KR102221339B1 - Method for producing functional tea and Sikhae comprising Gardenia jasminoides - Google Patents
Method for producing functional tea and Sikhae comprising Gardenia jasminoides Download PDFInfo
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- KR102221339B1 KR102221339B1 KR1020190075918A KR20190075918A KR102221339B1 KR 102221339 B1 KR102221339 B1 KR 102221339B1 KR 1020190075918 A KR1020190075918 A KR 1020190075918A KR 20190075918 A KR20190075918 A KR 20190075918A KR 102221339 B1 KR102221339 B1 KR 102221339B1
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- gardenia
- drying
- crushed
- medicinal plant
- tea
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- 241000411851 herbal medicine Species 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 210000002429 large intestine Anatomy 0.000 description 1
- 229940010454 licorice Drugs 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 239000000401 methanolic extract Substances 0.000 description 1
- XJMPAUZQVRGFRE-AYDWLWLASA-N methyl (1s,4as,7s,7as)-7-hydroxy-7-(hydroxymethyl)-1-[(2s,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy-4a,7a-dihydro-1h-cyclopenta[c]pyran-4-carboxylate Chemical compound O([C@@H]1OC=C([C@@H]2[C@H]1[C@](C=C2)(O)CO)C(=O)OC)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O XJMPAUZQVRGFRE-AYDWLWLASA-N 0.000 description 1
- GFSFCSVOGLOXMO-UHFFFAOYSA-N methyl deacetylasperuloside Natural products COCC1=CC2OC(=O)C3=COC(OC4OC(CO)C(O)C(O)C4O)C1C23 GFSFCSVOGLOXMO-UHFFFAOYSA-N 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 125000000896 monocarboxylic acid group Chemical group 0.000 description 1
- 229940116369 pancreatic lipase Drugs 0.000 description 1
- 150000003904 phospholipids Chemical class 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- YQUVCSBJEUQKSH-UHFFFAOYSA-N protochatechuic acid Natural products OC(=O)C1=CC=C(O)C(O)=C1 YQUVCSBJEUQKSH-UHFFFAOYSA-N 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 239000000932 sedative agent Substances 0.000 description 1
- 230000001624 sedative effect Effects 0.000 description 1
- 210000002966 serum Anatomy 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 229950000244 sulfanilic acid Drugs 0.000 description 1
- WKOLLVMJNQIZCI-UHFFFAOYSA-N vanillic acid Chemical compound COC1=CC(C(O)=O)=CC=C1O WKOLLVMJNQIZCI-UHFFFAOYSA-N 0.000 description 1
- TUUBOHWZSQXCSW-UHFFFAOYSA-N vanillic acid Natural products COC1=CC(O)=CC(C(O)=O)=C1 TUUBOHWZSQXCSW-UHFFFAOYSA-N 0.000 description 1
- SSFMJKGLSYRLSQ-UHFFFAOYSA-N vanillic acid 4-O-beta-D-(6'-sinapoyl)glucopyranoside Natural products COC1=CC(C(O)=O)=CC=C1OC1C(O)C(O)C(O)C(COC(=O)C=CC=2C=C(OC)C(O)=C(OC)C=2)O1 SSFMJKGLSYRLSQ-UHFFFAOYSA-N 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
- A23F3/14—Tea preparations, e.g. using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/30—Further treatment of dried tea extract; Preparations produced thereby, e.g. instant tea
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/10—Products from fruits or vegetables; Preparation or treatment thereof of tuberous or like starch containing root crops
- A23L19/105—Sweet potatoes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/20—Malt products
- A23L7/25—Fermentation of cereal malt or of cereal by malting
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/14—Extraction
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Biotechnology (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
본 발명은 (1) 치자 열매를 절단하여 분리한 치자 열매 과실과 씨를 건조한 후 분쇄하는 단계; (2) 흰민들레를 증열 처리하고 건조한 후 분쇄하는 단계; (3) 우엉을 건조한 후 볶고 분쇄하는 단계; (4) 아카시아꽃을 건조한 후 분쇄하는 단계; (5) 상기 (2)단계의 분쇄한 흰민들레, 상기 (3)단계의 분쇄한 우엉, 상기 (4)단계의 분쇄한 아카시아꽃 및 상기 (1)단계의 분쇄한 치자씨를 혼합한 약용식물 혼합물에 물을 첨가한 후 추출하여 약용식물 추출액을 제조하는 단계; (6) 상기 (1)단계의 분쇄한 치자 열매 과실에 상기 (5)단계의 제조한 약용식물 추출액을 분무한 후 증열 처리하는 단계; 및 (7) 상기 (6)단계의 증열 처리한 치자를 건조한 후 볶는 단계를 포함하여 제조하는 것을 특징으로 하는 치자차의 제조방법 및 상기 방법으로 제조된 치자차와 상기 치자차를 이용한 치자 고구마 식혜의 제조방법에 관한 것이다.The present invention comprises the steps of: (1) drying the gardenia fruit and seeds separated by cutting the gardenia fruit and pulverizing it; (2) steaming and drying the white dandelion and pulverizing it; (3) drying the burdock, then roasting and grinding; (4) pulverizing after drying the acacia flowers; (5) A medicinal plant mixture in which the crushed white dandelion in step (2), crushed burdock in step (3), crushed acacia flower in step (4), and crushed gardenia seeds in step (1) are mixed Preparing a medicinal plant extract by extracting after adding water to it; (6) spraying the extract of the medicinal plant prepared in step (5) on the pulverized gardenia fruit of step (1), followed by vaporization treatment; And (7) a method for producing gardenia tea, characterized in that it comprises the step of drying and roasting the gardenia obtained by the heat treatment of step (6), and gardenia sweet potato sikhye using the gardenia tea prepared by the method and the gardenia tea It relates to a method of manufacturing.
Description
본 발명은 전처리한 치자 열매 과실에 약용식물 추출액을 분무한 후 증열 처리하고 건조한 후 볶는 단계를 포함하여 제조하는 것을 특징으로 하는 치자차의 제조방법 및 상기 방법으로 제조된 치자차와 상기 치자차를 이용한 치자 고구마 식혜의 제조방법에 관한 것이다.The present invention comprises the step of spraying a medicinal plant extract on the pretreated gardenia fruit, then vaporizing, drying, and roasting, and the gardenia tea and the gardenia tea prepared by the above method It relates to a method of manufacturing the used gardenia sweet potato sikhye.
치자(Gardenia jasminoides)는 꼭두서니과(Rubiaceae)에 속하는 상록활엽 관목으로 한방에서 소염, 해열, 이뇨, 지혈, 진정, 이담, 혈압강하제로 사용되어 왔다. 치자의 황금색 색소는 식용 및 염료로서 오랫동안 이용되어온 색소로 카로티노이드(carotenoid)계의 크로세틴(crocetin)의 COOH기에 여러 가지 당이 결합된 배당체로 구성되어 있으며, 그 중 크로세틴 D-젠티오바이오사이드(crocetin D-gentiobioside)인 크로신(crocin)이 주성분으로 알려져 있다. 또한, 이리도이드(iridoid) 화합물인 게니핀(genipin), 게니포사이드(geniposide), 제니포시딕산(geniposidic acid), 가르데노사이드(gardenoside), 가도사이드(gardoside), 산지사이드(shanzhiside), 메틸 디아세틸 아스퍼루로사이드(methyl deacetyl asperuloside) 등과 플라보노이드(flavonoids) 계열의 가데닌(gardenin), 항염 활성 성분인 퀸산(quinic acid)과 그 유도체, 바닐릭산 4-O-β-D-(6'-시나포일) 글루코피라노사이드(vanillic acid 4-O-β-D-(6'-sinapoyl) glucopyranoside), 카페익산(caffeic acid) 등이 함유되어 있다. 치자 추출물은 피부미백 효과, MAO(monoamine oxidase) 저해 및 항염증 효과가 있는 것으로 보고되어 있다. 특히 치자의 게니포사이드(geniposide)는 혈청 트리글리세리드(triglyceride), 인지질, 지질과산화물, 간 트리글리세리드, 유리지방산 및 GPT(glutamic pyruvic transaminase) 값을 감소시키고 담즙 분비를 촉진하는 것으로 보고되어 있다. 그밖에 크로신(crocin)이 췌장 리파아제(pancreatic lipase)의 활성을 차단하여 LDL(low density lipoprotein)과 VLDL(very low density lipoprotein)의 수치를 낮추고, 대장에서의 지방 배설을 촉진함으로써 혈중지질의 양을 감소시키는 것으로 알려져 있다. Gardenia jasminoides is an evergreen broad-leaved shrub belonging to the Rubiaceae family, and has been used in herbal medicine as an anti-inflammatory, antipyretic, diuretic, hemostatic, sedative, ear infection, and blood pressure lowering agent. The golden pigment of gardenia is a pigment that has been used for a long time as food and dye. It is composed of glycosides in which various sugars are bonded to the COOH group of carotenoid-based crocetin. Among them, Crocetin D-Genthiobioside (crocetin D-gentiobioside), crocin, is known as the main component. In addition, iridoid compounds genipin, geniposide, geniposidic acid, gardenoside, gadoside, shanzhiside, methyl di Gardenin of flavonoids such as methyl deacetyl asperuloside, quinic acid and its derivatives, which are anti-inflammatory active ingredients, vanillic acid 4-O-β-D-(6'-) Cinafoyl) glucopyranoside (vanillic acid 4-O-β-D-(6'-sinapoyl) glucopyranoside) and caffeic acid. Gardenia extract has been reported to have skin whitening effect, MAO (monoamine oxidase) inhibition and anti-inflammatory effects. In particular, geniposide of gardenia has been reported to reduce serum triglycerides, phospholipids, lipid peroxides, liver triglycerides, free fatty acids and glutamic pyruvic transaminase (GPT) values and promote bile secretion. In addition, crocin blocks the activity of pancreatic lipase, lowering the levels of low density lipoprotein (LDL) and very low density lipoprotein (VLDL), and promoting the excretion of fat in the large intestine, thereby reducing the amount of blood lipids. It is known to reduce.
