beverage. When it is used above 0.2% by weight, citric acid is too strong to reduce palatability of acidic beverages. It is good to keep the weight percentage.
또한 산채추출물을 분말화 한 것을 함유하는 타브렛의 제조방법은 상기의 산채음료 제조하기 위한 참취 추출물, 곰취 추출물, 미역취 추출물 또는 섬쑥부쟁이 추출물 등의 산채추출물을 50∼70 brix로 농축 후 가당(加糖)하기 위하여 포도당 10∼20 중량% 첨가하고 건조한 후 분말화한 산채 추출물 분말 10∼30 중량%와 부재료로 맥주효모분말 40∼60 중량%, 폴리덱스트로스 10∼20 중량% 포함하도록 한다.In addition, the preparation method of the tablet containing powdered wild vegetable extract is concentrated to 50 ~ 70 brix of wild vegetable extract, such as sesame extract, bear odor extract, seaweed extract or wormwood extract for producing the above-mentioned wild vegetable beverage In order to add 10 to 20% by weight of glucose, and dried and 10-30% by weight of the powdered wild vegetable extract powder and 40 to 60% by weight of beer yeast powder and 10 to 20% by weight of polydextrose.
상기에서 산채 추출물을 50 brix 미만 농축하여 사용하면 저장성이 낮아지는 문제가 있고, 70 brix 초과 농축하여 사용하면 강한 점조성(粘稠性)으로 농축물을 다루기 어려울 뿐만 아니라 농축시 과도한 에너지가 소요되는 문제가 있어 산채 추출물은 50∼70 brix로 농축하는 것이 좋다.When the acid extract is concentrated below 50 brix, the storage property is lowered, and when it is used above 70 brix, it is difficult to handle the concentrate due to its strong consistency and the excessive energy is required during the concentration. There is a problem, and the extract of wild vegetables should be concentrated to 50 ~ 70 brix.
산채추출물을 가당하기 위하여 포도당 첨가시 10 중량% 미만이나 사용하거나 또는 20 중량% 초과 사용하면 타정이 되지 않는 문제가 있어 포도당은 10∼20 중량% 사용하는 것이 좋다.To add acid extract, less than 10% by weight, or more than 20% by weight of glucose, is not used for tableting, so it is better to use 10 to 20% by weight of glucose.
산채추출물을 분말화 한 것을 함유하는 타블렛의 제조시 산채추출물을 분말화 한 분말, 맥주효모분말, 폴리덱스트로스에 있어서 산채추출물을 분말화 한 분말은 10 중량% 미만 사용하면 과립형태의 분말이 형성되지 않는 문제가 있고, 30 중량% 초과 사용하면 과립형태의 분말에 있어서 분말의 과립조직이 단단해지는 문제가 있으며,In the manufacture of tablets containing powdered wild vegetable extract, powder of wild vegetable extract, brewer's yeast powder, and polydextrose powdered powder of wild vegetable extract do not form granular powder when used less than 10% by weight. There is a problem, and when used in excess of 30% by weight, there is a problem that the granular structure of the powder is hardened in the granular powder,
맥주효모분말은 40 중량% 미만 사용하면 타정이 어려운 문제가 있고, 60 중량% 초과 사용하면 타정된 타브렛의 강도가 너무 강한 문제가 있으며,Brewer's yeast powder has a problem that tableting is difficult when used less than 40% by weight, the strength of the tableted tablet is too strong when used over 60% by weight,
폴리덱스트로스는 10 중량% 미만 사용하면 결착력이 낮아지는 문제가 있고, 20 중량% 초과 사용하면 결착력이 강해 딱딱해지는 문제가 있어 산채추출물을 분말화 한 것을 함유하는 타블렛의 제조시 산채추출물을 분말화 한 과립분말은 10∼30 중량%, 맥주효모분말은 40∼60 중량%, 폴리덱스트로스는 10∼20 중량% 사용하는 것이 좋다.Polydextrose has a problem of low binding strength when used less than 10% by weight, and has a problem of hardening due to strong binding power when used above 20% by weight, and granules obtained by powdering wild vegetable extract during the manufacture of a tablet containing powdered acid extract It is preferable to use 10 to 30% by weight of powder, 40 to 60% by weight of beer yeast powder, and 10 to 20% by weight of polydextrose.
이하 본 발명을 다음의 실시예 및 시험예에 의하여 설명하고자 한다. 그러나 이들이 본 발명의 기술적 범위를 한정하는 것은 아니다.Hereinafter, the present invention will be described by the following examples and test examples. However, these do not limit the technical scope of the present invention.