식혜는 우리나라 전통 음료 중 하나로, 명절, 제례를 비롯하여 대소연회 및 일상식의 후식으로 이용되고 있으며, 캔음료 등과 같이 산업적으로 대량 생산되고 있다. 식혜의 조리법은 조리서마다 약간의 차이가 있으나, 기본조건은 엿기름 가루를 우려낸 물에 고두밥을 넣고 따뜻한 온도를 유지하면서 일정 시간을 삭혀서 만든 것이다. 식혜는 보통 단술 또는 감주라고 부르나, 밥알을 띄워서 먹는 것을 식혜라고 하고 다 삭은 것을 끓여서 밥알은 건져내고 물만 먹는 것을 감주라고 구별하기도 한다. 최근 전통음료인 식혜의 보급화, 고급화, 다양화 등을 위해 생리활성 물질이 강화된 식혜 개발의 필요성이 대두하고 있다.Sikhye is one of the traditional beverages in Korea, and is used as a dessert for large and small banquets and daily meals, including holidays and ceremonies, and is mass produced industrially, such as canned beverages. The recipe for Sikhye differs slightly from one recipe to another, but the basic condition is that it is made by adding godubap in malt powder and brewing it for a certain time while maintaining a warm temperature. Sikhye is usually called dansul or gamju, but it is also called sikhye, which is eaten with floating rice grains, and gamju, which eats only water while boiled, to remove the rice. Recently, the necessity of developing Sikhye enhanced with physiologically active substances has emerged for the popularization, high-end, and diversification of Sikhye, a traditional drink.
한국공개특허 제2009-0124303호에는 천연 치자 색소를 이용한 감귤 기능성 음료의 제조방법이 개시되어 있고, 한국등록특허 제0533284호에는 기능성 한방 식혜의 제조방법이 개시되어 있으나, 본 발명의 치자를 함유하는 기능성 차와 식혜의 제조방법과는 상이하다.Korean Patent Publication No. 2009-0124303 discloses a method of manufacturing a citrus functional beverage using natural gardenia pigments, and Korean Patent No. 0533284 discloses a method of manufacturing functional herbal sikhye, but containing the gardenia of the present invention. It is different from the manufacturing method of functional tea and sikhye.
본 발명은 상기와 같은 요구에 의해 안출된 것으로서, 본 발명의 목적은 치자차의 품질 및 기호도를 증진시킬 수 있는 특정 약용식물의 종류를 선정한 후, 전처리, 증열, 건조 등의 제조조건을 최적화하여 다양한 기능성 성분 및 생리활성이 우수하면서 기호도가 증진된 치자차와 이를 이용한 식혜의 제조방법을 제공하는 데 있다.The present invention was conceived in response to the above requirements, and an object of the present invention is to optimize the manufacturing conditions such as pretreatment, vaporization, drying, etc. after selecting the kind of specific medicinal plant that can improve the quality and preference of gardenia tea. It is to provide a variety of functional ingredients and excellent physiological activity and improved palatability of gardenia tea and a method of manufacturing sikhye using the same.
상기 과제를 해결하기 위해, 본 발명은 (1) 치자 열매를 절단하여 분리한 치자 열매 과실과 씨를 건조한 후 분쇄하는 단계; (2) 흰민들레를 증열 처리하고 건조한 후 분쇄하는 단계; (3) 우엉을 건조한 후 볶고 분쇄하는 단계; (4) 아카시아꽃을 건조한 후 분쇄하는 단계; (5) 상기 (2)단계의 분쇄한 흰민들레, 상기 (3)단계의 분쇄한 우엉, 상기 (4)단계의 분쇄한 아카시아꽃 및 상기 (1)단계의 분쇄한 치자씨를 혼합한 약용식물 혼합물에 물을 첨가한 후 추출하여 약용식물 추출액을 제조하는 단계; (6) 상기 (1)단계의 분쇄한 치자 열매 과실에 상기 (5)단계의 제조한 약용식물 추출액을 분무한 후 증열 처리하는 단계; 및 (7) 상기 (6)단계의 증열 처리한 치자를 건조한 후 볶는 단계를 포함하여 제조하는 것을 특징으로 하는 치자차의 제조방법을 제공한다.In order to solve the above problems, the present invention comprises the steps of: (1) drying and pulverizing the gardenia fruit and seeds separated by cutting the gardenia fruit; (2) steaming and drying the white dandelion and pulverizing it; (3) drying the burdock, then roasting and grinding; (4) pulverizing after drying the acacia flowers; (5) A medicinal plant mixture in which the crushed white dandelion in step (2), crushed burdock in step (3), crushed acacia flower in step (4), and crushed gardenia seeds in step (1) are mixed Preparing a medicinal plant extract by extracting after adding water to it; (6) spraying the extract of the medicinal plant prepared in step (5) on the pulverized gardenia fruit fruit in step (1), and then vaporizing treatment; And (7) it provides a method for producing a gardenia tea, characterized in that it comprises a step of roasting after drying the heat-treated gardenia in step (6).
또한, 본 발명은 상기 방법으로 제조된 치자차를 제공한다.In addition, the present invention provides a gardenia tea manufactured by the above method.
또한, 본 발명은 (1) 상기 치자차를 추출하여 치자차 추출액을 제조하는 단계; (2) 상기 (1)단계의 제조한 치자차 추출액에 엿기름 물 및 고두밥을 혼합한 후 당화시켜 식혜를 제조하는 단계; (3) 고구마에 상기 (1)단계의 제조한 치자차 추출액을 첨가한 후 찌고 으깨는 단계; 및 (4) 상기 (2)단계의 제조한 식혜에 상기 (3)단계의 으깬 고구마를 첨가한 후 끓이는 단계를 포함하여 제조하는 것을 특징으로 하는 치자 고구마 식혜의 제조방법을 제공한다.In addition, the present invention comprises the steps of (1) extracting the gardenia tea to prepare an extract of gardenia tea; (2) mixing malt water and godubap in the gardenia tea extract prepared in step (1) and saccharifying to prepare sikhye; (3) steaming and crushing after adding the gardenia tea extract prepared in step (1) to the sweet potato; And (4) adding the mashed sweet potato of the step (3) to the sikhye prepared in step (2) and then boiling it. It provides a method for producing a gardenia sweet potato sikhye, characterized in that it is prepared.
본 발명의 치자차는 구수하고 온화한 맛으로 인해 기호도가 우수하면서 다량의 기능성 성분 및 항산화 활성이 우수한 이점이 있다. 또한, 상기 치자차를 이용하여 식혜 제조 시 종래의 식혜에 비해 기능성이 높고 유색 식혜로 제조가 가능하여 컬러푸드에 대한 색감에 대한 기호도와 풍미가 우수한 식혜로 제조할 수 있다.Gardenia tea of the present invention has the advantage of excellent palatability due to its savory and mild taste, and has a large amount of functional ingredients and excellent antioxidant activity. In addition, when making sikhye using the gardenia tea, it has higher functionality than conventional sikhye and can be manufactured as colored sikhye, so that sikhye with excellent color preference and flavor for color food can be manufactured.
본 발명의 목적을 달성하기 위하여, 본 발명은In order to achieve the object of the present invention, the present invention
(1) 치자 열매를 절단하여 분리한 치자 열매 과실과 씨를 건조한 후 분쇄하는 단계;(1) cutting the gardenia fruit and drying the separated gardenia fruit and seeds, followed by grinding;
(2) 흰민들레를 증열 처리하고 건조한 후 분쇄하는 단계;(2) steaming and drying the white dandelion and pulverizing it;
(3) 우엉을 건조한 후 볶고 분쇄하는 단계;(3) drying the burdock, then roasting and grinding;
(4) 아카시아꽃을 건조한 후 분쇄하는 단계;(4) pulverizing after drying the acacia flowers;
(5) 상기 (2)단계의 분쇄한 흰민들레, 상기 (3)단계의 분쇄한 우엉, 상기 (4)단계의 분쇄한 아카시아꽃 및 상기 (1)단계의 분쇄한 치자씨를 혼합한 약용식물 혼합물에 물을 첨가한 후 추출하여 약용식물 추출액을 제조하는 단계;(5) A medicinal plant mixture in which the crushed white dandelion in step (2), crushed burdock in step (3), crushed acacia flower in step (4), and crushed gardenia seeds in step (1) are mixed Preparing a medicinal plant extract by extracting after adding water to it;
(6) 상기 (1)단계의 분쇄한 치자 열매 과실에 상기 (5)단계의 제조한 약용식물 추출액을 분무한 후 증열 처리하는 단계; 및(6) spraying the extract of the medicinal plant prepared in step (5) on the pulverized gardenia fruit fruit in step (1), and then vaporizing treatment; And
(7) 상기 (6)단계의 증열 처리한 치자를 건조한 후 볶는 단계를 포함하여 제조하는 것을 특징으로 하는 치자차의 제조방법을 제공한다.(7) It provides a method for producing a gardenia tea, characterized in that it comprises the step of roasting after drying the gardenia steamed in step (6).
본 발명의 치자차의 제조방법에서, 상기 (1)단계는 바람직하게는 치자 열매를 절단하여 분리한 치자 열매 과실과 씨를 55~60℃에서 12~16시간 동안 건조한 후 분쇄할 수 있다.In the manufacturing method of the gardenia tea of the present invention, the step (1) may preferably be pulverized after cutting the gardenia fruit and drying the separated gardenia fruit and seeds at 55 to 60°C for 12 to 16 hours.
또한, 본 발명의 치자차의 제조방법에서, 상기 (2)단계는 바람직하게는 흰민들레를 90~100℃에서 2~3분 동안 증열 처리하고 55~60℃에서 12~16시간 동안 건조한 후 분쇄할 수 있으며, 더욱 바람직하게는 흰민들레를 100℃에서 2~3분 동안 증열 처리하고 55~60℃에서 12~16시간 동안 건조한 후 분쇄할 수 있다.In addition, in the manufacturing method of the gardenia tea of the present invention, step (2) is preferably heat treated at 90 to 100°C for 2 to 3 minutes, dried at 55 to 60°C for 12 to 16 hours, and then pulverized It can be, more preferably, the white dandelion may be pulverized after vaporizing treatment at 100° C. for 2 to 3 minutes and drying at 55 to 60° C. for 12 to 16 hours.
또한, 본 발명의 치자차의 제조방법에서, 상기 (3)단계는 바람직하게는 우엉을 55~60℃에서 12~16시간 동안 건조하고 160~170℃에서 4~6분 동안 볶고 분쇄할 수 있으며, 더욱 바람직하게는 우엉을 55~60℃에서 12~16시간 동안 건조하고 160~170℃에서 5분 동안 볶고 분쇄할 수 있다.In addition, in the manufacturing method of the gardenia tea of the present invention, step (3) is preferably dried burdock at 55 to 60°C for 12 to 16 hours and roasted and crushed at 160 to 170°C for 4 to 6 minutes, and , More preferably, burdock may be dried at 55 to 60°C for 12 to 16 hours and roasted at 160 to 170°C for 5 minutes and pulverized.
또한, 본 발명의 치자차의 제조방법에서, 상기 (4)단계는 바람직하게는 아카시아꽃을 50~55℃에서 10~14시간 동안 건조한 후 분쇄할 수 있으며, 더욱 바람직하게는 아카시아꽃을 50~55℃에서 12시간 동안 건조한 후 분쇄할 수 있다.In addition, in the method for producing gardenia tea of the present invention, the step (4) is preferably dried at 50 to 55°C for 10 to 14 hours and then pulverized, and more preferably 50 to the acacia flowers After drying for 12 hours at 55 ℃ can be pulverized.
상기 (1) 내지 (4)단계와 같이 약용식물을 전처리하는 것이 약용식물 특유의 풋내와 쓴맛은 저감시키면서 고품질의 치자차 제조에 적합한 약용식물로 준비할 수 있었다.Pretreatment of the medicinal plant as in steps (1) to (4) was able to prepare a medicinal plant suitable for producing high-quality gardenia tea while reducing the greeniness and bitterness peculiar to medicinal plants.
또한, 본 발명의 치자차의 제조방법에서, 상기 (5)단계의 약용식물 추출액은 바람직하게는 약용식물 혼합물 총 중량 기준으로, 분쇄한 흰민들레 27~33 중량%, 분쇄한 우엉 36~44 중량%, 분쇄한 아카시아꽃 18~22 중량% 및 분쇄한 치자씨 8~12 중량%를 혼합한 약용식물 혼합물에 물을 10~15배(v/w) 첨가한 후 90~100℃에서 10~14시간 동안 추출하여 제조할 수 있으며, 더욱 바람직하게는 약용식물 혼합물 총 중량 기준으로, 분쇄한 흰민들레 30 중량%, 분쇄한 우엉 40 중량%, 분쇄한 아카시아꽃 20 중량% 및 분쇄한 치자씨 10 중량%를 혼합한 약용식물 혼합물에 물을 10~15배(v/w) 첨가한 후 95℃에서 12시간 동안 추출하여 제조할 수 있다. 상기와 같은 재료 종류, 배합비 및 추출조건으로 제조한 약용식물 추출액을 이용하여 치자차를 제조하는 것이 총 페놀 및 플라보노이드 함량이 증진되고 항산화 활성이 우수하면서 부드러운 풍미로 인해 기호도가 우수한 치자차로 제조할 수 있었다.In addition, in the method for producing gardenia tea of the present invention, the medicinal plant extract of step (5) is preferably based on the total weight of the medicinal plant mixture, pulverized white dandelion 27 to 33 wt%, crushed burdock 36 to 44 wt %, 10 to 15 times (v/w) of water was added to the medicinal plant mixture of 18 to 22% by weight of crushed acacia flowers and 8 to 12% by weight of crushed gardenia seeds, and then 10 to 14 at 90 to 100℃ It can be prepared by extraction for a period of time, and more preferably, based on the total weight of the medicinal plant mixture, crushed white dandelion 30% by weight, crushed burdock 40% by weight, crushed acacia flower 20% by weight, and crushed gardenia seed 10% by weight It can be prepared by adding water 10 to 15 times (v/w) to the mixed% medicinal plant mixture and then extracting at 95° C. for 12 hours. The production of Gardenia tea using the extract of medicinal plants prepared with the above material types, mixing ratios and extraction conditions increases the total phenol and flavonoid content, has excellent antioxidant activity, and has excellent palatability due to its soft flavor. there was.
또한, 본 발명의 치자차의 제조방법에서, 상기 (6)단계는 바람직하게는 분쇄한 치자 열매 과실에 약용식물 추출액을 0.8~1.2:0.8~1.2(w:v) 비율로 분무한 후 90~100℃에서 2~3분 동안 증열 처리할 수 있으며, 더욱 바람직하게는 분쇄한 치자 열매 과실에 약용식물 추출액을 1:1(w:v) 비율로 분무한 후 100℃에서 2~3분 동안 증열 처리할 수 있다. 상기와 같은 조건으로 증열 처리하는 것이 약용식물 추출액과 잘 어우러지면서 기능성 성분 및 항산화 활성이 더욱 증진된 치자차로 제조할 수 있었다.In addition, in the method for producing gardenia tea of the present invention, step (6) is preferably sprayed with a medicinal plant extract on the pulverized gardenia fruit in a ratio of 0.8 to 1.2: 0.8 to 1.2 (w: v), and then 90 to Evaporation treatment can be performed at 100°C for 2 to 3 minutes, and more preferably, a medicinal plant extract is sprayed on the pulverized gardenia fruit at a ratio of 1:1 (w:v), and then heated at 100°C for 2 to 3 minutes. You can handle it. Heat treatment under the same conditions as described above could be prepared as a gardenia tea having a functional ingredient and antioxidant activity further enhanced while being well harmonized with the medicinal plant extract.