<실시예 1><Example 1>
곰취, 참취, 미역취, 섬쑥부쟁이에 대해 물 또는 50∼99% 농도의 에탄올을 용매로 하고 60∼210W 강도의 마이크로파(microwave) 장치에서 10분 동안 처리하여 총 페놀 함량과 추출물의 전자공여능을 분석하여 그 결과를 표 1에 나타내었다.The total phenol content and the electron donating ability of extracts were analyzed by using water or 50 ~ 99% ethanol as a solvent for 10 minutes in a 60 ~ 210W intensity microwave apparatus The results are shown in Table 1.
표 1. 산채의 마이크로파 및 용매에 따른 페놀성분의 추출효과 및 전자공여능Table 1. Extraction Effect and Electron Donating Ability of Phenol Components by Microwave and Solvents of Wild Vegetables
A: 총 페놀 함량(%)A:% total phenolic content
B: 전자공여능(EDA%)B: electron donating ability (EDA%)
C: 50% 에탄올C: 50% ethanol
D: 70% 에탄올D: 70% ethanol
E: 99% 에탄올E: 99% ethanol
<실시예 2><Example 2>
곰취, 참취, 미역취, 섬쑥부쟁이에 대해 물 또는 50∼99% 농도의 에탄올을 용매로 하고 150W 강도의 마이크로파 장치에서 1∼15분 동안 처리하여 총 페놀 함량과 전자공여능을 분석하여 그 결과를 표 2에 나타내었다.Water, 50-99% ethanol as a solvent, and the total phenol content and electron donating ability were analyzed for 1-15 minutes in a 150W intensity microwave apparatus. 2 is shown.
표 2. 산채류의 마이크로파 처리시간 및 용매에 따른 페놀성분의 추출효과 및 전자공여능Table 2. Extraction Effect and Electron Donating Ability of Phenolic Compounds According to Microwave Processing Time and Solvent of Wild Vegetables
A: 총 페놀 함량(%)A:% total phenolic content
B: 전자공여능(EDA%)B: electron donating ability (EDA%)
C: 50% 에탄올C: 50% ethanol
D: 70% 에탄올D: 70% ethanol
E: 90% 에탄올E: 90% ethanol
<실시예 3><Example 3>
산채인 곰취, 참취, 미역취 또는 섬쑥부쟁이를 수세한 후 물기를 제거하고 곰취, 참취, 미역취 또는 섬쑥부쟁이를 20∼50메쉬(mesh)로 마쇄하였다.After washing the wild bear, tuna, seaweed or wormwood, the water was removed, and the bear, tuna, seaweed or wormwood was crushed to 20-50 mesh.
상기에서 마쇄한 곰취, 참취, 미역취 또는 섬쑥부쟁이를 물에 첨가하고 100∼150W의 마이크로파 에너지를 5∼10분 동안 처리하여 곰취 추출물, 참취 추출물, 미역취 추출물 또는 섬쑥부쟁이 추출물을 얻고 여과한 후 곰취 추출물은 1.6 brix로, 참취 추출물은 1.4 brix로, 미역취 추출물은 1.4 brix로 섬쑥부쟁이 추출물은 1.4 brix로 농축하였다.After adding the crushed bear odor, tuna odor, seaweed odor or wormwood to water and treating 100 ~ 150W microwave energy for 5-10 minutes to obtain the odor extract, tuna extract, seaweed odor extract or wormwood extract and filtered Bear extract was concentrated to 1.6 brix, sesame extract was 1.4 brix, seaweed extract was 1.4 brix, and wormwood extract was concentrated to 1.4 brix.
상기 단계에서 얻은 산채 추출물 0.3∼0.5 중량%, 정제수 80∼90 중량%, 황기추출물 0.2∼0.5 중량%, 대추추출물 0.1∼0.5 중량%, 계피추출물 0.01∼0.05 중량%, 설탕:고과당(1:1) 5∼12.0 중량%, 구연산 0.05∼0.2 중량%를 아래의 표 3과 같이 혼합하여 산채음료를 제조하였다.0.3 ~ 0.5% by weight of wild vegetable extract, 80-90% by weight of purified water, 0.2-0.5% by weight of astragalus extract, 0.1-0.5% by weight of jujube extract, 0.01-0.05% by weight of cinnamon extract, sugar: high fructose (1: 1) 5 to 12.0% by weight, 0.05 to 0.2% by weight citric acid was mixed as shown in Table 3 below to prepare an acidic beverage.
표 3. 산채음료 제품의 배합비(단위 : 중량%)Table 3. Mixing ratio of wild vegetable beverage products (unit: weight%)
<실시예 4><Example 4>
상기 실시예 3에서 제조한 곰취 추출물, 참취 추출물, 미역취 추출물 또는 섬쑥부쟁이 추출물 등의 산채 추출물 각각을 감압 농축기로 50∼70 brix 되게 농축하였다.Each of the wild vegetable extracts, such as bear extract, sesame extract, seaweed extract or wormwood extract prepared in Example 3, was concentrated to 50 to 70 brix with a reduced pressure concentrator.