또한, 본 발명의 치자차의 제조방법에서, 상기 (7)단계는 바람직하게는 증열 처리한 치자를 55~60℃에서 6~8시간 건조한 후 160~170℃에서 4~6분간 볶을 수 있으며, 더욱 바람직하게는 증열 처리한 치자를 55~60℃에서 6~8시간 건조한 후 160~170℃에서 5분간 볶을 수 있다. 상기와 같은 조건으로 건조한 후 볶음 처리하는 것이 품질이 우수하면서 고소한 맛과 향이 증진된 치자차로 제조할 수 있었다.In addition, in the manufacturing method of the gardenia tea of the present invention, the step (7) is preferably dried at 55 to 60°C for 6 to 8 hours and then roasted at 160 to 170°C for 4 to 6 minutes, More preferably, the heat-treated gardenia may be dried for 6 to 8 hours at 55 to 60°C and then roasted at 160 to 170°C for 5 minutes. After drying under the same conditions as described above, the roasting treatment was able to produce gardenia tea with excellent quality and enhanced savory taste and aroma.
본 발명의 치자차의 제조방법은, 보다 구체적으로는The method for producing gardenia tea of the present invention, more specifically
(1) 치자 열매를 절단하여 분리한 치자 열매 과실과 씨를 55~60℃에서 12~16시간 동안 건조한 후 분쇄하는 단계;(1) cutting the gardenia fruit and drying the separated gardenia fruit and seeds at 55 to 60° C. for 12 to 16 hours and then pulverizing;
(2) 흰민들레를 90~100℃에서 2~3분 동안 증열 처리하고 55~60℃에서 12~16시간 동안 건조한 후 분쇄하는 단계;(2) evaporating the white dandelion at 90 to 100°C for 2 to 3 minutes, drying at 55 to 60°C for 12 to 16 hours, then pulverizing;
(3) 우엉을 55~60℃에서 12~16시간 동안 건조하고 160~170℃에서 4~6분 동안 볶고 분쇄하는 단계;(3) drying the burdock at 55 to 60°C for 12 to 16 hours, roasting at 160 to 170°C for 4 to 6 minutes and grinding;
(4) 아카시아꽃을 50~55℃에서 10~14시간 동안 건조한 후 분쇄하는 단계;(4) pulverizing after drying the acacia flowers at 50 to 55°C for 10 to 14 hours;
(5) 약용식물 혼합물 총 중량 기준으로, 상기 (2)단계의 분쇄한 흰민들레 27~33 중량%, 상기 (3)단계의 분쇄한 우엉 36~44 중량%, 상기 (4)단계의 분쇄한 아카시아꽃 18~22 중량% 및 상기 (1)단계의 분쇄한 치자씨 8~12 중량%를 혼합한 약용식물 혼합물에 물을 10~15배(v/w) 첨가한 후 90~100℃에서 10~14시간 동안 추출하여 약용식물 추출액을 제조하는 단계;(5) Based on the total weight of the medicinal plant mixture, 27 to 33% by weight of crushed white dandelion in step (2), 36 to 44% by weight of crushed burdock in step (3), crushed in step (4) 10 to 15 times (v/w) water was added to the medicinal plant mixture in which 18 to 22% by weight of acacia flowers and 8 to 12% by weight of crushed gardenia seeds in step (1) are mixed, and then 10 to 15 times (v/w) of water is added. Extracting for ~ 14 hours to prepare a medicinal plant extract;
(6) 상기 (1)단계의 분쇄한 치자 열매 과실에 상기 (5)단계의 제조한 약용식물 추출액을 0.8~1.2:0.8~1.2(w:v) 비율로 분무한 후 90~100℃에서 2~3분 동안 증열 처리하는 단계; 및(6) Spray the medicinal plant extract prepared in step (5) on the pulverized gardenia fruit of step (1) at a ratio of 0.8 to 1.2:0.8 to 1.2 (w:v), and then at 90 to 100°C 2 Vaporizing treatment for ~3 minutes; And
(7) 상기 (6)단계의 증열 처리한 치자를 55~60℃에서 6~8시간 건조한 후 160~170℃에서 4~6분간 볶는 단계를 포함할 수 있으며,(7) It may include the step of drying the gardenia steamed in step (6) for 6 to 8 hours at 55 to 60°C and roasting at 160 to 170°C for 4 to 6 minutes,
더욱 구체적으로는More specifically
(1) 치자 열매를 절단하여 분리한 치자 열매 과실과 씨를 55~60℃에서 12~16시간 동안 건조한 후 분쇄하는 단계;(1) cutting the gardenia fruit and drying the separated gardenia fruit and seeds at 55 to 60° C. for 12 to 16 hours and then pulverizing;
(2) 흰민들레를 100℃에서 2~3분 동안 증열 처리하고 55~60℃에서 12~16시간 동안 건조한 후 분쇄하는 단계;(2) evaporating the white dandelion at 100°C for 2 to 3 minutes, drying at 55 to 60°C for 12 to 16 hours, and then pulverizing;
(3) 우엉을 55~60℃에서 12~16시간 동안 건조하고 160~170℃에서 5분 동안 볶고 분쇄하는 단계;(3) drying the burdock at 55 to 60°C for 12 to 16 hours, roasting at 160 to 170°C for 5 minutes and grinding;
(4) 아카시아꽃을 50~55℃에서 12시간 동안 건조한 후 분쇄하는 단계;(4) pulverizing after drying the acacia flowers at 50 ~ 55 ℃ for 12 hours;
(5) 약용식물 혼합물 총 중량 기준으로, 상기 (2)단계의 분쇄한 흰민들레 30 중량%, 상기 (3)단계의 분쇄한 우엉 40 중량%, 상기 (4)단계의 분쇄한 아카시아꽃 20 중량% 및 상기 (1)단계의 분쇄한 치자씨 10 중량%를 혼합한 약용식물 혼합물에 물을 10~15배(v/w) 첨가한 후 95℃에서 12시간 동안 추출하여 약용식물 추출액을 제조하는 단계;(5) Based on the total weight of the medicinal plant mixture, 30% by weight of crushed white dandelion in step (2), 40% by weight of crushed burdock in step (3), and 20% by weight of crushed acacia flower in step (4) % And 10 to 15 times (v/w) of water to the medicinal plant mixture in which the pulverized gardenia seeds in step (1) are mixed, and then extracted for 12 hours at 95° C. to prepare a medicinal plant extract step;
(6) 상기 (1)단계의 분쇄한 치자 열매 과실에 상기 (5)단계의 제조한 약용식물 추출액을 1:1(w:v) 비율로 분무한 후 100℃에서 2~3분 동안 증열 처리하는 단계; 및(6) Spray the medicinal plant extract prepared in step (5) on the pulverized gardenia fruit in step (1) at a ratio of 1:1 (w:v), and then heat-treat for 2 to 3 minutes at 100°C. Step to do; And
(7) 상기 (6)단계의 증열 처리한 치자를 55~60℃에서 6~8시간 건조한 후 160~170℃에서 5분간 볶는 단계를 포함할 수 있다.(7) It may include the step of roasting the gardenia obtained by the vaporization treatment of step (6) at 55 to 60°C for 6 to 8 hours and then roasting at 160 to 170°C for 5 minutes.
본 발명은 또한, 상기 방법으로 제조된 치자차를 제공한다.The present invention also provides a gardenia tea manufactured by the above method.
본 발명은 또한, 상기 치자차를 이용하여 제조하는 것을 특징으로 하는 치자 고구마 식혜의 제조방법을 제공한다.The present invention also provides a method of manufacturing gardenia sweet potato sikhye, characterized in that it is manufactured using the gardenia tea.
본 발명의 치자 고구마 식혜의 제조방법은, 보다 구체적으로는The manufacturing method of the gardenia sweet potato sikhye of the present invention, more specifically
(1) 치자차에 물을 15~20배(v/w) 첨가한 후 85~90℃에서 20~30분간 추출하여 치자차 추출액을 제조하는 단계;(1) preparing a Gardenia tea extract by adding water 15 to 20 times (v/w) to Gardenia tea and then extracting at 85 to 90°C for 20 to 30 minutes;
(2) 상기 (1)단계의 제조한 치자차 추출액에 엿기름 물 및 고두밥을 3~4:0.8~1.2:0.8~1.2 중량비율로 혼합한 후 50~60℃에서 5~7시간 동안 당화시켜 식혜를 제조하는 단계;(2) After mixing malt water and godubap in a weight ratio of 3-4:0.8-1.2:0.8-1.2 to the gardenia tea extract prepared in step (1), saccharify at 50-60℃ for 5-7 hours Manufacturing a;
(3) 고구마에 상기 (1)단계의 제조한 치자차 추출액을 첨가한 후 찌고 으깨는 단계; 및(3) steaming and crushing after adding the gardenia tea extract prepared in step (1) to the sweet potato; And
(4) 상기 (2)단계의 제조한 식혜에 상기 (3)단계의 으깬 고구마를 8.5~9.5:0.5~1.5(v:w) 비율로 첨가한 후 1~2시간 동안 끓이는 단계를 포함할 수 있으며,(4) adding the mashed sweet potato of the step (3) to the sikhye prepared in step (2) in a ratio of 8.5 to 9.5:0.5 to 1.5 (v:w), and then boiling it for 1 to 2 hours. And
더욱 구체적으로는More specifically
(1) 치자차에 물을 15~20배(v/w) 첨가한 후 85~90℃에서 20~30분간 추출하여 치자차 추출액을 제조하는 단계;(1) preparing a Gardenia tea extract by adding water 15 to 20 times (v/w) to Gardenia tea and then extracting at 85 to 90°C for 20 to 30 minutes;
(2) 상기 (1)단계의 제조한 치자차 추출액에 엿기름 물 및 고두밥을 3.5:1:1 중량비율로 혼합한 후 50~60℃에서 5~7시간 동안 당화시켜 식혜를 제조하는 단계;(2) preparing sikhye by mixing malt water and godubap at a weight ratio of 3.5:1:1 to the gardenia tea extract prepared in step (1) and saccharifying at 50-60° C. for 5-7 hours;
(3) 고구마에 상기 (1)단계의 제조한 치자차 추출액을 첨가한 후 찌고 으깨는 단계; 및(3) steaming and crushing after adding the gardenia tea extract prepared in step (1) to the sweet potato; And
(4) 상기 (2)단계의 제조한 식혜에 상기 (3)단계의 으깬 고구마를 9:1(v:w) 비율로 첨가한 후 1~2시간 동안 끓이는 단계를 포함할 수 있다.(4) After adding the mashed sweet potato of the step (3) to the prepared sikhye of the step (2) in a ratio of 9:1 (v:w), boiling for 1 to 2 hours may be included.
상기와 같은 조건으로 제조된 식혜는 치자와 고구마의 맛과 향이 잘 어우러지고 부드러운 풍미와 감미가 우수한 식혜로 제조할 수 있었다.Sikhye prepared under the above conditions could be prepared as Sikhye with excellent flavor and sweetness, and the taste and aroma of gardenia and sweet potatoes were well harmonized.
이하, 본 발명의 제조예 및 실시예를 들어 상세히 설명한다. 단, 하기 제조예 및 실시예는 본 발명을 예시하는 것일 뿐, 본 발명의 내용이 하기 제조예 및 실시예에 한정되는 것은 아니다.Hereinafter, preparation examples and examples of the present invention will be described in detail. However, the following Preparation Examples and Examples are only illustrative of the present invention, and the content of the present invention is not limited to the following Preparation Examples and Examples.
제조예Manufacturing example 1: One: 치자차Gardenia 제조 Produce
(1) 잘 선별하여 세척한 치자 열매를 5 mm 내외의 크기로 절단하여 분리한 치자 열매 과실과 씨를 55~60℃에서 12~16시간 동안 건조한 후 분쇄하였다.(1) The well-selected and washed gardenia fruit was cut into a size of 5 mm or so, and the separated gardenia fruit and seeds were dried at 55 to 60°C for 12 to 16 hours, and then pulverized.
(2) 잎과 이물질을 제거한 흰민들레를 세척하고 물기를 털어낸 후 100℃의 증기로 2~3분간 증열 처리하고 55~60℃에서 12~16시간 동안 건조한 후 분쇄하였다.(2) The white dandelion from which leaves and foreign substances were removed was washed, dried, and then evaporated with steam at 100℃ for 2~3 minutes, dried at 55~60℃ for 12~16 hours, and then pulverized.
(3) 우엉은 잘 세척하여 5~10 mm의 크기로 절단한 후 55~60℃에서 12~16시간 동안 건조하고 160~170℃에서 5분 동안 볶고 분쇄하였다.(3) Burdock was washed well, cut into a size of 5 to 10 mm, dried at 55 to 60°C for 12 to 16 hours, roasted at 160 to 170°C for 5 minutes, and pulverized.
(4) 아카시아꽃을 50~55℃에서 12시간 동안 건조한 후 분쇄하였다.(4) The acacia flowers were dried at 50-55℃ for 12 hours and then pulverized.
(5) 약용식물 혼합물 총 중량 기준으로, 상기 (2)단계의 분쇄한 흰민들레 30 중량%, 상기 (3)단계의 분쇄한 우엉 40 중량%, 상기 (4)단계의 분쇄한 아카시아꽃 20 중량% 및 상기 (1)단계의 분쇄한 치자씨 10 중량%를 혼합한 약용식물 혼합물에 정제수를 10~15배(v/w) 첨가한 후 95℃에서 12시간 환류 추출하여 약용식물 추출액을 제조하였다.(5) Based on the total weight of the medicinal plant mixture, 30% by weight of crushed white dandelion in step (2), 40% by weight of crushed burdock in step (3), and 20% by weight of crushed acacia flower in step (4) % And 10 to 15 times (v/w) of purified water was added to the medicinal plant mixture in which the pulverized gardenia seed in step (1) was mixed, and then refluxed at 95° C. for 12 hours to prepare a medicinal plant extract. .
(6) 상기 (1)단계의 분쇄한 치자 열매 과실에 상기 (5)단계의 제조한 약용식물 추출액을 1:1(w:v) 비율로 분무한 후 100℃의 증기로 2~3분 동안 증열 처리하였다. (6) Spraying the medicinal plant extract prepared in step (5) on the pulverized gardenia fruit of step (1) at a ratio of 1:1 (w:v) and then using steam at 100° C. for 2 to 3 minutes Evaporation treatment was performed.
(7) 상기 (6)단계의 증열 처리한 치자를 55~60℃에서 6~8시간 건조한 후 160~170℃에서 5분간 볶아 치자차를 제조하였다.(7) Gardenia tea was prepared by drying the heat-treated gardenia in step (6) for 6 to 8 hours at 55 to 60°C and roasting at 160 to 170°C for 5 minutes.
비교예Comparative example 1. One. 치자차Gardenia 제조 Produce
(1) 잘 선별하여 세척한 치자 열매를 55~60℃에서 12~16시간 동안 건조한 후 분쇄하였다.(1) The well-selected and washed gardenia fruit was dried at 55 to 60°C for 12 to 16 hours and then pulverized.
(2) 찜통에 물을 넣고 상기 (1)단계의 분쇄한 치자 열매를 찜통 채반에 올린 후 100℃의 증기로 2~3분 동안 증열 처리하였다. (2) Water was added to the steamer, and the pulverized gardenia fruit in step (1) was placed on a steamer tray, and then vapor-heated at 100°C for 2 to 3 minutes.
(3) 상기 (2)단계의 증열 처리한 치자를 55~60℃에서 6~8시간 건조한 후 160~170℃에서 5분간 볶아 치자차를 제조하였다.(3) Gardenia tea was prepared by drying the heat-treated gardenia in step (2) for 6 to 8 hours at 55 to 60°C and roasting at 160 to 170°C for 5 minutes.
비교예Comparative example 2 내지 4: 2 to 4: 치자차Gardenia 제조 Produce
상기 제조예 1의 방법으로 치자차를 제조하되, 상기 (5)단계의 약용식물 혼합물 배합 시 상기 표 1의 재료 및 배합비로 배합한 약용식물 혼합물을 이용하여 비교예 2 내지 4의 치자차를 제조하였다.Gardenia tea was prepared by the method of Preparation Example 1, but when mixing the medicinal plant mixture in step (5), using a medicinal plant mixture mixed with the materials and mixing ratios of Table 1, to prepare Gardenia tea of Comparative Examples 2 to 4 I did.
비교예Comparative example 5: 5: 치자차Gardenia 제조 Produce
(1) 잘 선별하여 세척한 치자 열매를 5 mm 내외의 크기로 절단하여 분리한 치자 열매 과실과 씨를 70℃에서 8시간 동안 건조한 후 분쇄하였다.(1) The well-selected and washed gardenia fruit was cut into a size of 5 mm or so, and the separated gardenia fruit and seeds were dried at 70°C for 8 hours and then pulverized.
(2) 잎과 이물질을 제거한 흰민들레를 세척하고 물기를 털어낸 후 55~60℃에서 12~16시간 동안 건조한 후 분쇄하였다.(2) The white dandelion from which leaves and foreign substances were removed was washed, dried, and dried at 55~60℃ for 12~16 hours, and then pulverized.
(3) 우엉은 잘 세척하여 5~10 mm의 크기로 절단한 후 45℃에서 24시간 동안 건조하고 140℃에서 5분 동안 볶고 분쇄하였다.(3) Burdock was washed well, cut into a size of 5-10 mm, dried at 45° C. for 24 hours, roasted at 140° C. for 5 minutes, and pulverized.