산채 추출물을 농축 후 포도당 15 중량%을 첨가하고 공지의 방법으로 분무건조하여 분말화 한 후 과립분말을 제조하였으며 아래의 표 4와 같이 상기 산채 추출물을 분말화 한 과립분말 30 중량%, 맥주효모분말 60 중량%, 및 폴리덱스트로스 10중량%로 타브렛 제품을 제조하였다.After the acid extract was concentrated, 15% by weight of glucose was added, and the powder was dried by spray drying by a known method, and then granulated powder was prepared. Tabret products were made at 60% by weight, and 10% by weight polydextrose.
표 4. 산채 타블렛 제품 배합비(단위 : 중량%)Table 4. Composition of Wild Vegetable Tablets (Unit: wt%)
<시험예 1><Test Example 1>
남녀 각각 25명으로 구성된 관능평가 요원으로 하여금 5점 척도법에 의하여 상기 실시예 3에 의한 시료 1, 시료 2, 시료 3 및 시료 4에 대한 관능평가를 실시하여 그 결과를 아래의 표 5에 나타내었다.Sensory evaluation personnel consisting of 25 men and women each performed sensory evaluation on Sample 1, Sample 2, Sample 3, and Sample 4 according to Example 3 by the 5-point scale method, and the results are shown in Table 5 below. .
관능검사 결과는 남녀 각각 25명이 5점을 만점으로 하여 각각의 점수를 합한 후 이를 인원수로 나눈 결과로서 소수점 2자리에서 반올림한 결과이다.The result of sensory test was the result of twenty-five males and five males, each of which scores were summed and divided by the number of people.
표 5. 산채음료의 관능검사 결과Table 5. Sensory Test Results of Wild Vegetable Beverage
<시험예 2><Test Example 2>
남녀 각각 25명으로 구성된 관능평가 요원으로 하여금 5점 척도법에 의하여 상기 실시예 4에 의한 시료 5, 시료 6, 시료 7 및 시료 8의 맛에 대한 관능평가를 실시하여 그 결과를 아래의 표 5에 나타내었다.Sensory evaluation personnel consisting of 25 men and women each performed sensory evaluation on the taste of Sample 5, Sample 6, Sample 7 and Sample 8 according to Example 4 by the 5-point scale method and the results are shown in Table 5 below. Indicated.
관능검사 결과는 남녀 각각 25명이 5점을 만점으로 하여 각각의 점수를 합한 후 이를 인원수로 나눈 결과로서 소수점 2자리에서 반올림한 결과이다.The result of sensory test was the result of twenty-five males and five males, each of which scores were summed and divided by the number of people.
표 6. 산채 추출물 분말을 함유한 타블렛의 관능검사 결과Table 6. Sensory Test Results of Tablets Containing Wild Vegetable Extract Powder
본 발명은 우리나라 야산에서 자생하거나 재배하고 있는 산채인 참취, 곰취 및 섬쑥부쟁이에서 전자공여능 등 항산화력이 우수한 성분을 마이크로웨이브 및 용매를 이용하여 효율적으로 추출하고 기호성과 편이성을 부여함으로서 산채류의 이용도를 높이고 소비자의 건강향상도를 제고할 수 있는 참취, 곰취 및 섬쑥부쟁이등 산채를 이용한 산채음료 및 그 제조방법을 제공함으로서 관련산업의 발전과 국민건강에 크게 기여할 수 있다.The present invention effectively extracts the components with excellent antioxidant power, such as electron donating ability, from the wild cherries, bear odors, and wormwood cultivated wild vegetables grown or cultivated in Yasan, Korea by using microwaves and solvents and by using palatability and convenience It can contribute greatly to the development of related industries and public health by providing wild vegetable drinks using wild vegetables and manufacturing methods of wild vegetables such as sesame, bear and wormwood that can improve the health and improve the health of consumers.
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KR100478301B1 (en) * | 2001-08-03 | 2005-03-24 | 성덕모 | Method for extracting wild plants used in composition for healthy food capable of removing toxic oxygen |
WO2014185641A2 (en) * | 2013-05-14 | 2014-11-20 | Park Jong-Eon | Method for preparing health food supplement containing aster scaber |
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KR100478301B1 (en) * | 2001-08-03 | 2005-03-24 | 성덕모 | Method for extracting wild plants used in composition for healthy food capable of removing toxic oxygen |
WO2014185641A2 (en) * | 2013-05-14 | 2014-11-20 | Park Jong-Eon | Method for preparing health food supplement containing aster scaber |
KR101486328B1 (en) * | 2013-05-14 | 2015-01-26 | 박종언 | Producing method of health supplement food containing aster scaber |
WO2014185641A3 (en) * | 2013-05-14 | 2015-04-09 | 박종언 | Method for preparing health food supplement containing aster scaber |
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