(4) 아카시아꽃을 100℃의 증기로 2~3분간 증열 처리하고 50~55℃에서 12시간 동안 건조한 후 분쇄하였다.(4) Acacia flowers were evaporated for 2 to 3 minutes with steam at 100°C, dried at 50 to 55°C for 12 hours, and then pulverized.
(5) 약용식물 혼합물 총 중량 기준으로, 상기 (2)단계의 분쇄한 흰민들레 30 중량%, 상기 (3)단계의 분쇄한 우엉 40 중량%, 상기 (4)단계의 분쇄한 아카시아꽃 20 중량% 및 상기 (1)단계의 분쇄한 치자씨 10 중량%를 혼합한 약용식물 혼합물에 정제수를 10~15배(v/w) 첨가한 후 80℃에서 24시간 환류 추출하여 약용식물 추출액을 제조하였다.(5) Based on the total weight of the medicinal plant mixture, 30% by weight of crushed white dandelion in step (2), 40% by weight of crushed burdock in step (3), and 20% by weight of crushed acacia flower in step (4) % And 10 to 15 times (v/w) of purified water was added to the medicinal plant mixture in which the pulverized gardenia seed in step (1) was mixed, and then refluxed at 80° C. for 24 hours to prepare a medicinal plant extract. .
(6) 상기 (1)단계의 분쇄한 치자 열매 과실에 상기 (5)단계의 제조한 약용식물 추출액을 1:1(w:v) 비율로 분무한 후 100℃의 증기로 5분 동안 증열 처리하였다. (6) Spraying the medicinal plant extract prepared in step (5) on the pulverized gardenia fruit in step (1) at a ratio of 1:1 (w:v) and then vaporizing it with steam at 100°C for 5 minutes I did.
(7) 상기 (6)단계의 증열 처리한 치자를 25~30℃에서 16시간 건조한 후 190℃에서 3분간 볶아 치자차를 제조하였다.(7) After drying the gardenia obtained by the vaporization treatment of step (6) for 16 hours at 25 to 30° C. and roasting at 190° C. for 3 minutes, gardenia tea was prepared.
제조예Manufacturing example 2. 치자를 함유한 고구마 식혜 제조 2. Manufacture of sweet potato sikhye containing gardenia
(1) 제조예 1의 제조한 치자차에 정제수를 15~20배(v/w) 첨가한 후 85~90℃에서 20~30분간 추출하여 치자차 추출액을 제조하였다.(1) After 15 to 20 times (v/w) of purified water was added to the prepared gardenia tea in Preparation Example 1, the extract was prepared by extracting at 85 to 90°C for 20 to 30 minutes.
(2) 보리(겉보리:유색보리=1:1)를 혼합한 혼합 보리에 2배에 해당되는 물을 준비하여 18시간 동안 침지하였다. 침지한 보리종자는 1~2일간 평균 1.0 cm 정도의 크기로 발아될 때까지 22±3℃ 범위의 온도 하에서 재배하였다. 새싹 길이가 1 cm 크기로 발아된 맥아를 건조시키기 위해 상기 맥아의 수분 함유량이 13%(v/w)가 될 때까지 50℃의 온풍을 통해 건조시켰다. 건조된 맥아를 분쇄하여 0.5~2.0 ㎜ 크기의 분말상 엿기름을 얻었다. 상기 얻은 엿기름 분말 5 kg을 25 L의 따뜻한 물에 풀어 약 30℃ 정도의 온도에서 4시간 방치한 다음 원심분리기 또는 여과기로 찌꺼기를 제거한 엿기름 물을 제조하였다.(2) Water equivalent to twice the mixed barley mixed with barley (cover barley: colored barley = 1:1) was prepared and immersed for 18 hours. Soaked barley seeds were cultivated under a temperature in the range of 22±3℃ until germination to an average size of 1.0 cm for 1-2 days. In order to dry the germinated malt with a sprout length of 1 cm, the malt was dried through warm air at 50°C until the moisture content of the malt reached 13% (v/w). The dried malt was pulverized to obtain powdery malt having a size of 0.5 to 2.0 mm. 5 kg of the malt powder obtained above was dissolved in 25 L of warm water and allowed to stand at a temperature of about 30° C. for 4 hours, and then debris was removed with a centrifuge or filter to prepare malt water.
(3) 상기 (1)단계의 제조한 치자차 추출액, 상기 (2)단계의 제조한 엿기름 물 및 고두밥을 3.5:1:1 중량비율로 혼합한 후 50~60℃에서 6시간 동안 당화시켜 식혜를 제조하였다.(3) After mixing the gardenia tea extract prepared in step (1), the malt water and godubap prepared in step (2) at a weight ratio of 3.5:1:1, saccharify at 50-60°C for 6 hours to Was prepared.
(4) 절단한 고구마에 상기 (1)단계의 제조한 치자차 추출액을 첨가하여 찐 후 믹서에 갈고 으깨었다.(4) To the cut sweet potatoes, the gardenia tea extract prepared in step (1) was added and steamed, and then ground in a mixer and crushed.
(5) 상기 (3)단계의 제조한 식혜에 상기 (4)단계의 으깬 고구마를 9:1(v:w) 비율로 첨가한 후 1~2시간 동안 끓였다.(5) The mashed sweet potato of the step (4) was added to the sikhye prepared in step (3) in a ratio of 9:1 (v:w), and then boiled for 1 to 2 hours.
비교예Comparative example 5: 치자 식혜 5: gardenia sikhye
상기 제조예 2의 방법으로 식혜를 제조하되, (4) 및 (5)단계는 생략하여 치자 식혜를 제조하였다.Sikhye was prepared by the method of Preparation Example 2, but steps (4) and (5) were omitted to prepare gardenia sikhye.
실시예Example 1: One: 치자차의Gardenia 총 페놀화합물 함량 측정 Measurement of total phenolic compound content
총 페놀화합물 함량은 폴린-데니스(Folin-Denis) 방법에 따라 분석하였다. 시료액 1 ㎖에 증류수 3 ㎖를 넣고 Folin & Ciocalteu's 페놀 시약 1 ㎖를 첨가한 후 27℃ 쉐이킹배스(shaking bath)에서 혼합하였다. 5분 후 NaCO3 포화용액 1 ㎖를 넣고 혼합하여 실온에서 1시간 방치한 후 640 nm에서 분광광도계(UV-1650PC, SHIMADZU)로 흡광도를 측정하였다. 페놀화합물 함량은 카테킨(catechin), 탄닌산(tannic acid), 클로로겐산(chlorogenic acid)의 농도를 이용하여 검량선을 작성한 다음 정량하였다.The total phenolic compound content was analyzed according to the Folin-Denis method. 3 ml of distilled water was added to 1 ml of the sample solution, 1 ml of Folin &Ciocalteu's phenol reagent was added, and the mixture was mixed in a shaking bath at 27°C. After 5 minutes, 1 ml of saturated NaCO 3 solution was added, mixed, and allowed to stand at room temperature for 1 hour, and absorbance was measured at 640 nm with a spectrophotometer (UV-1650PC, SHIMADZU). The content of phenolic compounds was quantified after preparing a calibration curve using the concentrations of catechin, tannic acid, and chlorogenic acid.
제조예 1과 비교예들의 방법으로 제조된 치자차의 총 페놀 함량은 표 2에 나타내었다. 표 2에서 알 수 있는 바와 같이, 클로로겐산 함량이 카테킨과 탄닌산 함량보다 높은 함량을 보였다. 클로로겐산 함량 기준으로 제조예 1의 총 페놀 함량이 69.7 ㎎/㎏으로 가장 높았고 비교예 1이 44.2 ㎎/㎏으로 가장 낮았다. 카테킨과 탄닌산 함량 역시 제조예 1이 각각 43.3과 49.3 ㎎/㎏으로 가장 높게 나타났고, 비교예 1이 각각 21.5과 26.4 ㎎/㎏으로 가장 낮게 나타났다. 따라서 제조예 1의 방법으로 제조된 치자차가 가장 높은 총 페놀 함량을 보여 가장 바람직한 것으로 나타났다.The total phenol content of Gardenia tea prepared by the method of Preparation Example 1 and Comparative Examples is shown in Table 2. As can be seen from Table 2, the content of chlorogenic acid was higher than that of catechin and tannic acid. Based on the chlorogenic acid content, the total phenol content of Preparation Example 1 was the highest at 69.7 mg/kg, and Comparative Example 1 was the lowest at 44.2 mg/kg. The content of catechin and tannic acid was also highest in Preparation Example 1 at 43.3 and 49.3 mg/kg, respectively, and Comparative Example 1 was the lowest at 21.5 and 26.4 mg/kg, respectively. Therefore, the gardenia tea prepared by the method of Preparation Example 1 showed the highest total phenol content and was found to be the most preferable.
실시예Example 2: 2: 치자차의Gardenia 총 플라보노이드 함량 측정 Determination of total flavonoid content
제조예 1과 비교예들의 방법으로 제조된 치자차 1.0 ㎖를 시험관에 취하고 10 ㎖의 디에틸렌 글리콜(diethylen glycol)을 가하여 잘 혼합하였다. 다시 여기에 1N NaOH 0.1 ㎖를 잘 혼합시켜 37℃의 항온수조(water bath)에서 1시간 동안 반응시킨 후 420 nm에서 흡광도를 측정하였다. 공시험은 시료 용액 대신 50% 메탄올 용액을 동일하게 처리하였으며, 표준곡선은 나린진(Sigma Co., USA)을 이용하여 작성하고 이로부터 총 플라보노이드 함량을 구하였다.1.0 ml of Gardenia tea prepared by the method of Preparation Example 1 and Comparative Examples was taken into a test tube, and 10 ml of diethylen glycol was added and mixed well. Again, 0.1 ml of 1N NaOH was well mixed and reacted in a water bath at 37° C. for 1 hour, and the absorbance was measured at 420 nm. In the blank test, a 50% methanol solution was treated in the same manner instead of the sample solution, and a standard curve was prepared using Narinjin (Sigma Co., USA), and the total flavonoid content was calculated from this.
제조예 1과 비교예들의 방법으로 제조된 치자차의 총 플라보노이드 함량을 상기 표 3에 나타내었다. 표 3에서 알 수 있는 바와 같이, 제조예 1의 총 플라보노이드 함량이 22.2 ㎎/㎏으로 가장 높았고 비교예 1이 11 ㎎/㎏으로 가장 낮았다. 따라서 제조예 1의 치자차가 가장 높은 총 플라보노이드 함량을 보여 가장 바람직한 것으로 나타났다.Table 3 shows the total flavonoid content of gardenia tea prepared by the method of Preparation Example 1 and Comparative Examples. As can be seen from Table 3, the total flavonoid content of Preparation Example 1 was the highest at 22.2 mg/kg, and Comparative Example 1 was the lowest at 11 mg/kg. Therefore, the gardenia tea of Preparation Example 1 showed the highest total flavonoid content and was found to be the most preferable.
실시예Example 3: 3: 치자차의Gardenia DPPHDPPH 라디칼Radical 소거능Scavenging ability 시험 exam
제조예 1과 비교예들의 방법으로 제조된 치자차의 수소전자공여능에 의한 항산화 활성을 측정하였다. 각 시료를 메탄올(또는 DMSO) 용매로 용해하여, 900 ㎕의 DPPH 용액(100 uM)과 각 시료 100 ㎕를 혼합하여 교반하였다. 이 혼합 시료를 암소에서 30분간 반응시킨 후 517 nm에서 흡광도를 측정하였다. 수소전자공여능은 각 실험을 3회 반복하여 평균을 낸 다음 대조구에 대한 흡광도의 감소 정도를 다음 식에 의하여 계산하였다.Antioxidant activity by hydrogen electron donating ability of the gardenia tea prepared by the method of Preparation Example 1 and Comparative Examples was measured. Each sample was dissolved in methanol (or DMSO) solvent, and 900 µl of DPPH solution (100 uM) and 100 µl of each sample were mixed and stirred. The mixed sample was reacted in the dark for 30 minutes, and then absorbance was measured at 517 nm. The hydrogen electron donating ability was averaged by repeating each experiment three times, and then the degree of decrease in absorbance for the control was calculated by the following equation.
An = (A0-A)/A0 × 100An = (A 0 -A)/A 0 × 100
An: DPPH 라디칼 소거능에 대한 항산화 활성(%)An: Antioxidant activity against DPPH radical scavenging activity (%)
A0: 시료가 첨가되지 않은 DPPH 용액의 흡광도A 0 : Absorbance of DPPH solution without sample added
A: 반응용액 중의 DPPH와 시료의 반응한 흡광도A: absorbance of the sample with DPPH in the reaction solution
제조예 1과 비교예들의 방법으로 제조된 치자차의 DPPH 라디칼 소거능 결과는 상기 표 4에 나타내었다. 치자차 2500 ppm 농도에서 제조예 1의 DPPH 라디칼 소거능 활성이 72.2%로 가장 높았고, 비교예 1의 경우 51.5%로 가장 낮게 나타났다. 따라서, 제조예 1의 치자차가 가장 높은 DPPH 라디칼 소거능을 보여 항산화성이 가장 높음을 알 수 있었다. The DPPH radical scavenging activity results of the gardenia tea prepared by the method of Preparation Example 1 and Comparative Examples are shown in Table 4 above. At a concentration of 2500 ppm of Gardenia tea, the DPPH radical scavenging activity of Preparation Example 1 was the highest at 72.2%, and in Comparative Example 1, the lowest at 51.5%. Therefore, it was found that the gardenia tea of Preparation Example 1 showed the highest DPPH radical scavenging activity, and thus the antioxidant activity was the highest.
실시예Example 4: 치자차의 아질산염 4: Nitrite of Gardenia Tea 소거능Scavenging ability 시험 exam
치자차 시료의 메탄올 추출물로부터 아질산염 소거작용의 측정은 1mM NaNO2 20 ㎕에 시료의 추출액 40 ㎕와 0.1N HCl(pH 1.2) 또는 0.2M 시트레이트 버퍼(citrate buffer, pH 4.2) 또는 0.2M 시트레이트 버퍼(citrate buffer, pH 6.0)를 140 ㎕ 사용하여 부피를 200 ㎕로 맞추었다. 이 반응액을 37℃ 항온수조에서 1시간 반응시킨 후 2% 아세트산(acetic acid) 1,000 ㎕, 그리스(Griess) 시약(30% 아세트산으로 조제한 1% 설파닐산(sulfanilic acid)과 1% 나프틸아민(naphthylamine)을 1:1 비율로 혼합한 것, 사용 직전에 조제) 80 ㎕를 가하여 잘 혼합시켜 빛을 차단한 상온에서 15분간 반응시킨 후 520 nm에서 흡광도를 측정하여 아래와 같은 식을 이용하여 아질산염 소거능을 구하였다.Measurement of the nitrite scavenging activity from the methanol extract of Gardenia tea sample is 1 mM NaNO 2 in 20 μl of the sample extract 40 μl and 0.1N HCl (pH 1.2) or 0.2M citrate buffer (citrate buffer, pH 4.2) or 0.2M citrate. The volume was adjusted to 200 μl using 140 μl of a buffer (citrate buffer, pH 6.0). After reacting the reaction solution in a constant temperature water bath at 37°C for 1 hour, 1,000 μL of 2% acetic acid, 1% sulfanilic acid prepared with 30% acetic acid and 1% naphthylamine ( naphthylamine) in a 1:1 ratio, prepared immediately before use) 80 µl is added and mixed well, reacted for 15 minutes at room temperature where light is blocked, and absorbance is measured at 520 nm using the following equation. Was obtained.
N(%) = [1-(A-C)/B] × 100N(%) = [1-(A-C)/B] × 100
N: 아질산염 소거능N: nitrite scavenging ability
A: 1 mM NaNO2에 샘플 첨가 1시간 후 흡광도A: Absorbance 1 hour after sample addition to 1 mM NaNO 2
B: 1 mM NaNO2 흡광도B: 1 mM NaNO 2 Absorbance
C: 대조구 흡광도C: control absorbance
치자차의 아질산염 소거능 결과는 상기 표 5에 나타내었다. 표 5에서 알 수 있는 바와 같이, 추출물 1000 ppm 농도에서 제조예 1의 아질산염 소거능 활성이 가장 높았고, 비교예 1이 가장 낮게 나타났다.The results of the nitrite scavenging ability of Gardenia tea are shown in Table 5 above. As can be seen in Table 5, the nitrite scavenging activity of Preparation Example 1 was the highest at the concentration of 1000 ppm of the extract, and Comparative Example 1 was the lowest.
실시예Example 5: 치자차의 관능검사 5: sensory test of gardenia tea
어린이 10명(8~13세, 남녀 5명씩), 청소년 10명(14~18세, 남녀 5명씩), 여성(19~64세) 10명, 남성(19~64세) 10명, 65세 이상 여성 5명, 65세 이상 남성 5명, 총 50명을 대상으로 제조예 1과 비교예들의 방법으로 제조된 치자차를 시음하게 하고 색, 향, 맛 및 종합 기호도 평가를 실시하였다. 5점 척도법(1점: 매우 나쁨, 2점: 나쁨, 3점: 보통, 4점: 좋음, 5점: 매우 좋음)으로 점수를 매겨 그 결과를 표 6에 나타내었다.10 children (8 to 13 years old, 5 men and women each), 10 adolescents (14 to 18 years old, 5 men and women each), 10 women (19 to 64 years old), 10 men (19 to 64 years old), 65 years old Five or more women, five men 65 years or older, and a total of 50 people were subjected to tasting the gardenia tea prepared by the method of Preparation Example 1 and Comparative Examples, and color, aroma, taste, and overall preference were evaluated. The score was scored on a 5-point scale (1 point: very bad, 2 points: bad, 3 points: moderate, 4 points: good, 5 points: very good), and the results are shown in Table 6.
(Color)color
(Color)
(Aroma)incense
(Aroma)
(taste)flavor
(taste)
(Overall acceptability)Overall preference map
(Overall acceptability)
그 결과, 표 6에서 알 수 있는 바와 같이, 제조예 1의 치자차가 비교예들보다 전반적으로 높게 나타나 평가자들에 의해 선호됨을 확인할 수 있었다.As a result, as can be seen in Table 6, it was confirmed that the gardenia difference of Preparation Example 1 was generally higher than that of the comparative examples, which was preferred by the evaluators.
실시예Example 6: 식혜의 관능검사 6: Sikhye's sensory test
제조예 2와 비교예 6의 식혜를 가지고 상기 실시예 5의 방법과 동일한 방법으로 관능검사를 실시하였다.With the sikhye of Preparation Example 2 and Comparative Example 6, a sensory test was performed in the same manner as in Example 5.
(Color)color
(Color)
(Aroma)incense
(Aroma)
(taste)flavor
(taste)
(Overall acceptability)Overall preference map
(Overall acceptability)
표 7에서 알 수 있는 바와 같이, 제조예 2의 식혜가 비교예 6의 식혜에 비해 모든 항목에서 높은 점수를 나타내어, 치자를 이용하여 식혜 제조 시 으깬 고구마를 첨가하여 제조하는 것이 기호도가 증진됨을 확인할 수 있었다.As can be seen from Table 7, the Sikhye of Preparation Example 2 exhibited a higher score in all items than the Sikhye of Comparative Example 6, and thus, it was confirmed that the preference was improved by adding mashed sweet potatoes when preparing Sikhye using gardenia. Could
이상에서 본 발명의 제조예 및 실시예가 제시되어 있지만 본 발명이 상기에 한정되는 것은 아니며 본 발명의 기술 사상 범위 내에서 다양하게 변형 가능하고 이러한 변형은 하기한 본 발명의 청구범위에 속한다 할 것이다.Although the manufacturing examples and examples of the present invention have been presented above, the present invention is not limited to the above, and various modifications are possible within the scope of the technical spirit of the present invention, and such modifications will fall within the scope of the claims of the present invention.
Claims (5)
(2) 흰민들레를 증열 처리하고 건조한 후 분쇄하는 단계;
(3) 우엉을 건조한 후 볶고 분쇄하는 단계;
(4) 아카시아꽃을 건조한 후 분쇄하는 단계;
(5) 약용식물 혼합물 총 중량 기준으로, 상기 (2)단계의 분쇄한 흰민들레 27~33 중량%, 상기 (3)단계의 분쇄한 우엉 36~44 중량%, 상기 (4)단계의 분쇄한 아카시아꽃 18~22 중량% 및 상기 (1)단계의 분쇄한 치자씨 8~12 중량%를 혼합한 약용식물 혼합물에 물을 첨가한 후 추출하여 약용식물 추출액을 제조하는 단계;
(6) 상기 (1)단계의 분쇄한 치자 열매 과실에 상기 (5)단계의 제조한 약용식물 추출액을 분무한 후 증열 처리하는 단계; 및
(7) 상기 (6)단계의 증열 처리한 치자를 건조한 후 볶는 단계를 포함하여 제조하는 것을 특징으로 하는 치자차의 제조방법.(1) cutting the gardenia fruit and drying the separated gardenia fruit and seeds, followed by grinding;
(2) steaming and drying the white dandelion and pulverizing it;
(3) drying the burdock, then roasting and grinding;
(4) pulverizing after drying the acacia flowers;
(5) Based on the total weight of the medicinal plant mixture, 27 to 33% by weight of crushed white dandelion in step (2), 36 to 44% by weight of crushed burdock in step (3), crushed in step (4) Preparing a medicinal plant extract by adding water to the medicinal plant mixture in which 18 to 22% by weight of acacia flowers and 8 to 12% by weight of the pulverized gardenia seeds in the step (1) are mixed, followed by extraction;
(6) spraying the extract of the medicinal plant prepared in step (5) on the pulverized gardenia fruit of step (1), followed by vaporization treatment; And
(7) A method for producing a gardenia tea, characterized in that it comprises the step of drying and roasting the gardenia obtained by the heat treatment of step (6).
(1) 치자 열매를 절단하여 분리한 치자 열매 과실과 씨를 55~60℃에서 12~16시간 동안 건조한 후 분쇄하는 단계;
(2) 흰민들레를 90~100℃에서 2~3분 동안 증열 처리하고 55~60℃에서 12~16시간 동안 건조한 후 분쇄하는 단계;
(3) 우엉을 55~60℃에서 12~16시간 동안 건조하고 160~170℃에서 4~6분 동안 볶고 분쇄하는 단계;
(4) 아카시아꽃을 50~55℃에서 10~14시간 동안 건조한 후 분쇄하는 단계;
(5) 약용식물 혼합물 총 중량 기준으로, 상기 (2)단계의 분쇄한 흰민들레 27~33 중량%, 상기 (3)단계의 분쇄한 우엉 36~44 중량%, 상기 (4)단계의 분쇄한 아카시아꽃 18~22 중량% 및 상기 (1)단계의 분쇄한 치자씨 8~12 중량%를 혼합한 약용식물 혼합물에 물을 10~15배(v/w) 첨가한 후 90~100℃에서 10~14시간 동안 추출하여 약용식물 추출액을 제조하는 단계;
(6) 상기 (1)단계의 분쇄한 치자 열매 과실에 상기 (5)단계의 제조한 약용식물 추출액을 0.8~1.2:0.8~1.2(w:v) 비율로 분무한 후 90~100℃에서 2~3분 동안 증열 처리하는 단계; 및
(7) 상기 (6)단계의 증열 처리한 치자를 55~60℃에서 6~8시간 건조한 후 160~170℃에서 4~6분간 볶는 단계를 포함하여 제조하는 것을 특징으로 하는 치자차의 제조방법.The method of claim 1,
(1) pulverizing after cutting the gardenia fruit and drying the separated gardenia fruit and seeds at 55 to 60° C. for 12 to 16 hours;
(2) evaporating the white dandelion at 90 to 100°C for 2 to 3 minutes, drying at 55 to 60°C for 12 to 16 hours, then pulverizing;
(3) drying the burdock at 55~60℃ for 12~16 hours, roasting at 160~170℃ for 4~6 minutes and grinding;
(4) pulverizing after drying the acacia flowers at 50 to 55°C for 10 to 14 hours;
(5) Based on the total weight of the medicinal plant mixture, 27 to 33% by weight of crushed white dandelion in step (2), 36 to 44% by weight of crushed burdock in step (3), crushed in step (4) 10 to 15 times (v/w) water was added to the medicinal plant mixture in which 18 to 22% by weight of acacia flowers and 8 to 12% by weight of crushed gardenia seeds in step (1) are mixed, and then 10 to 15 times (v/w) of water is added. Extracting for ~ 14 hours to prepare a medicinal plant extract;
(6) Spray the medicinal plant extract prepared in step (5) on the pulverized gardenia fruit of step (1) at a ratio of 0.8 to 1.2:0.8 to 1.2 (w:v), and then at 90 to 100°C 2 Vaporizing treatment for ~3 minutes; And
(7) A method for producing gardenia tea, characterized in that it comprises the step of drying the gardenia (6) heat-treated for 6 to 8 hours at 55 to 60°C and roasting at 160 to 170°C for 4 to 6 minutes .
(2) 상기 (1)단계의 제조한 치자차 추출액에 엿기름 물 및 고두밥을 혼합한 후 당화시켜 식혜를 제조하는 단계;
(3) 고구마에 상기 (1)단계의 제조한 치자차 추출액을 첨가한 후 찌고 으깨는 단계; 및
(4) 상기 (2)단계의 제조한 식혜에 상기 (3)단계의 으깬 고구마를 첨가한 후 끓이는 단계를 포함하여 제조하는 것을 특징으로 하는 치자 고구마 식혜의 제조방법.(1) extracting the gardenia tea of claim 4 to prepare a gardenia tea extract;
(2) preparing sikhye by mixing malt water and godubap in the gardenia tea extract prepared in step (1) and saccharifying;
(3) steaming and crushing after adding the gardenia tea extract prepared in step (1) to the sweet potato; And
(4) A method for producing gardenia sweet potato sikhye, characterized in that it comprises the step of boiling after adding the mashed sweet potato of the step (3) to the sikhye prepared in step (2).
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